IP Library Granted Patent US 9,066,980
Granted Patent B2
US 9,066,980 · App. 13/902,299 · Granted Jun 30, 2015

Liquid pharmaceutical formulations of palonosetron

Inventors: Giorgio Calderari (Rancate, CH); Daniele Bonadeo (Casalzuigno, IT); Roberta Cannella (Varese, IT); Alberto Macciocchi (Melide, CH); Andrew Miksztal (Palo Alto, CA); Thomas Malefyt (Carmel Valley, CA); Kathleen M Lee (Palo Alto, CA)
Assignees: Helsinn Healthcare SA; Roche Palo Alto LLC
A61K47/26A61K47/183A61K47/12A61K47/00A61K31/473A61K47/02A61K9/0019A61K9/0095
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Quick Facts
Patent No.
US 9,066,980
App. No.
13/902,299
Granted
Jun 30, 2015
Kind
B2
Abstract

The present invention relates to shelf-stable liquid formulations of palonosetron for reducing chemotherapy and radiotherapy induced emesis with palonosetron. The formulations are particularly useful in the preparation of intravenous and oral liquid medicaments.

Claims (22)

1. A pharmaceutical single-use, unit-dose formulation for intravenous administration to a human to reduce the likelihood of cancer chemotherapy-induced nausea and vomiting, comprising a 5 mL sterile aqueous solution, said solution comprising:

a) palonosetron hydrochloride in an amount of 0.25 mg based on the weight of its free base,

b) optionally a chelating agent, and

c) a tonicifying agent in an amount sufficient to make said solution isotonic, wherein said formulation is stable at 24 months when stored at room temperature.

2. The pharmaceutical formulation of claim 1 , wherein said solution is buffered at a pH of 5.0±0.5.

3. The pharmaceutical formulation of claim 1 , wherein said tonicifying agent is mannitol.

4. The pharmaceutical formulation of claim 3 , wherein said mannitol is in an amount from 10 mg/mL to 80 mg/mL.

5. The pharmaceutical formulation of claim 4 , wherein said mannitol is in an amount of 41.5 mg/mL.

6. The pharmaceutical formulation of claim 1 , wherein said formulation comprises a chelating agent.

7. The pharmaceutical formulation of claim 6 , wherein said chelating agent is EDTA.

8. The pharmaceutical formulation of claim 7 , wherein said EDTA is in an amount of from 0.005 mg/mL to 1.0 mg/mL.

9. The pharmaceutical formulation of claim 8 , wherein said EDTA is in an amount of 0.5 mg/mL.

10. The pharmaceutical formulation of claim 1 , wherein said solution further comprises a citrate buffer.

11. The pharmaceutical formulation of claim 10 , wherein said citrate buffer is at a concentration of 20 millimolar.

12. A method for reducing the likelihood of cancer chemotherapy-induced nausea and vomiting, comprising intravenously administering to a human in need thereof the pharmaceutical formulation of claim 1 , wherein said intravenous administration to said human occurs before the start of the cancer chemotherapy.

13. The method of claim 12 , wherein said intravenous administration to said human occurs over a period of time of 10 to 60 seconds.

14. The method of claim 12 , wherein said intravenous administration reduces the likelihood of acute nausea and vomiting in said human.

15. The method of claim 12 , wherein said intravenous administration reduces the likelihood of delayed nausea and vomiting in said human.

16. A pharmaceutical single-use, unit-dose formulation for intravenous administration to a human to reduce the likelihood of cancer chemotherapy-induced nausea and vomiting, comprising a 5 mL sterile aqueous solution, said solution comprising:

a) palonosetron hydrochloride in an amount of 0.25 mg based on the weight of its free base,

b) optionally a chelating agent, and

c) a tonicifying agent in an amount sufficient to make said solution isotonic, wherein said formulation is stable at 18 months when stored at room temperature.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded Sep 20, 2023
From: HAMILTON SA LLC
To: HELSINN HEALTHCARE SA; HELSINN THERAPEUTICS (U.S.), INC.; HELSINN BIREX PHARMACEUTICALS LIMITED
Reel/Frame 064961/0567 →
SECURITY INTEREST Recorded Dec 30, 2022
From: HELSINN HEALTHCARE SA; HELSINN THERAPEUTICS (U.S.), INC.; HELSINN BIREX PHARMACEUTICALS LIMITED
To: HAMILTON SA LLC
Reel/Frame 062254/0888 →
CORRECTIVE ASSIGNMENT TO CORRECT THE 1. SPELLING OF ASSIGNEE NAME HELSINN BIREX PHARMACEUTICALS LTD.; 2. ADDRESSES OF ASSIGNEES PREVIOUSLY RECORDED ON REEL 047534 FRAME 0024. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT CO-OWNERSHIP AGREEMENT. Recorded Nov 21, 2018
From: HELSINN HEALTHCARE SA
To: HELSINN ADVANCED SYNTHESIS SA; HELSINN BIREX PHARMACEUTICALS, LTD.; HELSINN THERAPEUTICS (U.S.), INC.
Reel/Frame 047617/0285 →
PATENT CO-OWNERSHIP AGREEMENT Recorded Nov 14, 2018
From: HELSINN HEALTHCARE SA
To: HELSINN ADVANCED SYNTHESIS SA; HELSINN BIREX PHARMACEUTIALS LTD.; HELSINN THERAPEUTICS (U.S.), INC.
Reel/Frame 047534/0024 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 14, 2018
From: CALDERARI, GIORGIO; BONADEO, DANIELE; CANNELLA, ROBERTA; MACCIOCCHI, ALBERTO; PANUCCIO, CARMINE
To: HELSINN HEALTHCARE SA
Reel/Frame 047498/0916 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 14, 2018
From: MIKSZTAL, ANDREW; MALEFYT, THOMAS; LEE, KATHLEEN M
To: ROCHE PALO ALTO LLC
Reel/Frame 047498/0945 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 11, 2016
From: ROCHE PALO ALTO LLC
To: HELSINN HEALTHCARE SA
Reel/Frame 038544/0269 →
Continuity (6)
Continuation 13901437 · May 23, 2013
Continuation In Part 13087012 · Apr 14, 2011
Continuation 11186311 · Jul 21, 2005
Continuation PCTEP2004000888 · Jan 30, 2004
Provisional Application 60444351 · Jan 30, 2003
Related Publication 20130289065A1 · Oct 31, 2013