Method of evaluating silica powder, vitreous silica crucible, and method of manufacturing vitreous silica crucible
The present invention provides a method of evaluating silica powder which, enables precise prediction of easiness of crystallization of a vitreous silica crucible. According to the present invention, provided is a method of evaluating silica powder including a sample preparation process for preparing a vitrified sample by fusing silica powder at a fusing temperature of 1700 to 1900 deg. C., followed by cooling; a sample heat treatment process for retaining the sample for 30 minutes or more at a temperature of 1400 to 1750 deg. C., followed by cooling; and a sample evaluation process for evaluating a state of opacification of the sample after the sample heat treatment process.
1. A method of evaluating silica powder comprising:
a sample preparation process for preparing a transparent vitrified sample by fusing silica powder at a fusing temperature of 1780 to 1790 deg. C, followed by cooling;
a sample heat treatment process for retaining the sample for 30 minutes or more at a temperature of 1400 to 1750 deg. C, followed by cooling; and
a sample evaluation process for evaluating the silica powder according to a state of opacification of the sample after the sample heat treatment process, wherein the state of opacification is accessed by measuring the number density of opaque spots contained in the sample.
2. The method of claim 1 , wherein, in the sample preparation process, plural samples are prepared at different fusing temperatures, and in the sample evaluation process, the state of opacification of the sample is evaluated by a density of opaque spots contained in the sample.
3. The method of claim 1 , wherein the silica powder is natural silica powder.
4. The method of claim 1 , wherein the silica powder is silica powder doped with a mineralizer.
5. A vitreous silica crucible having a vitreous silica layer obtained by fusing silica powder, followed by cooling, wherein the silica powder is silica powder, the state of opacification of which has been evaluated according to the method of claim 1 .
6. A method of manufacturing a vitreous silica crucible comprising the processes of:
a silica powder evaluation process for evaluating silica powder by the method of claim 1 ,
a vitreous silica layer formation process for forming a vitreous silica layer by fusing the silica powder after the evaluation, followed by cooling.