IP Library Granted Patent US 9,457,318
Granted Patent B2
US 9,457,318 · App. 13/993,582 · Granted Oct 4, 2016

Anion exchange membranes, methods of preparation and uses

Inventors: Charles Linder (Rehovot, IL); Ora Kedem (Haifa, IL); Rami Messalem (Omer, IL)
Assignee: Ben-Gurion University of the Negev Research and Development Authority
B01D61/44B01J41/125C08J5/2256C08J2381/06
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Quick Facts
Patent No.
US 9,457,318
App. No.
13/993,582
Granted
Oct 4, 2016
Kind
B2
Abstract

The present invention provides anion exchange membranes, processes for producing same and uses thereof. The anion exchange membranes according to embodiments of the present invention achieve a desirable combination of low resistance, high permselectivity and low degree of dimensional swelling. Anion exchange membranes according to embodiments of the present invention are also cost effective.

Claims (18)

1. A coating for a spacer in an electrodialysis unit, the coating comprising:

i) a first aromatic polymer comprising cationic groups bound to an aromatic backbone of the first aromatic polymer through alkylene groups; and

ii) a second aromatic polymer comprising aromatic amino groups, wherein an amine is directly attached to the aromatic ring;

wherein the first aromatic polymer and the second aromatic polymer are crosslinked through an alkylene bridge between an aromatic ring of the aromatic backbone of the first aromatic polymer and the amine of the second aromatic polymer.

2. The coating of claim 1 , wherein the first aromatic polymer comprising cationic groups is based on a polymer selected from the group consisting of alkylated polyphenylene oxide, alkylated polyphenylsulfone, polysulfone based on bisphenol A, alkylated polyethersulfone, alkylated polyaromatic ether ketone and aromatic alkylated polystyrene.

3. The coating of claim 1 , wherein the alkylene group of the first aromatic polymer comprising cationic groups, the alkylene bridge, or both, are a short-chain alkylene containing 1 to 6 methylene groups.

4. The coating of claim 1 , wherein the cationic groups are selected from the group consisting of quaternary ammonium, phosphonium and sulfonium group.

5. The coating of claim 1 , wherein the ion exchange capacity of the cationic groups ranges from 0.2 to 5 meq/gr.

6. The coating of claim 1 , wherein the second aromatic polymer comprising aromatic amino groups is based on an aromatic condensation polymer.

7. The coating of claim 6 , wherein the aromatic condensation polymer is selected from the group consisting of polyphenylsulfone, polysulfone, polyethersulfone, polyetherketone, polyetheretherketone and polyphenylsulfide.

8. The coating of claim 1 , wherein the amine content on the second aromatic polymer comprising aromatic amino groups ranges from 0.2 to 4 meq/gr.

9. The coating of claim 1 , further comprising an aromatic polymer selected from an aromatic non-derivatized polymer and an aromatic polymer derivatized with hydrophobic moieties.

10. The coating of claim 9 , wherein the additional aromatic polymer constitutes up to 50% of the total polymer content of the coating.

11. The coating of claim 1 , wherein the first aromatic polymer comprising cationic groups, the second aromatic polymer comprising aromatic amino groups, or both, further comprises a functional group selected from the group consisting of nitro and halide groups on at least part of the aromatic rings of said first and/or second aromatic polymers.

12. The coating of claim 1 , wherein the coating maintains its lateral dimensions in both dry and wet conditions to within 10%.

13. The coating of claim 1 , comprising at least one layer.

14. The coating of claim 1 , further comprising a surface coating made of non-charged crosslinked hydrophilic polymers or of an amphoteric film.

15. The coating of claim 14 , wherein the surface coating is separated from the underlying spacer coating by a thin hydrophilic neutral layer.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 9, 2013
From: LINDER, CHARLES; KEDEM, ORA; MESSALEM, RAMI
To: BEN-GURION UNIVERSITY OF THE NEGEV RESEARCH AND DEVELOPMENT AUTHORITY
Reel/Frame 030979/0055 →
Continuity (2)
Provisional Application 61422173 · Dec 12, 2010
Related Publication 20130292252A1 · Nov 7, 2013