IP Library Granted Patent US 9,447,503
Granted Patent B2
US 9,447,503 · App. 11/755,281 · Granted Sep 20, 2016

Closed pore ceramic composite article

Inventors: Susan M. Tholen (Kennebunk, ME); Christopher W. Strock (Kennebunk, ME)
Assignee: United Technologies Corporation
C23C28/04C04B38/0061C04B2111/00525C04B2111/00982F01D11/08F01D11/12F01D25/005F05D2300/6033F05D2300/611Y10T428/24997
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Quick Facts
Patent No.
US 9,447,503
App. No.
11/755,281
Granted
Sep 20, 2016
Kind
B2
Abstract

A composite article includes a substrate and a thermal barrier secured to the substrate. The thermal barrier includes a plurality of closed pores within a ceramic matrix. For example, the closed pores comprise 20 vol % to 80 vol % of the thermal barrier.

Claims (22)

1. A composite article comprising:

a substrate; and

a thermal barrier secured to the substrate, the thermal barrier comprising a plurality of closed pores within a ceramic matrix, wherein the ceramic matrix comprises at least one of yttria stabilized zirconia and molybdenum disilicide.

2. The composite article as recited in claim 1 , wherein the plurality of closed pores are each entirely surrounded by the ceramic matrix.

3. The composite article as recited in claim 1 , wherein the plurality of closed pores comprise about 20 vol % to 80 vol % of the thermal barrier.

4. The composite article as recited in claim 3 , wherein the plurality of closed pores comprise about 33 vol % to 66 vol % of the thermal barrier.

5. The composite article as recited in claim 3 , wherein the plurality of closed pores comprise about 66 vol % of the thermal barrier.

6. The composite article as recited in claim 1 , further comprising a bond coat between the substrate and the thermal barrier.

7. The composite article as recited in claim 1 , wherein the thermal barrier comprises a thickness of about 20 mils to 150 mils.

8. The composite article as recited in claim 7 , wherein the thickness is about 20 mils to 50 mils.

9. The composite article as recited in claim 1 , wherein the plurality of closed pores is an inherent porosity in the ceramic matrix material.

10. The composite article as recited in claim 1 , wherein each of the plurality of closed pores is bounded by a side wall, and the ceramic matrix material is the side wall.

11. The composite article as recited in claim 1 , wherein the ceramic matrix comprises the yttria stabilized zirconia.

12. The composite article as recited in claim 1 , wherein the ceramic matrix comprises the molybdenum disilicide.

13. A method of manufacturing a thermal barrier, comprising:

forming the thermal barrier with a plurality of closed pores within a ceramic matrix, including forming the thermal barrier from a ceramic material having a pore-forming agent including nano-sized ceramic particles and sintering the pore-forming agent to reduce the size of the pore-forming agent and thereby form the closed pores.

14. The method as recited in claim 13 , wherein the ceramic matrix comprises at least one of yttria stabilized zirconia and molybdenum disilicide.

15. The method as recited in claim 14 , wherein the ceramic matrix comprises the molybdenum disilicide.

16. A turbine blade outer air seal comprising:

a body extending between two circumferential sides, a leading edge and a trailing edge, and a radially inner side and a radially outer side; and

a thermal barrier secured to the body, the thermal barrier comprising a plurality of closed pores within a ceramic matrix, wherein the ceramic matrix comprises at least one of yttria stabilized zirconia and molybdenum disilicide.

17. The turbine blade outer air seal as recited in claim 16 , wherein the plurality of closed pores comprise about 33 vol % to 66 vol % of the thermal barrier, and wherein the thermal barrier comprises a thickness between about 20 mils and 50 mils.

Assignments (4)
CHANGE OF NAME Recorded Jul 27, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064714/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE AND REMOVE PATENT APPLICATION NUMBER 11886281 AND ADD PATENT APPLICATION NUMBER 14846874. TO CORRECT THE RECEIVING PARTY ADDRESS PREVIOUSLY RECORDED AT REEL: 054062 FRAME: 0001. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF ADDRESS. Recorded Mar 4, 2021
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 055659/0001 →
CHANGE OF NAME Recorded Sep 4, 2020
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 054062/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 30, 2007
From: THOLEN, SUSAN M.; STROCK, CHRISTOPHER W.
To: UNITED TECHNOLOGIES CORPORATION
Reel/Frame 019355/0913 →
Continuity (1)
Related Publication 20090130424A1 · May 21, 2009