Encapsulation compositions and process for preparing the same
Encapsulation compositions in which an encapsulate (A) is encapsulated in a matrix (B) may be prepared by: (i) mixing matrix (B) with a liquid plasticizer and encapsulate (A) in an extruder, to obtain a melted mixture of encapsulate (A) and matrix (B); and (ii) extruding the melted mixture, to obtain an extruded mixture.
1. A process for preparing an encapsulation composition, comprising:
(A) an encapsulate, encapsulated in:
(B) a glassy matrix, said matrix comprising:
60 to 99% by weight, based on the total weight of said matrix (B), of larch gum; and
1 to 40% by weight, based on the total weight of said matrix (B), of a low molecular weight carbohydrate or polyol, wherein said low molecular weight carbohydrate or polyol is selected from the group consisting of glucose, sucrose, maltose, lactose, 42 D.E. corn syrup solid, 36 D.E. corn syrup solid, erythritol, lactitol, mannitol, sorbitol, maltitol, isomalt, xylitol, hydrogenated corn syrup, hydrogenated glucose syrup, hydrogenated maltose syrup, hydrogenated lactose syrup, and a mixture thereof,
and wherein said glassy matrix has a glass transition temperature of from room temperature to 55.7° C.;
said process comprising:
(i) mixing matrix (B) with a liquid plasticizer and encapsulate (A) in an extruder, to obtain a melted mixture which comprises encapsulate (A) and matrix (B); and
(ii) extruding said melted mixture, to obtain an extruded mixture.
2. The process of claim 1 , wherein said liquid plasticizer is selected from the group consisting of water; glycerol; propylene glycol; aqueous solutions of glycerol, propylene glycol, monosaccharides, and disaccharides; and invert and high fructose corn syrups.
3. The process of claim 1 , wherein said liquid plasticizer is water.
4. The process of claim 1 , further comprising cooling said extruded mixture.
5. The process of claim 1 , wherein said encapsulate is selected from the group consisting of medications, pesticides, vitamins, preservatives, and flavoring agents.
6. The process of claim 1 , wherein said encapsulate is a flavoring agent.
7. The process of claim 6 , wherein said flavoring agent is selected from the group consisting of natural extracts, oleoresins, essential oils, protein hydrolysates, aqueous reaction flavors, compounded natural flavors, and artificial flavors.
8. The process of claim 6 , wherein said flavoring agent comprises a plasticizer or an emulsifier.
9. The process of claim 1 , wherein said extruder is a twin screw extruder.
10. The process of claim 1 , wherein said matrix (B) comprises:
60 to 80% by weight, based on the total weight of said matrix (B), of larch gum; and
20 to 40% by weight, based on the total weight of said matrix (B), of said low molecular weight carbohydrate or polyol.
11. The process of claim 1 , wherein said glassy matrix has a glass transition temperature of from 30° C. to 55.7° C.
12. The process of claim 1 , wherein said glassy matrix has a glass transition temperature of from 30° C. to 40° C.