IP Library › Granted Patent US 9,603,385
Granted Patent B2
US 9,603,385 · App. 13/793,537 · Granted Mar 28, 2017

Immobilized diluents for smoking articles

Inventors: Shuzhong Zhuang (Richmond, VA); Georgios D. Karles (Richmond, VA)
Assignee: Philip Morris USA Inc.
A24D3/06A24B15/245A24B15/246A24B15/28A24B15/287
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,603,385
App. No.
13/793,537
Granted
Mar 28, 2017
Kind
B2
Abstract

Immobilized diluents in a smoking article are provided, wherein diluents can be immobilized through absorption and/or adsorption of the diluents into immobilizing materials, such as sorbents like silica gels. By immobilizing diluents, the diluents can be available for vaporization, while still being protected from migration and/or loss of the diluents in a smoking article.

Claims (14)

1. A method of reducing tar generated from tobacco combustion, pyrolysis or distillation in tobacco smoke, comprising:

heating a tobacco-containing portion of a smoking article; and

releasing diluents immobilized within porous immobilizing particles in the tobacco-containing portion of the smoking article by heating the diluents immobilized within the porous immobilizing particles, wherein the released diluent alters the composition of the total particulate matter (TPM) in the tobacco smoke,

wherein the diluents immobilized within the porous immobilizing particles are sealed with a coating, and

wherein the porous immobilizing particles comprise silica gels, molecular sieves, activated carbons, or combinations thereof.

2. The method of claim 1 , wherein the heating the diluents immobilized within the porous immobilizing particles comprises:

heating porous immobilizing particles which comprise non-combustible sorbents, wherein the sorbents have a pore volume of about 0.2 cc/g to about 1.5 cc/g, a surface area of about 100 m 2 /g to about 1000 m 2 /g, and/or a transverse dimension of about 0.05 mm to about 2 mm; and

vaporizing the diluents immobilized within the porous immobilizing particles.

3. The method of claim 2 , wherein the vaporizing the diluents immobilized within the porous immobilizing particles comprises:

heating the diluents to temperatures at or above 180° C. to vaporize the diluents, wherein the diluents comprise glycerin, propylene glycol, triacetin, triethylene glycol, triethyl citrate, or combinations thereof.

4. The method of claim 1 , wherein the porous immobilizing particles consist of a non-combustible sorbent.

5. The method of claim 1 , wherein the method further comprises reducing the concentration of carbonyls, volatile organic compounds, polycyclic aromatic hydrocarbons, tobacco specific nitrosamines, and/or phenolic compounds in the tobacco smoke.

6. The method of claim 1 , further comprising impregnating the porous immobilizing particles by contacting sorbent particles with the diluent, pressurizing and/or heating the sorbent and diluent until the sorbent is loaded with the diluent in an amount ranging from about 60 wt. % to about 120 wt. %.

7. The method of claim 1 , wherein the diluents immobilized within the porous immobilizing particles are sealed with a layer of a polysaccharide.

Continuity (3)
Division 11812028 · Jun 14, 2007
Provisional Application 60835090 · Aug 3, 2006
Related Publication 20130220351A1 · Aug 29, 2013