IP Library › Granted Patent US 9,227,181
Granted Patent B2
US 9,227,181 · App. 13/231,522 · Granted Jan 5, 2016

Catalyst to increase propylene yields from a fluid catalytic cracking unit

Inventor: David H. Harris (Mountainside, NJ)
Assignee: BASF Corporation
B01J29/80B01J29/40B01J37/28C07C4/06C10G11/18B01J29/084B01J29/088B01J29/7007B01J35/1066B01J2229/42C07C2529/08C07C2529/40C07C2529/70C07C2529/80
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Quick Facts
Patent No.
US 9,227,181
App. No.
13/231,522
Granted
Jan 5, 2016
Kind
B2
Abstract

A catalyst composition resulting in increased propylene yields during fluid catalytic cracking processes comprises (i) Y zeolite, (ii) ZSM-5 zeolite, and (iii) Beta zeolite.

Claims (26)

1. A hydrocarbon conversion catalyst blend comprising:

(a) a Y zeolite in an amount of 5 to 50 wt. % of said catalyst blend;

(b) a ZSM-5 zeolite in an amount of 5 to 40 wt. % of said catalyst blend; and

(c) a Beta zeolite in an amount of 35 to 70 wt. % of said catalyst blend, wherein each of said ZSM-5 zeolite, said Beta zeolite, and said Y zeolite is a separate microsphere.

2. The catalyst blend of claim 1 , wherein the Y zeolite is a large-pore zeolite comprising Y zeolite crystallized as a layer on the surface of a porous alumina-containing matrix, said zeolite-layered matrix arranged in a configuration to provide macropores in which the zeolite layer is provided on the walls of the macropores.

3. The catalyst blend of claim 1 , wherein the Y zeolite contains up to 12% of a rare earth element ion exchanged onto the Y zeolite.

4. The catalyst blend of claim 1 wherein the ZSM-5 additive contains zeolite comprises phosphorus stabilized ZSM-5 zeolite, alumina, and kaolin bound together with phosphorus-containing compound.

5. The catalyst blend of claim 1 wherein the Beta zeolite is a H-Beta with a silica/alumina ratio greater than 10.

6. The catalyst blend of claim 5 wherein the silica/alumina ratio of the Beta zeolite is greater than 100.

7. The catalyst blend of claim 1 wherein the Beta zeolite is modified with a phosphorus-containing compound.

8. The catalyst blend of claim 7 wherein the Beta zeolite has a phosphorus level between 1-7% P 2 O 5 .

9. The catalyst blend of claim 8 wherein the phosphorus level is between 3-5% P 2 O 5 .

10. The catalyst blend of claim 1 wherein the catalyst comprises 25-30 wt. % of said Y zeolite, 15-20 wt. % of said ZSM-5 zeolite, and 50-60 wt. % of said Beta zeolite.

11. A hydrocarbon conversion catalyst blend comprising:

(a) a Y zeolite, wherein the Y zeolite is a large-pore zeolite comprising Y zeolite crystallized as a layer on the surface of a porous alumina-containing matrix, said zeolite-layered matrix arranged in a configuration to provide macropores in which the zeolite layer is provided on the walls of the macropores;

(b) a ZSM-5 zeolite; and

(c) a Beta zeolite,

wherein said blend contains by wt. % more said Beta zeolite than said Y zeolite, and more said Y zeolite than said ZSM-5 zeolite, and each of said ZSM-5 zeolite, said Beta zeolite, and said Y zeolite is a separate microsphere.

12. The catalyst of claim 11 wherein the catalyst blend comprises 5-50 wt. % of said Y zeolite, 5-40 wt. % ZSM-5 zeolite, and 35-70 wt. % of said Beta zeolite.

13. The catalyst of claim 11 wherein the catalyst blend comprises 25-30 wt. % of said Y zeolite, 15-20 wt. % of said ZSM-5 zeolite, and 50-60 wt. % of said Beta zeolite.

14. The catalyst of claim 11 wherein the ZSM-5 zeolite is a phosphorus stabilized ZSM-5 zeolite, alumina, and kaolin bound together with a phosphorus-containing compound.

15. The catalyst of claim 14 , wherein the Y zeolite contains 1% or less of a rare earth element ion exchanged onto the Y zeolite.

16. The catalyst of claim 14 wherein the Beta zeolite is a H-Beta with a silica/alumina ratio greater than 100.

17. The catalyst of claim 14 wherein the Beta zeolite is modified with a phosphorous-containing compound.

18. A process for the improved production of propylene comprising cracking a hydrocarbon feedstock under fluid catalytic cracking conditions with the catalyst of claim 1 .

19. A process for the improved production of propylene comprising cracking a hydrocarbon feedstock under fluid catalytic cracking conditions with the catalyst of claim 15 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 28, 2011
From: HARRIS, DAVID H
To: BASF CORPORATION
Reel/Frame 027137/0992 →
Continuity (1)
Related Publication 20130066131A1 · Mar 14, 2013