IP Library Granted Patent US 9,080,089
Granted Patent B2
US 9,080,089 · App. 13/627,749 · Granted Jul 14, 2015

Nanoparticles for heat transfer and thermal energy storage

Inventors: Dileep Singh (Naperville, IL); Sreeram Cingarapu (Darian, IL); Elena V. Timofeeva (Chicago, IL); Michael Moravek (Lemont, IL)
Assignee: UChicago Argonne, LLC
C09K5/063C09K5/10C09K5/12B82Y30/00B82Y40/00
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Quick Facts
Patent No.
US 9,080,089
App. No.
13/627,749
Granted
Jul 14, 2015
Kind
B2
Abstract

An article of manufacture and method of preparation thereof. The article of manufacture and method of making the article includes an eutectic salt solution suspensions and a plurality of nanocrystalline phase change material particles having a coating disposed thereon and the particles capable of undergoing the phase change which provides increase in thermal energy storage. In addition, other articles of manufacture can include a nanofluid additive comprised of nanometer-sized particles consisting of copper decorated graphene particles that provide advanced thermal conductivity to heat transfer fluids.

Claims (18)

1. An article of manufacture, comprising:

an alkali halide eutectic salt solution; and

a plurality of nanocrystalline metal particles dispersed in the alkali halide eutectic salt solution, the plurality of nanocrystalline metal particles having a coating disposed thereon and the particles capable of undergoing a phase change.

2. The article of manufacture as described in claim 1 wherein the alkali halide eutectic salt solution comprises an alkali chloride eutectic salt solution.

3. The article of manufacture as defined in claim 1 wherein the nanocrystalline metal particles consist of zinc particles.

4. The article of manufacture as defined in claim 1 wherein the coating comprises an oxide.

5. The article of manufacture as defined in claim 4 wherein the oxide comprises trioctyl phosphine oxide.

6. The article of manufacture as defined in claim 1 wherein the nanocrystalline metal particles have a size of about 600 nm to 5 micrometers.

7. The article of manufacture as defined in claim 1 further comprising the plurality of nanocrystalline metal particles comprising zinc up to 10 volume % of the total volume of nanocrystalline metal particles and alkali halide eutectic salt solution.

8. A method of preparing a material having selected heat transfer and thermal properties, comprising:

providing an alkali halide eutectic salt; and

dispersing in the alkali halide eutectic salt a plurality of nanocrystalline metal particles having a coating disposed thereon the metal particles.

9. The method as described in claim 8 wherein the alkali halide eutectic salt comprises an alkali chloride eutectic salt.

10. The method as defined in claim 8 wherein the nanocrystalline metal particles consist of zinc particles.

11. The method as defined in claim 8 wherein the coating comprises an oxide.

12. The method as defined in claim 11 wherein the oxide comprises trioctyl phosphine oxide.

13. The method as defined in claim 8 wherein the nanocrystalline metal particles have a size of about 600 nm to 5 micrometers.

14. The method as defined in claim 8 wherein the alkali halide eutectic salt is provided as a 85-90% eutectic salt solution.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 25, 2015
From: SINGH, DILEEP; TIMOFEEVA, ELENA V.; MORAVEK, MICHAEL R.; CINGARAPU, SREERAM
To: UCHICAGO ARGONNE, LLC
Reel/Frame 035256/0813 →
CONFIRMATORY LICENSE Recorded Oct 26, 2012
From: UCHICAGO ARGONNE, LLC
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 029236/0444 →
Continuity (1)
Related Publication 20140084205A1 · Mar 27, 2014