IP Library Granted Patent US 9,304,074
Granted Patent B2
US 9,304,074 · App. 13/553,555 · Granted Apr 5, 2016

Methods for making and compositions of two dimensional particle arrays

Inventors: Sanford A. Asher (Pittsburgh, PA); Alexander Tilchonov (Pittsburgh, PA); Luling Wang (Mesa, AZ); Jian-Tao Zhang (Pittsburgh, PA)
Assignee: University of Pittsburgh—Of The Commonwealth System of Higher Education
G01N21/01G01N21/4788
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Quick Facts
Patent No.
US 9,304,074
App. No.
13/553,555
Granted
Apr 5, 2016
Kind
B2
Abstract

A method of preparation of a 2-D array of particles comprising: mixing the particles and a first liquid, the first liquid having the properties of being soluble in water and reducing surface tension of a water surface; adding the mixture to the water surface; and transferring the 2-D array onto a solid surface. A composition comprising: a 2-D array of particles; and a polymer substantially enveloping the 2-D array of particles.

Claims (10)

1. A method of sensing a condition, molecule or chemical comprising:

providing a sensor comprising a self-assembled 2-D photonic crystal (PC) array or colloidal crystal array (CCA) of polymeric particles embedded in a matrix comprising a polymer and a recognition agent; wherein the self-assembled 2-D photonic crystal (PC) array or colloidal crystal array (CCA) of polymeric particles was formed by solvent evaporation on a liquid surface; and wherein the recognition agent causes the matrix to swell or shrink in the presence of the condition, molecule or chemical;

exhibiting by the sensor a first light diffraction of a first wavelength in the absence of the condition, molecule or chemical;

exposing the sensor to the condition, molecule or chemical causing the matrix to swell or shrink, thereby altering a spacing of the 2-D PC array or CCA of particles in the matrix such that a second light diffraction from the sensor shows a visually evident color change compared to the first light diffraction.

2. The method of claim 1 wherein the condition, molecule or chemical is pH.

3. The method of claim 1 wherein the recognition agent is selected from the group consisting of carboxylic acid, acrylic acid, urea, uric acid, antigens, antibodies, cations, sodium, potassium, calcium, magnesium, mercury, ammonia, anions, chloride, carbonate, bicarbonate, phosphate and chelating agents, crown ethers, azacrown ethers, borane complexes, calixarene, and cation selective binding proteins.

4. The method of claim 1 wherein the condition, molecule or chemical is lead.

5. The method of claim 1 wherein the polymeric particles comprise polystyrene.

6. The method of claim 1 wherein the liquid comprises water.

7. The method of claim 1 wherein the liquid comprises mercury.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 8, 2013
From: ASHER, SANFORD A.; TIKHONOV, ALEXANDER; WANG, LULING; ZHANG, JIAN-TAO
To: UNIVERSITY OF PITTSBURGH -- OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION
Reel/Frame 029780/0329 →
Continuity (2)
Provisional Application 61509284 · Jul 19, 2011
Related Publication 20140204364A1 · Jul 24, 2014