IP Library Granted Patent US 8,846,970
Granted Patent B2
US 8,846,970 · App. 13/896,416 · Granted Sep 30, 2014

Metal carbamates formed from tolylenediamines

Inventors: Andreas Leitner (Pittsburgh, PA); Robert Baumann (Mannheim, DE); Wolfgang Siegel (Limburgerhof, DE)
Assignee: BASF SE
C07C269/04C07C271/28C07C269/06
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Quick Facts
Patent No.
US 8,846,970
App. No.
13/896,416
Granted
Sep 30, 2014
Kind
B2
Abstract

The invention provides metal carbamates of the general formula (I) where R1 and R2 are the same or different and are each an alkyl group having 1-18 carbon atoms and M is an alkali metal atom.

Claims (11)

1. A process for preparing tolylenediurethane, which comprises reacting a metal carbamate of the following general formula (I) with water

where R1 and R2 are the same or different and are each an alkyl group having 1 to 18 carbon atoms, the alkyl group optionally comprising one or more heteroatoms, and M is an alkali metal.

2. The process according to claim 1 , wherein the alkyl groups R1 and R2 each comprise 2-18 carbon atoms in the chain.

3. The process according to claim 1 , wherein the alkyl groups R1 and R2 each comprise 2-7 carbon atoms in the chain.

4. The process according to claim 1 , wherein the alkyl groups R1 and R2 are selected from the group consisting of an ethyl, propyl, butyl, 2-methylpropyl, 3-methylbutyl, n-pentyl, 2-methoxyethyl, 2-ethoxyethyl and a 2,2,2-trifluoroethyl group.

5. The process according to claim 1 , wherein the alkyl groups comprise one or more heteroatoms.

6. The process according to claim 1 , wherein the alkyl groups comprise one or more oxygen atoms.

7. The process according to claim 1 , wherein no heteroatoms are present in R1 and R2.

8. The process according to claim 1 , wherein R1 and R2 are identical.

9. The process according to claim 1 , wherein R1 and R2 are branched or unbranched.

10. The process according to claim 1 , wherein the metal carbamate is solid at room temperature.

Priority Claims (1)
EP 08152943 · Mar 18, 2008 · regional
Continuity (2)
Division 12920224
Related Publication 20130231495A1 · Sep 5, 2013