IP Library Granted Patent US 8,574,555
Granted Patent B2
US 8,574,555 · App. 11/670,229 · Granted Nov 5, 2013

Stable one-part aqueous tooth whitening composition

Inventors: James J. Longo, Jr. (Wilmington, DE); William A. McHale (Collegeville, PA)
Assignee: Premier Dental Products Company
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Quick Facts
Patent No.
US 8,574,555
App. No.
11/670,229
Granted
Nov 5, 2013
Kind
B2
Abstract

The invention relates to a high-temperature stable, one-part, aqueous tooth bleaching composition for contacting a tooth surface. The composition comprises a bleaching agent comprising a high level of a aqueous hydrogen peroxide. The bleaching agent is derived from multiple components within the composition and comprises at least about 15% by weight of the total composition weight. The Composition also comprises a bleaching agent stabilizer comprising from about 0.01% to about 1.00% by weight of the total composition weight.

Claims (22)

1. A one-part, aqueous tooth bleaching composition for contacting a tooth surface comprising:

hydrogen peroxide solution;

a crosslinked polyvinylpyrrolidone/hydrogen peroxide complex;

a bleaching agent stabilizer; and

at least 50% by weight of water;

wherein the composition maintains greater than 95% available hydrogen peroxide content after 12 weeks storage at 40 degrees C. with no loss of gel viscosity.

2. The tooth bleaching composition according to claim 1 , wherein the bleaching agent stabilizer comprises a 1:1 ratio by weight of ethylenediaminetetraacetic acid disodium salt and etidronic acid.

3. The tooth bleaching composition according to claim 2 , wherein the ratio by weight of hydrogen peroxide to bleaching agent stabilizer is about 25:1 to about 60:1.

4. The tooth bleaching composition according to claim 1 , wherein the ratio of hydrogen peroxide by weight to bleaching agent stabilizer is about 25:1 to about 60:1.

5. The tooth bleaching composition according to claim 1 , wherein the polyvinylpyrrolidone/hydrogen peroxide complex comprises at least 10.0% by weight of the total composition weight.

6. The tooth bleaching composition according to claim 1 , wherein the bleaching agent stabilizer is selected from a group consisting of ethylenediamineteraacetic acid, disodium salt; ethylenediamineteraacetic acid, tetrasodium salt; ethylenediaminetetraacetic acid, calcium disodium salt; etidronic acid; citric acid; gluconic acid; sodium citrate; sodium gluconate; sodium phosphate; disodium phosphate; trisodium phosphate; tetrapotassium pyrophosphate; sodium tripolyphosphate and potassium stannate.

7. The tooth bleaching composition according to claim 1 , further comprising at least one chelating agent selected from the group consisting of ethylenediamineteraacetic acid, disodium salt; ethylenediamineteraacetic acid, tetrasodium salt; ethylenediaminetetraacetic acid, calcium disodium salt; citric acid; gluconic acid; sodium citrate; sodium gluconate; sodium phosphate; disodium phosphate; trisodium phosphate; tetrapotassium pyrophosphate; and sodium tripolyphosphate.

8. The tooth bleaching composition according to claim 7 , wherein the at least one chelating agent comprises from about 0.01% to about 0.50% by weight of the total composition weight.

9. The tooth bleaching composition according to claim 1 , further comprising at least one chelating agent, the chelating agent being disodium EDTA.

10. The tooth bleaching composition according to claim 1 , further comprising at least one hygroscopic agent selected from the polyol group consisting of glycerin, polyethylene glycol, propylene glycol and sorbitol.

11. The tooth bleaching composition according to claim 10 , wherein the at least one hydroscopic agent comprises from about 1.0% to about 10.0% by weight of the total composition weight.

12. The tooth bleaching composition according to claim 11 , wherein the at least one hygroscopic agent is glycerin.

13. The tooth bleaching composition according to claim 1 , further comprising at least one neutralizing agent selected from a group consisting of triethanolamine, tromethamine, sodium hydroxide, potassium hydroxide, and ammonium hydroxide.

14. The tooth bleaching composition according to claim 13 , wherein the at least one neutralizing agent adjusts the pH of the final tooth whitening composition between about 6.0 to about 7.0.

15. The tooth bleaching composition according to claim 13 , wherein the at least one neutralizing agent comprises from about 0.50% to about 5.00% by weight of the total composition weight.

16. The tooth bleaching composition according to claim 13 , wherein the at least one neutralizing agent is ammonium hydroxide.

17. The tooth bleaching composition according to claim 1 , further comprising at least one chelating agent, the chelating agent being etidronic acid.

Assignments (3)
SECURITY INTEREST Recorded Mar 27, 2025
From: PREMIER DENTAL PRODUCTS COMPANY, LLC
To: FIDELITY DIRECT LENDING LLC, AS ADMINISTRATIVE AGENT
Reel/Frame 070650/0397 →
ENTITY CONVERSION Recorded Mar 17, 2025
From: PREMIER DENTAL PRODUCTS COMPANY
To: PREMIER DENTAL PRODUCTS COMPANY, LLC
Reel/Frame 070537/0105 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 10, 2007
From: LONGO, JAMES J., JR.; MCHALE, WILLIAM A.
To: PREMIER DENTAL PRODUCTS COMPANY
Reel/Frame 019276/0577 →
Continuity (2)
Provisional Application 60764072 · Feb 1, 2006
Related Publication 20070202059A1 · Aug 30, 2007