IP Library › Granted Patent US 9,376,536
Granted Patent B2
US 9,376,536 · App. 13/584,616 · Granted Jun 28, 2016

Carbon fibre compositions comprising lignin derivatives

Inventor: Alex Berlin (Davis, CA)
Assignee: FIBRIA INNOVATIONS INC.
C08H6/00C07G1/00C08H8/00C08L97/005D01F9/17
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Quick Facts
Patent No.
US 9,376,536
App. No.
13/584,616
Granted
Jun 28, 2016
Kind
B2
Abstract

The present disclosure provides derivatives of native lignin suitable for production of carbon fibers wherein the derivatives of native lignin have a certain alkoxy content and/or a certain carbon content. The present lignin derivatives can have acceptable spinnability performance characteristics for producing carbon fibers having acceptable tensile strengths and acceptable modulus of elasticity.

Claims (24)

1. A lignin derivative comprising a carbon content of 68.5 wt. % or greater and an alkoxy content of 0.45 mmol/g or greater.

2. The lignin derivative according to claim 1 , wherein the derivative has a carbon content of 69.5 wt. % or greater.

3. The lignin derivative according to claim 1 , wherein the derivative has an alkoxy content of about 0.6 mmol/g or greater.

4. The lignin derivative according to claim 1 , wherein the lignin is derived from hardwood biomass.

5. The lignin derivative according to claim 1 , wherein the lignin is derived from softwood biomass.

6. The lignin derivative according to Claim 1 , wherein the lignin is derived from annual fibre biomass.

7. The lignin derivative according to claim 1 , wherein the lignin is derived from biomass comprising Populus spp, Eucalyptus spp., Acacia spp., or combinations/hybrids thereof.

8. The lignin derivative according to claim 7 , wherein the biomass comprises Populus tremuloides, Eucalyptus globulus, Acacia dealbata, or combinations/hybrids thereof.

9. The lignin derivative according to claim 1 , wherein the lignin is derived from biomass comprising pine; spruce; or combinations/hybrids thereof.

10. The lignin derivative according to claim 1 , wherein the lignin is derived from biomass comprising Pinus radiata, Pinus taeda, BC spruce, and combinations/hybrids thereof.

11. The lignin derivative according to claim 1 , wherein the lignin is derived from biomass comprising wheat straw, bagasse, corn cobs, or combinations/hybrids thereof.

12. The lignin derivative of claim 1 , wherein the carbon content is measured following combustion at 975° C. in a pure oxygen environment.

13. A carbon fibre composition comprising the lignin derivative according to claim 1 .

14. A method of producing a carbon fibre composition from the lignin derivative according to claim 1 , comprising the steps of:

a. collecting biomass;

b. extracting the lignin derivatives according to claim 1 and spinning the lignin derivatives into fibres;

c. melting the fibres;

d. stabilizing the fibres; and

e. carbonizing the fibres.

15. A lignin derivative comprising a carbon content of 66.5 wt. % or greater and an ethoxy content of 0.45 mmol/g or greater.

16. The lignin derivative according to claim 15 , wherein the derivative has the ethoxy content of about 0.6 mmol/g or greater.

17. A hardwood lignin derivative comprising a carbon content from about 67.5 wt. % to about 75.5 wt. % and an ethoxy content of from 0.45 mmol/g to about 1.4 mmol/g.

18. A softwood lignin derivative comprising a carbon content from about 66.5 wt. % to about 80.0 wt. % and an ethoxy content of from about 0.35 mmol/g to about 1.4 mmol/g.

19. The softwood lignin derivative of claim 18 , wherein the carbon content is measured following combustion at 975° C. in a pure oxygen environment.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2019
From: FIBRIA INNOVATIONS INC.
To: SUZANO CANADA INC.
Reel/Frame 051135/0966 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 1, 2016
From: LIGNOL INNOVATIONS LTD.
To: FIBRIA INNOVATIONS INC.
Reel/Frame 038760/0120 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 28, 2013
From: BERLIN, ALEX
To: LIGNOL INNOVATIONS LTD.
Reel/Frame 029706/0740 →
Continuity (3)
Continuation PCTCA2011000184 · Feb 15, 2011
Provisional Application 61304752 · Feb 15, 2010
Related Publication 20130211056A1 · Aug 15, 2013