ATR objective for an IR microscope and method for operation thereof
An ATR objective ( 1 ) for an IR microscope has a Cassegrain objective ( 2 ), an ATR crystal ( 7 ), a holding bar ( 8 ) to one end of which on the side of the sample, the ATR crystal ( 7 ) is mounted, a holding element ( 10 ), thin struts ( 9 ) which rigidly connect the holding bar ( 8 ) to the holding element ( 10 ) and intersect an optical path of the ATR objective ( 1 ) entering or exiting the Cassegrain objective ( 2 ) in such a fashion that they shade less than 10% of the beam cross-section of the optical path, and a motor drive ( 12 ) for axial movement of the holding element ( 10 ) relative to the sample position ( 3 ). The automated ATR objective thereby enables simple adjustment of operating modes and different contact pressures of the ATR crystal with respect to a sample ( 19 ).
1. An ATR (attenuated total reflection) objective for examination of a sample in an IR (infrared) microscope, the objective comprising:
a frame structure;
a Cassegrain objective cooperating with said frame structure, said Cassegrain objective focussing IR radiation onto the sample at a sample position, said Cassegrain objective comprising a first mirror having a first central bore and a second mirror having a second central bore;
an ATR crystal;
a holding bar guided through said first and said second central bores, said holding bar having an end facing the sample to which said ATR crystal is mounted;
a holding element disposed proximate to or beyond a side of said Cassegrain objective facing away from the sample;
thin struts, which rigidly connect said holding bar to said holding element and intersect an optical path of said ATR objective entering or exiting said Cassegrain objective, wherein said thin struts shade less than 10% of a beam cross-section of said optical path; and
a motor drive for axial movement of said holding element relative to the sample position.
2. The ATR objective of claim 1 , further comprising a first travel sensor for detecting an axial position of said holding bar relative to said frame structure.
3. The ATR objective of claim 1 , further comprising a lifting element disposed on said frame structure for axial motion relative thereto, wherein said frame structure is rigidly connected to said Cassegrain objective and said holding element is coupled to said lifting element, wherein, in dependence on an operating state, said holding element is axially moved relative to said lifting element by means of said motor drive or is fixed relative to said lifting element and further comprising a spring configuration for providing a counterforce in response to axial movement of said lifting element away from the sample position.
4. The ATR objective in claim 3 , wherein said counterforce is an increasing force.
5. The ATR objective of claim 3 , wherein said spring configuration comprises several spring elements and a spring constant of an overall spring configuration varies with an axial position of said lifting element.
6. The ATR objective of claim 5 , wherein said spring constant of said overall spring configuration increases with increasing axial separation between said lifting element and the sample position.
7. The ATR objective of claim 3 , wherein a relief spring is disposed between said lifting element and said frame structure for complete or partial compensation of dead weight of axially movable parts.
8. The ATR objective of claim 3 , wherein said lifting element comprises one or more lifting element components for reducing axial movement of said lifting element relative to the sample position with respect to said spring configuration.
9. The ATR objective of claim 3 , further comprising a second travel sensor for detecting an axial position of said lifting element relative to said frame structure.
10. The ATR objective of claim 3 , wherein said frame structure comprises an axial stop for said holding element or said holding bar.
11. A method for operating the ATR objective of claim 10 , the method comprising the steps of:
a) moving the holding element to the sample position using the motor drive;
b) stopping axial movement of the holding element using the axial stop as soon as a measuring surface of the ATR crystal has exceeded the sample position by a predetermined axial distance (S1);
c) moving the lifting element, using the motor drive, against a force of the spring configuration away from the sample position via a previously selected axial distance (S2), thereby pressing the holding element or the holding bar against the stop;
d) axially moving the sample from a side facing away from the Cassegrain objective to the sample position to bring the sample into contact with the ATR crystal and further moving the sample until a measuring surface of the ATR crystal is in a focus of the Cassegrain objective.
12. The ATR objective of claim 1 , wherein said motor drive comprises a piezo translator system.