IP Library › Granted Patent US 9,617,156
Granted Patent B2
US 9,617,156 · App. 13/824,310 · Granted Apr 11, 2017

Carbon nanostructures and networks produced by chemical vapor deposition

Inventors: Krishna Narayan Kumar Kowlgi (Delft, NL); Gerardus Joseph Maria Koper (Delft, NL); Rutger Alexander David Van Raalten (Delft, NL)
Assignee: CarbonX B.V.
C01B31/0226B01J21/185B01J23/42B01J35/0013B01J37/0238B82Y30/00B82Y40/00C01B31/00C01B31/0206B01J37/16H01M4/926H01M4/96Y10T428/256Y10T428/31678
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Quick Facts
Patent No.
US 9,617,156
App. No.
13/824,310
Granted
Apr 11, 2017
Kind
B2
Abstract

The invention pertains to a method for manufacturing crystalline carbon nanostructures and/or a network of crystalline carbon nanostructures, comprising: (i) providing a bicontinuous micro-emulsion containing metal nanoparticles having an average particle size between 1 and 100 nm; (ii) bringing said bicontinuous micro-emulsion into contact with a substrate; and (iii) subjecting said metal nanoparticles and a gaseous carbon source to chemical vapor deposition, thus forming carbon nanostructures and/or a network of carbon nanostructures. Therewith, it is now possible to obtain crystalline carbon nanostructures networks, preferably carbon nanotubes networks.

Claims (10)

1. A method for manufacturing a chemically interconnected network of crystalline carbon nanostructures, comprising

(i) contacting a substrate with a bicontinuous micro-emulsion comprising metal nanoparticles having an average particle size between 1 and 100 nm, wherein deviations in paticles size from the average particle size are less than 10 %;

(ii) subjecting the metal nanoparticles and a gaseous carbon source to chemical vapor deposition, thus forming a network of carbon nanostructures; and

(iii) obtaining a network of chemically interconnected crystalline carbon nanostructures.

2. The method according to claim 1 , wherein the bicontinuous micro-emulsion comprises at least 15 nM metal nanoparticles calculated on the aqueous phase.

3. A network of chemically interconnected crystalline carbon nanostructures obtainable by the method according to claim 1 .

4. The network according to claim 3 , wherein metal nanoparticles having an average size between 1 and 100 nm are embedded in said network.

5. The network according to claim 3 , being a carbon nanotubes network.

6. A composite composition comprising a carbon nanostructure network according to claim 3 and a polymer.

7. The composite composition according to claim 6 , comprising the network in an amount of 0.1-10 wt %, based on total polymer weight in the composite composition.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 5, 2014
From: DELFT ENTERPRISES B.V.
To: CARBONX B.V.
Reel/Frame 033040/0608 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 11, 2013
From: KOWLGI, KRISHNA NARAYAN KUMAR; KOPER, GERARDUS JOSEPH MARIA; VAN RAALTEN, RUTGER ALEXANDER DAVID
To: DELFT ENTERPRISES B.V.
Reel/Frame 031386/0152 →
Priority Claims (1)
NL 2005365 · Sep 17, 2010 · national
Continuity (1)
Related Publication 20130244023A1 · Sep 19, 2013