IP Library Granted Patent US 9,466,853
Granted Patent B2
US 9,466,853 · App. 13/247,417 · Granted Oct 11, 2016

High energy density aluminum battery

Inventors: Gilbert M. Brown (Knoxville, TN); Mariappan Parans Paranthaman (Knoxville, TN); Sheng Dai (Knoxville, TN); Nancy J. Dudney (Knoxville, TN); Arumugan Manthiram (Austin, TX); Timothy J. McIntyre (Knoxville, TN); Xiao-Guang Sun (Knoxville, TN); Hansan Liu (Burnaby, CA)
Assignees: UT-Battelle, LLC; Board of Regents, The University of Texas System
H01M10/056H01M4/463H01M10/054H01M10/0525H01M4/50H01M6/16H01M10/058Y02E60/122Y10T29/49108
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Quick Facts
Patent No.
US 9,466,853
App. No.
13/247,417
Granted
Oct 11, 2016
Kind
B2
Abstract

Compositions and methods of making are provided for a high energy density aluminum battery. The battery comprises an anode comprising aluminum metal. The battery further comprises a cathode comprising a material capable of intercalating aluminum or lithium ions during a discharge cycle and deintercalating the aluminum or lithium ions during a charge cycle. The battery further comprises an electrolyte capable of supporting reversible deposition and stripping of aluminum at the anode, and reversible intercalation and deintercalation of aluminum or lithium at the cathode.

Claims (32)

1. A battery comprising:

an anode comprising aluminum metal;

a cathode comprising spinel AIMn 2 O 4 ; and

an electrolyte, wherein the electrolyte is an ionic liquid comprising an aluminate selected from the group consisting of alkylimidazolium aluminates, alkylpyridinium aluminates, alkylfluoropyrazolium aluminates, alkyltriazolium aluminates, aralkylammonium aluminates, alkylalkoxyammonium aluminates, aralkylphosphonium aluminates, aralkylsulfonium aluminates, and mixtures thereof.

2. The battery of claim 1 , wherein the battery is a secondary battery.

3. The battery of claim 2 , wherein the secondary battery maintains a discharge capacity of at least 50% of an initial discharge capacity after 50 discharge cycles.

4. The battery of claim 1 , wherein the anode is an aluminum metal alloy.

5. The battery of claim 4 , wherein the aluminum metal alloy comprises an element selected from the group consisting of: copper, magnesium, manganese, silicon, titanium, zinc, and mixtures thereof.

6. The battery of claim 1 , wherein the aluminate is ethylmethylimidazolium tetrachloroaluminate having a molar ratio of aluminum chloride to EMIC greater than 1:1.

7. The battery of claim 6 , wherein the electrolyte further comprises an alkali metal halide additive.

8. The battery of claim 7 , wherein the alkali metal halide additive is selected from the group consisting of: NaCl, KCl, NH 4 Cl, and mixtures thereof.

9. The battery of claim 1 , wherein the ionic liquid comprises ethylmethylimidazolium tetrachloroaluminate.

10. A method of making a battery comprising:

providing an anode comprising aluminum metal;

providing a cathode comprising spinel AIMn 2 O 4 ; and

providing an electrolyte, wherein the electrolyte is an ionic liquid comprising an aluminate selected from the group consisting of alkylimidazolium aluminates, alkylpyridinium aluminates, alkylfluoropyrazolium aluminates, alkyltriazolium aluminates, aralkylammonium aluminates, alkylalkoxyammonium aluminates, aralkylphosphonium aluminates, aralkylsulfonium aluminates, and mixtures thereof.

11. The method of claim 10 , wherein the aluminate is ethylmethylimidazolium tetrachloroaluminate having a molar ratio of aluminum chloride to EMIC of greater than 1:1.

12. The method of claim 10 , wherein the electrolyte further comprises an alkali metal halide additive.

13. The method of claim 11 , wherein the electrolyte further comprises an alkali metal halide additive.

14. The battery of claim 1 , wherein the cathode further comprises a carbon material and a binder.

15. The battery of claim 14 , wherein the cathode comprises:

approximately 50-90% of the spinel AlMn 2 O 4 ;

approximately 1-20% of the binder; and

approximately 1-40% of the carbon material.

16. The battery of claim 15 , wherein the carbon material is carbon black.

17. The battery of claim 1 , wherein the cathode comprises an active material, the active material being the spinel AlMn 2 O 4 .

18. The battery of claim 17 , wherein the cathode further comprises a carbon material and a binder.

19. The battery of claim 18 , wherein the cathode comprises:

approximately 50-90% of the spinel AlMn 2 O 4 as the active material of the cathode;

approximately 1-20% of the binder; and

approximately 1-40% of the carbon material.

20. The battery of claim 19 , wherein the carbon material is carbon black.

Assignments (6)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 25, 2016
From: MANTHIRAM, ARUMUGAM
To: BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM
Reel/Frame 039541/0610 →
CORRECTIVE ASSIGNMENT TO CORRECT THE THIRD INVENTOR NAME PREVIOUSLY RECORDED AT REEL: 027424 FRAME: 0130. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 20, 2016
From: BROWN, GILBERT M.; MC INTYRE, TIMOTHY J.; SUN, XIAO-GUANG; PARANTHAMAN, MARIAPPAN PARANS; DAI, SHENG; DUDNEY, NANCY J.
To: UT-BATTELLE, LLC
Reel/Frame 039079/0837 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 29, 2012
From: OAK RIDGE ASSOCIATED UNIVERSITIES
To: UT-BATTELLE, LLC
Reel/Frame 028467/0261 →
CONFIRMATORY LICENSE Recorded Jan 30, 2012
From: UT-BATTELLE, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 027614/0651 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2011
From: LIU, HANSAN
To: OAK RIDGE ASSOCIATED UNIVERSITIES
Reel/Frame 027424/0053 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2011
From: BROWN, GILBERT M.; MCINTYRE, TIMOTHY J.; SUN, XIAGO-GUANG; PARANTHAMAN, MARIAPPAN PARANS; DAI, SHENG; DUDNEY, NANCY J.
To: UT-BATTELLE, LLC
Reel/Frame 027424/0130 →
Continuity (2)
Continuation In Part 12895487 · Sep 30, 2010
Related Publication 20120082905A1 · Apr 5, 2012