IP Library Granted Patent US 8,182,757
Granted Patent B2
US 8,182,757 · App. 13/191,749 · Granted May 22, 2012

Method and apparatus for manufacturing of a calcium carbonate product, the product and its use

Assignee: FP-Pigments Oy
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Quick Facts
Patent No.
US 8,182,757
App. No.
13/191,749
Granted
May 22, 2012
Kind
B2
Abstract

A method and apparatus for producing a calcium carbonate product formed of small <100 μm sized separate calcium carbonate particles. Calcium hydroxide is fed through a disintegration and spraying apparatus ( 14 ), operating on the principle of a pin mill, into a gas which contains carbon dioxide for precipitating calcium carbonate particles and which is inside a precipitation reactor ( 10 ). The temperature in the precipitation reactor is maintained at <65° C.

Claims (13)

1. An apparatus for producing a calcium carbonate product from calcium hydroxide, comprising small calcium carbonate particles, which apparatus comprises

at least one precipitation reactor into which the calcium hydroxide or other corresponding Ca ++ ion source is disintegrated or sprayed as fine drops and/or particles and inside of which the calcium hydroxide is brought into contact with gas which contains carbon dioxide and

apparatuses for feeding the calcium hydroxide or other corresponding Ca ++ ion source into the precipitation reactor, and apparatuses for removing the calcium carbonate product from the precipitation reactor, wherein the apparatus additionally comprises

a disintegration and spraying apparatus, operating on the principle of a pin mill, for disintegrating the calcium hydroxide as small drops and/or particles into the precipitation reactor, wherein the disintegration and spraying apparatus is located inside the precipitation reactor, and

cooling apparatuses for maintaining a lowered temperature in the precipitation reactor.

2. The apparatus according to claim 1 , wherein the cooling apparatuses comprise

apparatuses for lowering the temperature of a material, such as the calcium hydroxide, carbon dioxide or circulating calcium carbonate to be fed into the precipitation reactor and/or

apparatuses for keeping the temperature of the material in the precipitation reactor low.

3. The apparatus according to claim 1 , wherein

the apparatus comprises two or several sequential precipitation reactors which have flow connections to each other, and wherein

coolers for cooling the calcium carbonate material flowing from one reactor to another are arranged between the sequentially arranged precipitation reactors.

4. The apparatus according to claim 1 , wherein the ring speed of the rotors of the disintegration and spraying apparatus operating on the principle of a pin mill is 1-250 m/s, and wherein the speed difference of the rings of the rotors rotating in different or in the same directions, or the speed difference of the rings of adjacent rotors and stators is 5-400 m/s.

5. The apparatus according to claim 4 , wherein the speed difference of the rings of the rotors rotating in different or in the same directions, or the speed difference of the rings of adjacent rotors and stators, is 5-200 m/s.

Priority Claims (1)
FI 20040976 · Jul 13, 2004 · national
Continuity (2)
Division 11631325
Related Publication 20110280777A1 · Nov 17, 2011