IP Library › Granted Patent US 9,580,622
Granted Patent B2
US 9,580,622 · App. 14/556,286 · Granted Feb 28, 2017

Crosslinkable composition, a method of making the same and a crosslinked composition produced therefrom

Inventors: Jeff R. Anderson (Midland, MI); Gary E. Spilman (Midland, MI); Paul J. Popa (Auburn, MI); John N. Argyropoulos (Midland, MI)
Assignee: Dow Global Technologies LLC
C09D175/04C08F8/30C08G16/0225C08G16/06C09D133/066C09D161/00C09D175/16Y10T428/31551Y10T428/31591Y10T428/31598Y10T428/31605
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Quick Facts
Patent No.
US 9,580,622
App. No.
14/556,286
Granted
Feb 28, 2017
Kind
B2
Abstract

A crosslinkable composition comprising: (i) one or more polycarbamates; (ii) one or more polyaldehydes; (iii) one or more polyols; and (iv) an acid catalyst is provided. Further provided are a method for making the crosslinkable composition, a crosslinked composition made therefrom, a coating comprising the crosslinked composition and articles comprising a substrate and the coating.

Claims (13)

1. A crosslinkable composition comprising: (i) one or more polycarbamates; (ii) one or more polyaldehydes; (iii) one or more polyols; and (iv) an acid catalyst;

wherein the one or more polyols are selected from the group consisting of 1,4-butanediol, 1,5-pentanediol, 1,6-hexanediol and 1,4-cyclohexanedimethanol, linear aliphatic polycarbonate polyesters, linear aliphatic polycarbonate diol, and linear aliphatic polyester polyols.

2. The crosslinkable composition according to claim 1 , further comprising a polyisocyanate.

3. The crosslinkable composition according to claim 1 , wherein component (iii) is a linear aliphatic polycarbonate polyester having a weight average molecular weight from 800 to 1200 daltons.

4. The crosslinkable composition according to claim 1 , wherein component (iii) is a linear aliphatic polycarbonate diol having a weight average molecular weight from 450 to 850 daltons.

5. A crosslinked composition produced by curing the crosslinkable composition according to claim 1 , wherein the curing occurs at a temperature from 0 to 80° C.

6. A coating composition comprising the crosslinked composition according to claim 5 .

7. An article comprising a substrate and a coating composition according to claim 6 .

8. The article according to claim 7 , wherein the substrate is one or more selected from the group consisting of woods, composites, concretes, metals, and plastics.

9. A method of making a crosslinkable composition comprising: selecting (i) one or more polycarbamates; selecting (ii) one or more polyaldehydes; selecting (iii) one or more polyols; and mixing components (i)-(iii) in any order; wherein the one or more polyols are selected from the group consisting of 1,4-butanediol, 1,5-pentanediol, 1,6-hexanediol and 1,4-cyclohexanedimethanol, linear aliphatic polycarbonate polyesters, linear aliphatic polycarbonate diol, and linear aliphatic polyester polyols.

10. The method of making a crosslinkable composition according to claim 9 wherein components (ii) and (iii) are mixed together prior to addition to component (i).

11. The coating composition according to claim 6 , wherein the coating composition exhibits an improvement in direct impact resistance of at least 50% over the impact resistance of a comparative coating having the same composition with the exception that the comparative coating is produced from a crosslinkable composition which is produced from a crosslinkable composition with no polyol.

12. The coating composition according to claim 6 , wherein the coating composition exhibits an improvement in MEK resistance of at least 50% over the impact resistance of a comparative coating having the same composition with the exception that the comparative coating is produced from a crosslinkable composition which is produced from a crosslinkable composition with no polyol.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 12, 2017
From: ANDERSON, JEFF R.; SPILMAN, GARY E.; POPA, PAUL J.; ARGYROPOULOS, JOHN N.
To: DOW GLOBAL TECHNOLOGIES LLC
Reel/Frame 040954/0139 →
Continuity (2)
Provisional Application 61916438 · Dec 16, 2013
Related Publication 20150166828A1 · Jun 18, 2015