IP Library Granted Patent US 9,115,397
Granted Patent B2
US 9,115,397 · App. 14/488,751 · Granted Aug 25, 2015

Fluorescent chemical compounds having high selectivity for double stranded DNA, and methods for their use

Inventors: Jolene Bradford (Eugene, OR); Ching-Ying Cheung (San Ramon, CA); Shih-Jung Huang (Eugene, OR); Patrick Pinson (Eugene, OR); Stephen Yue (Eugene, OR)
Assignee: LIFE TECHNOLOGIES CORPORATION
C12Q1/6876C07D215/10C07D215/227C07D277/72C07D277/74C07D417/04C07D417/06C07D417/14G01N21/6486
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Quick Facts
Patent No.
US 9,115,397
App. No.
14/488,751
Granted
Aug 25, 2015
Kind
B2
Abstract

Chemical compounds having a high selectivity for double stranded DNA over RNA and single stranded DNA are disclosed. The chemical compounds are stains that become fluorescent upon illumination and interaction with double stranded DNA, but exhibit reduced or no fluorescence in the absence of double stranded DNA. The compounds can be used in a variety of biological applications to qualitatively or quantitatively assay DNA, even in the presence of RNA.

Claims (17)

1. A method of detecting the presence or absence of double stranded DNA in a sample, the method comprising:

providing a sample suspected of containing double stranded DNA;

contacting the sample with a chemical compound to prepare a test sample;

illuminating the test sample with energy; and

detecting emission of energy from the test sample;

wherein the chemical compound has the structure:

wherein:

n is 0;

X is oxygen;

R′, R 2 , R 3 , R 4 , R 5 , R 6 , R 7 , R 8 , R 10 and R 11 independently comprise hydrogen, a hydroxyl group, an alkoxy group, a thiol, a thioalkyl, a thioaryl, a halogen, an alkyl group, an alkenyl group, an alkynyl group, an aromatic group, a primary amine group, a secondary amine group, a tertiary amine group, a reactive group, or combinations thereof, wherein at least one of R 1 , R 2 , R 3 and R 4 comprises an aromatic group or an alkynyl group;

R 9 comprises an aromatic group or alkyl-aromatic group; and

R 12 is an alkyl group.

2. The method of claim 1 , further comprising calculating the concentration of double stranded DNA in the sample after the detecting step.

3. The method of claim 1 , wherein R 10 is an amine group.

4. The method of claim 1 , wherein R 12 is a C 1 -C 8 alkyl group.

5. The method of claim 1 , wherein R 12 is a methyl group.

6. The method of claim 1 , wherein the chemical compound further comprises one or more cations or anions.

Continuity (7)
Division 13861123 · Apr 11, 2013
Continuation 13559300 · Jul 26, 2012
Continuation 13104413 · May 10, 2011
Continuation 12573809 · Oct 5, 2009
Continuation 11432814 · May 11, 2006
Provisional Application 60680243 · May 11, 2005
Related Publication 20150004597A1 · Jan 1, 2015