Ceramic composite material
A ceramic composite material is comprised of a fabric of fibers of an inorganic substance; and a matrix for combining the fibers. The matrix consists essentially of a ceramic. The matrix is formed by burying the fabric in a mixture of a powder of carbon, a powder of silicon and a medium including an organic solvent, producing an oscillation in the mixture to impregnate the fabric with the mixture, and calcining the fabric impregnated with the mixture.
1. A method for producing a ceramic composite material, comprising:
preparing a first mixture consisting essentially of a carbon powder, a silicon powder and an organic solvent;
resting the first mixture to form a second mixture having a precipitation portion enriched in the carbon powder and the silicon powder relative to the first mixture, and a second portion enriched in the organic solvent relative to the first mixture;
immersing a fabric of fibers consisting essentially of an inorganic substance in the precipitation portion of the second mixture;
producing an oscillation in the second mixture containing the fabric of fibers immersed in the precipitation portion to impregnate the fabric of fibers with the carbon powder, the silicon powder, and the organic solvent; and
calcining the fabric of fibers impregnated with the carbon powder, the silicon powder, and the organic solvent to form a silicon carbide in and on the fabric of fibers.
2. The method of claim 1 , further comprising:
leaving the mixture at rest so as to form a precipitation, wherein the fabric is buried in the precipitation at the step of burying.
3. The method of claim 1 , wherein the medium includes an organic silicon polymer.
4. The method of claim 3 , further comprising:
preparing the medium so as to have a viscosity of from 0.8 mPaS to 4 mPaS.
5. The method of claim 1 , wherein an ultrasonic oscillation is applied at the step of producing.
6. The method of claim 1 , wherein the powder of carbon has a grain size of from 1 μm to 20 μm and the powder of silicon has a grain size of from 1 μm to 75 μm.
7. The method of claim 1 , wherein the powder of carbon has a specific surface of 14.2 m 2 /g or less.
8. The method of claim 1 , wherein the organic solvent consists essentially of xylene.
9. The method of claim 1 , further comprising:
forming a interface layer on the fibers by a CVD method.
10. The method of claim 1 , further comprising:
infiltrating a second ceramic phase of SiC into spaces among the fibers by a CVI method.
11. A method for producing a ceramic composite material, comprising:
preparing a mixture consisting essentially of a powder of carbon, a powder of silicon, an organic silicon polymer and a medium including an organic solvent and having a viscosity of from 0.8 mPaS to 4 mPaS;
burying a fabric of fibers consisting essentially of an inorganic substance in the mixture;
producing an oscillation in the mixture to impregnate the fabric with the mixture; and
calcining the fabric impregnated with the mixture to form a silicon carbide in and on the fabric of fibers.
12. A method for producing a ceramic composite material, comprising:
preparing a mixture consisting essentially of a powder of carbon, a powder of silicon and a medium including an organic solvent, wherein the powder of carbon has a specific surface of 14.2 m 2 /g or less;
burying a fabric of fibers consisting essentially of an inorganic substance in the mixture;
producing an oscillation in the mixture to impregnate the fabric with the mixture; and
calcining the fabric impregnated with the mixture to form a silicon carbide in and on the fabric of fibers.