IP Library Granted Patent US 9,604,979
Granted Patent B2
US 9,604,979 · App. 14/349,228 · Granted Mar 28, 2017

Pyrroloquinoline quinone alcohol adduct

Inventors: Kazuto Ikemoto (Niigata, JP); Hitoshi Sakamoto (Niigata, JP)
Assignee: Mitsubishi Gas Chemical Company, Inc.
C07D471/04A23K20/137A23L2/52A23L2/58A23L5/47A23L33/10A61K8/4926A61K31/122A61K31/4745A61Q1/06A61Q1/10A61Q5/02A61Q19/007A61Q19/08A23V2002/00A61K2800/42
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Quick Facts
Patent No.
US 9,604,979
App. No.
14/349,228
Granted
Mar 28, 2017
Kind
B2
Abstract

The present invention relates to a compound represented by the formula (A) or (B), or a salt thereof capable of improving a red color of pyrroloquinoline quinone (PQQ) and obtaining functions of original PQQ, and to a method of efficiently manufacturing the compound. wherein R is an alkyl group, a hydroxyalkyl group, a dihydroxyalkyl group, or an alkoxyalkyl group.

Claims (28)

1. A composition comprising:

(a) a compound represented by formula (A) or (B), or a salt thereof:

where R is alkyl, hydroxyalkyl, dihydroxyalkyl, or alkoxylalkyl; and

(b) coenzyme Q10.

2. A beverage, comprising the composition of claim 1 .

3. A food, comprising the composition of claim 1 .

4. A cosmetic, comprising the composition of claim 1 .

5. The composition according to claim 1 , wherein the composition is in a form of a powder, a tablet, a chewable tablet, a capsule, a granule, an injectable, a liquid, an eye drop, a lotion, a hair tonic, a cosmetic emulsion, a spray liquid, an aerosol, a drink liquid, a liquid fertilizer, or a preservation solution.

6. A method for manufacturing the composition according to claim 1 , the method comprising:

(a) adding one equivalent of an alcohol represented by formula (2) to the pyrroloquinoline quinone represented by formula (1) or a salt thereof:

wherein where R is alkyl, hydroxyalkyl, dihydroxyalkyl, or alkoxylalkyl; and

(b) admixing coenzyme Q10 with the compound obtained by step (a).

7. The method according to claim 6 , wherein said adding is performed in a solvent having a water content of 50 mass % or less.

8. The method according to claim 6 , comprising adding the alcohol represented by formula (2) to a monoalkali metal salt of the pyrroloquinoline quinone.

9. The method according to claim 7 , comprising adding the alcohol represented by formula (2) to a monoalkali metal salt of the pyrroloquinoline quinone.

10. A compound by formula (A) or (B), or a salt thereof:

where R is hydroxyalkyl, dihydroxyalkyl, or alkoxylalkyl.

11. A composition, comprising the compound or the salt thereof of claim 10 .

12. The composition according to claim 11 , wherein the composition is selected from a beverage, a food or a cosmetic.

13. The composition according to claim 11 , comprising coenzyme Q10.

14. The composition according to claim 13 , wherein the composition is in a form of a powder, a tablet, a chewable tablet, a capsule, a granule, an injectable, a liquid, an eye drop, a lotion, a hair tonic, a cosmetic emulsion, a spray liquid, an aerosol, a drink liquid, a liquid fertilizer, or a preservation solution.

15. The composition according to claim 13 , wherein the composition is selected from a beverage, a food or a cosmetic.

16. A method for manufacturing the compound or the salt thereof according to claim 10 , the method comprising:

adding one equivalent of an alcohol represented by formula (2) to the pyrroloquinoline quinone represented by formula (1) or a salt thereof:

wherein R is hydroxyalkyl, dihydroxyalkyl, or alkoxylalkyl.

17. The method according to claim 16 , wherein said adding is performed in a solvent having a water content of 50 mass % or less.

18. The method according to claim 16 , comprising adding the alcohol represented by formula (2) to a monoalkali metal salt of the pyrroloquinoline quinone.

19. The method according to claim 16 , further comprising admixing coenzyme Q10 to the compound thus obtained.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 25, 2014
From: IKEMOTO, KAZUTO; SAKAMOTO, HITOSHI
To: MITSUBISHI GAS CHEMICAL COMPANY, INC.
Reel/Frame 032753/0905 →
Priority Claims (1)
JP 2011-218968 · Oct 3, 2011 · national
Continuity (1)
Related Publication 20150037308A1 · Feb 5, 2015