Multi-function epoxy casting resin system
Disclosed herein are embodiments of an epoxy casting resin system which can be used to at least partially cover an electronic component or mechanism. In some embodiments, the epoxy resin can have a low viscosity, while maintaining advantageous physical, thermal, and electrical properties. Further described are methods for making embodiments of the epoxy casting resin.
1. An uncured epoxy resin comprising:
15-26 wt. % of at least one epoxy resin base reactive constituent, wherein the at least one epoxy resin base reactive constituent comprises bisphenol F epoxy resin;
2-5 wt. % of diluent, wherein the diluent comprises butyl glycidyl ether;
0.5-1.5 wt. % of at least one color pigment;
40-60 wt. % of at least one thermally conductive filler, wherein the at least one thermally conductive filler comprises aluminum oxide;
2.5-4.0 wt. % of at least one reactive constituent, wherein the at least one reactive constituent comprises phosphorous salt;
8.5-16 wt. % of at least one flame retardant, wherein the at least one flame retardant comprises 7%-12% alumina trihydrate and 1.5%-4% ammonium poly phosphate;
5-10 wt. % of at least one reactive agent, wherein the at least one reactive agent comprises polyglycol diamine; and
1-3 wt. % catalyst, wherein the catalyst comprises a polyamine blend.
2. The uncured epoxy resin system of claim 1 , wherein the viscosity of the resin is 3,500-4500 cP mixed measured at 24° C.
3. A cured epoxy formed from the uncured epoxy resin of claim 2 .
4. The cured epoxy resin of claim 3 , wherein the cured resin has a thermal conductivity of 0.70 W/(m·K) at 60° C.
5. The cured epoxy resin of claim 3 , wherein the cured resin has a volume resistivity of 3.95×10 15 ohm·cm.
6. The cured epoxy resin of claim 3 , wherein the cured resin has a relative temperature index for impact, strength, and electrical of 130° C.
7. The cured epoxy resin of claim 3 , wherein the cured resin has a 200 g. pot life of 1 to 2 hours at 25° C.
8. The uncured epoxy resin of claim 1 , wherein the aluminum oxide has a mesh size of less than 50 Mesh.
9. The uncured epoxy resin of claim 1 comprising:
about 17.2%-21.2% bisphenol F epoxy resin;
about 2.4%-4.4% butyl glycidyl ether;
about 0.5%-1.0% color pigment;
about 51%-57% aluminum oxide;
about 2.5%-4% phosphorous salt;
about 7%-11% alumina trihydrate;
about 1.5%-3.3% ammonium poly phosphate;
about 5%-8.8% polyglycol diamine; and
about 1%-1.9% of polyamine blend.
10. The uncured epoxy resin of claim 9 comprising:
about 19.2% bisphenol F epoxy resin;
about 3.4% butyl glycidyl ether;
about 0.75% color pigment;
about 54% aluminum oxide;
about 3.4% phosphorous salt;
about 9% alumina trihydrate;
about 2.3% ammonium poly phosphate;
about 6.8% polyglycol diamine; and
about 1.4% of polyamine blend.
11. The uncured epoxy resin of claim 1 , the uncured epoxy resin consisting essentially of:
about 15%-26% bisphenol F epoxy resin;
about 2%-5% butyl glycidyl ether;
about 0.5%-1.5% color pigment;
about 40%-60% aluminum oxide;
about 2.5%-4% phosphorous salt;
about 7%-12% alumina trihydrate;
about 1.5%-4% ammonium poly phosphate;
about 5%-10% polyglycol diamine; and
about 1%-3% of polyamine blend.
12. The uncured epoxy resin of claim 11 , the uncured epoxy resin consisting essentially of:
about 19.2% bisphenol F epoxy resin;
about 3.4% butyl glycidyl ether;
about 0.75% color pigment;
about 54% aluminum oxide;
about 3.4% phosphorous salt;
about 9% alumina trihydrate;
about 2.3% ammonium poly phosphate;
about 6.8% polyglycol diamine; and
about 1.4% of polyamine blend.
13. An uncured epoxy resin consisting essentially of, in wt. %:
about 15%-26% bisphenol F epoxy resin;
about 2%-5% butyl glycidyl ether;
about 0.5%-1.5% of at least one color pigment;
about 40%-60% aluminum oxide;
about 2.5%-4% phosphorous salt;
about 7%-12% alumina trihydrate;
about 1.5%-4% ammonium poly phosphate;
about 5%-10% polyglycol diamine; and
about 1%-3% of polyamine blend.
14. The uncured epoxy resin of claim 13 , the uncured epoxy resin consisting essentially of:
about 19.2% bisphenol F epoxy resin;
about 3.4% butyl glycidyl ether;
about 0.75% color pigment;
about 54% aluminum oxide;
about 3.4% phosphorous salt;
about 9% alumina trihydrate;
about 2.3% ammonium poly phosphate;
about 6.8% polyglycol diamine; and
about 1.4% of polyamine blend.
15. The uncured epoxy resin of claim 13 , wherein the viscosity of the resin is 3,500-4,500 cP mixed measured at 24° C.
16. The uncured epoxy resin of claim 13 , wherein the aluminum oxide has a mesh size of less than 50 Mesh.
17. A cured epoxy formed from the uncured epoxy resin of claim 13 .
18. The cured epoxy resin of claim 17 , wherein the cured resin has a thermal conductivity of 0.70 W/(m·K) at 60° C.
19. The cured epoxy resin of claim 17 , wherein the cured resin has a volume resistivity of 3.95×10 15 ohm·cm.
20. The cured epoxy resin of claim 17 , wherein the cured resin has a relative temperature index for impact, strength, and electrical of 130° C.
21. The cured epoxy resin of claim 17 , wherein the cured resin has a 200 g. pot life of 1 to 2 hours at 25° C.