IP Library Granted Patent US 8,278,344
Granted Patent B2
US 8,278,344 · App. 12/859,997 · Granted Oct 2, 2012

Heterocyclic inhibitors of necroptosis

Assignees: The Brigham and Women's Hospital, Inc.; President and Fellows of Harvard College; Tufts University
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Quick Facts
Patent No.
US 8,278,344
App. No.
12/859,997
Granted
Oct 2, 2012
Kind
B2
Abstract

The invention features a series of heterocyclic derivatives that inhibit tumor necrosis factor alpha (TNF-α) induced necroptosis. The heterocyclic compounds of the invention are described by Formulas (I) and (Ia)-(Ie) and are shown to inhibit TNF-α induced necroptosis in FADD-deficient variant of human Jurkat T cells. The invention further features pharmaceutical compositions featuring the compounds of the invention. The compounds and compositions of the invention may also be used to treat disorders where necroptosis is likely to play a substantial role.

Claims (27)

1. A method of treating necrosis or necroptosis in a subject having a condition selected from stroke, myocardial infarction, organ ischemia, traumatic brain injury, liver disease, cancer chemo/radiation therapy-induced necrosis, acute necrotizing pancreatitis, or a neurodegenerative disease, said method comprising the step of administering a compound according to the following formula,

wherein

R 1 is a lower alkyl group;

R 2 is selected from hydrogen and an electron withdrawing group;

R 3 is selected from hydrogen and an (S)-lower alkyl group;

each of R 4 , R 5 , and R 6 is independently selected from hydrogen, lower alkyl, halogen, amino, amido, alkoxy, and cyano; and

each X 1 and X 2 is, independently, halogen;

or any pharmaceutically acceptable salt thereof, or stereoisomer thereof.

2. The method of claim 1 , wherein said condition is a neurodegenerative disease.

3. The method of claim 1 , wherein said condition is stroke, liver disease, myocardial infarction, or retinal ischemia.

4. The method of claim 1 , wherein

R 1 is selected from methyl, ethyl, propyl, and butyl;

R 2 is selected from hydrogen, halogen and cyano; and

R 3 is selected from hydrogen, (S)-methyl, (S)-ethyl, (S)-propyl, and (S)-butyl.

5. The method of claim 4 , wherein

R 1 is selected from methyl and isopropyl;

R 2 is selected from hydrogen, chlorine, bromine and cyano;

R 3 is selected from hydrogen and (S)-methyl; and

each X 1 and X 2 is independently chlorine or fluorine.

6. The method of claim 5 , wherein R 1 is methyl, R 2 is cyano, R 3 is (S)-methyl, X 1 is chlorine, and X 2 is fluorine.

7. A method of treating necrosis or necroptosis in a subject having a condition selected from organ ischemia, traumatic brain injury, liver disease, cancer chemo/radiation therapy-induced necrosis, acute necrotizing pancreatitis, or a neurodegenerative disease, said method comprising the step of administering a compound selected from the group consisting of:

or any pharmaceutically acceptable salt thereof, or stereoisomer thereof,

to said subject in a dosage sufficient to decrease necroptosis or said necrosis.

8. The method of claim 7 , wherein said compound is

or any pharmaceutically acceptable salt thereof, or stereoisomer thereof.

9. The method of claim 7 , wherein said condition is a neurodegenerative disease.

10. The method of claim 7 , wherein said condition is stroke, liver disease, myocardial infarction, or retinal ischemia.

Assignments (4)
CONFIRMATORY LICENSE Recorded Jul 30, 2018
From: HARVARD UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 047260/0782 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 20, 2012
From: CUNY, GREGORY D.; TENG, XIN
To: THE BRIGHAM AND WOMEN'S HOSPITAL, INC.
Reel/Frame 028814/0611 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 20, 2012
From: YUAN, JUNYING
To: PRESIDENT AND FELLOWS OF HARVARD COLLEGE
Reel/Frame 028814/0644 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 20, 2012
From: DEGTEREV, ALEXEI
To: PRESIDENT AND FELLOWS OF HARVARD COLLEGE; TUFTS UNIVERSITY
Reel/Frame 028814/0688 →
Continuity (4)
Continuation 12228750 · Aug 15, 2008
Provisional Application 60955966 · Aug 15, 2007
Provisional Application 61038175 · Mar 20, 2008
Related Publication 20100317701A1 · Dec 16, 2010