Analyzing device and method for controlling same
An analyzing device includes a feeder connected to a container in which a sample is contained for sucking the sample from the container and feeding the sample, and a controller for performing control for feeding from the feeder to a measurer. In measuring the sample, the controller performs control so that results of a plurality of times of measurement are obtained with respect to the single container in which the sample is contained, without changing the container. This arrangement allows quick accuracy check.
1. An analyzing device comprising:
a feeder connected to a container in which a sample is contained, the feeder being configured to suck the sample from the container, hold an amount of the sample necessary for two or more measurements, and configured to feeding the sample to an injection valve with multiple ports;
the feeder further comprise of a tubular portion directly connected to one of the multiple ports of the injection valve;
a controller for performing control for feeding the sample from the feeder to a measurer;
wherein, in measuring the sample, the controller performs control so that results of a plurality of measurements are obtained with respect to the single container in which the sample is contained, without changing the container;
the measurer includes a column containing a filler and an injection valve with multiple ports, capable of introducing a predetermined amount of sample into the column and also capable of feeding a mobile phase into the column, the measurer being configured so that the sample adsorbed to the filler is desorbed by the mobile phase and an effluent thereby produced is subjected to measurement for obtaining measurement results; and
in checking accuracy by using a sample of a known concentration as the sample, the controller performs control of the feeder and the measurer so that results of a plurality of measurements are obtained with respect to the single container in which the sample of the known concentration is contained, without changing the container.
2. The analyzing device according to claim 1 , wherein: the tubular portion is capable of retaining therein the sample of an amount necessary for two or more times of measurement; and
the controller first performs control of the feeder and the measurer so that part of the sample retained by the feeder is fed to the measurer, and then, after a single measurement, the controller performs control of the feeder and the measurer so that at least part of the remaining sample retained by the feeder is fed to the measurer.
3. A method of controlling an analyzing device comprising a feeder connected to a container in which a sample is contained for sucking the sample from the container and feeding the sample, a tubular portion capable of retaining therein the sample of an amount necessary for two or more times of measurement and a measurer to which the sample is fed from the feeder, the measurer includes a column containing a filler, and an injection valve capable of introducing a predetermined amount of sample into the column and also capable of feeding a mobile phase into the column, the measurer being configured so that the sample adsorbed to the filler is desorbed by the mobile phase and an effluent thereby produced is subjected to measurement for obtaining measurement results; and the feeder is configured to feed the sample to the injection valve with multiple ports,
the method comprising
a step of first controlling the feeder and the measurer so that part of the sample retained by the feeder is fed to the measurer, and then, after a single measurement, controlling the feeder and the measurer so that at least part of the remaining sample retained by the feeder is fed to the measurer,
a step of controlling the measurer when measuring the sample, so that a plurality of measurements are obtained with respect to the single container in which the sample is contained, without changing the container, and
a step controlling the feeder and the measurer in checking accuracy by using a sample of a known concentration as the sample, so that results of a plurality measurements are obtained with respect to the single container in which the sample of the known concentration is contained, without changing the container.
4. The method of controlling an analyzing device according to claim 3 ,
the method further comprises controlling the feeder and the measurer so that part of the sample retained by the feeder is fed to the column via the injection valve with multiple ports, and then, after a measurement, controlling the feeder and the measurer so that at least part of the remaining sample retained by the feeder is fed to the column via the injection valve with multiple ports.