IP Library Granted Patent US 8,398,847
Granted Patent B2
US 8,398,847 · App. 12/845,500 · Granted Mar 19, 2013

Method for making a usable hydrocarbon product from used oil

Inventors: Gregory Odell Wallace (Baytown, TX); John G. Schulz (Spring, TX); Benjamin P. Cowart (Houston, TX)
Assignee: Vertex Energy, LP
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Quick Facts
Patent No.
US 8,398,847
App. No.
12/845,500
Granted
Mar 19, 2013
Kind
B2
Abstract

One or more computer implemented methods for continuously processing used oils are provided. The method can include a feedstock tank containing feedstock. The feedstock tank can have a sparger and a level sensor. The feedstock tank can be in fluid communication with a first pump, a first filter, a heater, a second filter, first flow meter, a primary nozzle, a secondary nozzle, a motionless inline static mixer, and a first reactor.

Claims (21)

1. A computer implemented method for processing used oils for a usable hydrocarbon product comprising:

a. providing a feedstock stream;

b. filtering the feedstock stream;

c. heating the feedstock stream;

d. filtering the heated feedstock stream;

e. monitoring a flow rate of the feedstock stream;

f. injecting an aqueous sulfuric acid into the heated feedstock stream;

g. injecting a concentrated sulfuric acid into the heated feedstock stream;

h. blending the aqueous sulfuric acid, concentrated sulfuric acid, and the heated feedstock stream to form a mixed stream;

i. separating the mixed stream into a first interface layer, an intermediate oil product, and a water layer;

j. injecting an aromatic solvent release agent into the intermediate oil product,

k. mixing the intermediate oil product and the aromatic solvent release agent to form a blended intermediate oil product;

l. separating the blended intermediate oil product into a finished oil product, a second interface layer, and a second water layer; and

m. pumping the finished oil product to a first settling tank and allowing any remaining particulate to fall out of solution to form a finished product.

2. The method of claim 1 , further comprising using a heater to heat the feedstock stream.

3. The method of claim 2 , further comprising using steam to heat the heater.

4. The method of claim 1 , further comprising using at least a two stage filter to filter the feedstock stream, wherein each stage is at least a four hundred micron filter.

5. The method of claim 1 , wherein the heated feedstock stream is filtered using a one hundred micron filter.

6. The method of claim 1 , wherein the aqueous sulfuric acid, the concentrated sulfuric acid, or both is injected at a ratio from two gallons per one thousand gallons of feedstock to four gallons per one thousand gallons of feedstock.

7. The method of claim 1 , wherein the first interface layer includes at least fifty percent hydrocarbons.

8. The method of claim 1 , wherein the aromatic solvent release agent is injected at a ratio of from four gallons per one thousand gallons of feedstock to seven gallons per one thousand gallons of feedstock.

Assignments (15)
RELEASE OF SECURITY INTEREST Recorded Feb 7, 2022
From: ENCINA BUSINESS CREDIT, LLC
To: VERTEX ENERGY OPERATING, LLC
Reel/Frame 058910/0210 →
RELEASE OF SECURITY INTEREST Recorded Feb 7, 2022
From: ENCINA BUSINESS CREDIT, LLC
To: VERTEX ENERGY OPERATING, LLC
Reel/Frame 058911/0203 →
CORRECTIVE ASSIGNMENT TO CORRECT THE NATURE OF CONVEYANCE PREVIOUSLY RECORDED AT REEL: 041362 FRAME: 0292. ASSIGNOR(S) HEREBY CONFIRMS THE RELEASE OF SECURITY INTEREST. Recorded Apr 7, 2017
From: MIDCAP BUSINESS CREDIT LLC
To: VERTEX ENERGY OPERATING, LLC
Reel/Frame 042190/0716 →
RELEASE OF SECURITY INTEREST Recorded Mar 31, 2017
From: MIDCAP BUSINESS CREDIT LLC
To: VERTEX ENERGY OPERATING, LLC
Reel/Frame 041815/0639 →
RELEASE OF SECURITY INTEREST Recorded Mar 16, 2017
From: GOLDMAN SACHS BANK USA
To: VERTEX ENERGY OPERATING, LLC; VERTEX REFINING LA, LLC
Reel/Frame 041591/0629 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 23, 2017
From: MIDCAP BUSINESS CREDIT LLC
To: VERTEX ENERGY OPERATING, LLC
Reel/Frame 041362/0292 →
SECURITY INTEREST Recorded Feb 1, 2017
From: VERTEX ENERGY OPERATING, LLC
To: ENCINA BUSINESS CREDIT, LLC, AS AGENT
Reel/Frame 041148/0083 →
SECURITY INTEREST Recorded Feb 1, 2017
From: VERTEX ENERGY OPERATING, LLC
To: ENCINA BUSINESS CREDIT, LLC, AS AGENT
Reel/Frame 041147/0939 →
RELEASE OF SECURITY INTEREST Recorded Apr 8, 2015
From: BANK OF AMERICA, N.A.
To: VERTEX ENERGY OPERATING, LLC; VERTEX REFINING LA, LLC
Reel/Frame 035356/0431 →
SECURITY INTEREST Recorded Apr 1, 2015
From: VERTEX ENERGY OPERATING, LLC
To: MIDCAP BUSINESS CREDIT LLC
Reel/Frame 035307/0785 →
SECURITY INTEREST Recorded May 7, 2014
From: VERTEX REFINING LA, LLC; VERTEX ENERGY OPERATING, LLC
To: BANK OF AMERICA, N.A.
Reel/Frame 032837/0293 →
SECURITY INTEREST Recorded May 2, 2014
From: VERTEX ENERGY OPERATING, LLC; VERTEX REFINING LA, LLC
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 032813/0353 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 10, 2014
From: VERTEX HOLDINGS, LP
To: VERTEX ENERGY OPERATING, LLC
Reel/Frame 032651/0432 →
CHANGE OF NAME Recorded Jul 19, 2012
From: VERTEX ENERGY, LP
To: VERTEX HOLDINGS, LP
Reel/Frame 028603/0055 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 28, 2010
From: WALLACE, GREGORY ODELL; SCHULZ, JOHN G.; COWART, BENJAMIN P.
To: VERTEX ENERGY, LP
Reel/Frame 024754/0881 →
Continuity (2)
Provisional Application 61230214 · Jul 31, 2009
Related Publication 20110024329A1 · Feb 3, 2011