IP Library Granted Patent US 9,136,146
Granted Patent B2
US 9,136,146 · App. 14/073,460 · Granted Sep 15, 2015

Femtosecond laser-induced formation of submicrometer spikes on a semiconductor substrate

Inventors: Eric Mazur (Concord, MA); Mengyan Shen (Belmont, MA)
Assignee: President And Fellows Of Harvard College
H01L21/67075B23K26/121H01L21/0259H01L21/02686H01L21/02532Y10S438/94
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Quick Facts
Patent No.
US 9,136,146
App. No.
14/073,460
Granted
Sep 15, 2015
Kind
B2
Abstract

The present invention generally provides semiconductor substrates having submicronsized surface features generated by irradiating the surface with ultra short laser pulses. In one aspect, a method of processing a semiconductor substrate is disclosed that includes placing at least a portion of a surface of the substrate in contact with a fluid, and exposing that surface portion to one or more femtosecond pulses so as to modify the topography of that portion. The modification can include, e.g., generating a plurality of submicron-sized spikes in an upper layer of the surface.

Claims (19)

1. A system for fabricating a radiation-absorbing semiconductor substrate, comprising:

a laser radiation system for generating laser pulses,

a vacuum chamber including a window for entry of said laser pulses into the chamber,

a translation stage disposed in said vacuum chamber and configured for supporting a sample, said stage allowing moving the sample relative to the laser pulses for exposing different portions of a surface of the sample to said laser pulses,

a liquid cell coupled to the stage so as to provide contact between a liquid contained therein and said surface of the sample,

wherein the vacuum chamber is configured to allow pumping out air bubbles in said liquid.

2. The system of claim 1 , further comprising a lens for focusing said laser radiation pulses through said window of the vacuum chamber onto said substrate surface.

3. The system of claim 1 , wherein said laser pulses have a pulsewidth in a range of 50 fs to a few ns.

4. The system of claim 1 , wherein said laser pulses have a pulsewidth in a range of 50 fs to about 500 fs.

5. The system of claim 1 , wherein said laser radiation system comprises a regenerative amplifier for amplifying said laser pulses.

6. The system of claim 5 , wherein said laser radiation system further comprises a harmonic generation system for receiving said amplified pulses and generating second-harmonic pulses.

7. The system of claim 6 , wherein said laser radiation system further comprises a dichroic mirror for directing said second-harmonic pulses via said window of the vacuum chamber onto said sample surface.

8. The system of claim 2 , wherein said focused radiation pulses exhibit a fluence in a range of about 1 kJ/cm 2 to about 8 kJ/cm 2 at said sample surface.

9. The system of claim 1 , wherein said laser radiation system comprises an amplified, Ti:Sapphire laser system.

10. The system of claim 1 , wherein said translation stage is a 3-D translation stage.

11. The system of claim 1 , further comprising an optical imaging system for monitoring said sample surface during irradiation by the laser pulses.

12. The system of claim 1 , wherein said liquid is transparent to radiation having wavelength components in a range of about 400 nm to about 800 nm.

13. The system of claim 1 , wherein said liquid presents a thickness in a range of 1 nm to about 20 nm to said laser pulses.

14. The system of claim 1 , wherein said liquid comprises any of water, alcohol or silicon oil.

Assignments (2)
CONFIRMATORY LICENSE Recorded Sep 30, 2015
From: HARVARD UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 036722/0394 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 11, 2014
From: MAZUR, ERIC; SHEN, MENGYAN
To: PRESIDENT AND FELLOWS OF HARVARD COLLEGE
Reel/Frame 032400/0900 →
Continuity (6)
Continuation 13021409 · Feb 4, 2011
Continuation In Part 12235086 · Sep 22, 2008
Division 11196929 · Aug 4, 2005
Continuation In Part 10950230 · Sep 24, 2004
Continuation 10950248 · Sep 24, 2004
Related Publication 20140060737A1 · Mar 6, 2014