IP Library Granted Patent US 9,759,721
Granted Patent B2
US 9,759,721 · App. 14/161,117 · Granted Sep 12, 2017

Rapid method for detection of pathogen

Inventors: Pablo Lozano Sánchez (Tarragona, ES); Gemma Freixes Prous (Barcelona, ES); Sergio Martinez Montequín (Tarragona, ES); Anna Pallares Lleo (Tarragona, ES); Cristina Perez Girona (Lleida, ES); Katia Uliaque Cugat (Tarragona, ES)
Assignee: IMICROQ, S.L.
G01N33/56916C12Q1/04C12Q1/045C12Q1/6888G01N33/569
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Quick Facts
Patent No.
US 9,759,721
App. No.
14/161,117
Granted
Sep 12, 2017
Kind
B2
Abstract

The present specification discloses methods of detecting a pathogen of interest and components useful in carrying out these methods, including a pre-enrichment media, and enrichment media and a detection solution.

Claims (13)

1. A method of detecting Salmonella in a sample, the method consisting essentially of:

a) incubating the sample in a liquid pre-enrichment medium consisting essentially of a peptone low growth nutrient component, a malachite green growth inhibiting agent, and a nonylphenol ethoxylate surfactant with bacteriostatic or bactericidal action, wherein the incubation is at about 35° C. to about 39° C. for about 14 to 15 hours, and wherein the sample is a food sample, a feces sample or a raw livestock sample:

b) incubating an aliquot of the pre-enrichment medium from step (a) in a separate liquid enrichment medium, the enrichment medium consisting essentially of a peptone high growth nutrient component and ferric ammonium citrate, wherein the incubation is at about 39° C. to about 43° C. for about 5-7 hours, wherein the aliquot of the pre-enrichment medium is about 1/50 to about 1/1000 a volume of the enrichment medium;

c) purifying the liquid enrichment medium to increase concentration of the Salmonella and/or decrease contaminants using an immuno-precipitation method employing antibodies for the Salmonella linked to magnetic particles; and

d) detecting the presence or absence of the Salmonella by analyzing an aliquot of the purified enrichment medium from step (c), using an electrochemical sensor-based detection method.

2. The method according to claim 1 , wherein the nonylphenol ethoxylate surfactant is selected from the group consisting of Nonoxynol-4 (NP-4), Nonoxynol-6 (NP-6), Nonoxynol-7 (NP-7), Nonoxynol-8 (NP-8), Nonoxynol-9 (NP-9), Nonoxynol-10 (NP-10), Nonoxynol-11 (NP-11), Nonoxynol-12 (NP-12), Nonoxynol-13 (NP-13), Nonoxynol-15 (NP-15), Nonoxynol-30 (NP-30), Nonoxynol-40 (NP-40), Nonoxynol-50 (NP-50), Nonoxynol-55 (NP-55), and Nonoxynol-70 (NP-70).

3. The method according to claim 1 , wherein the malachite green growth inhibiting agent is selected from the group consisting of malachite green dye and brilliant green dye.

4. The method according to claim 1 , wherein the aliquot of pre-enrichment medium in step (b) is about 1/50 to about 1/500 of the volume of the enrichment medium used in step (b).

5. The method according to claim 1 , wherein the ammonium ferric citrate is at a concentration of about 0.1 mg/m L to about 5.0 mg/m L.

6. The method according to claim 1 , wherein the electrochemical sensor-based detection method is a biosensor-based detection method.

7. The method according to claim 1 , wherein the Salmonella is Salmonella typhimurium or Salmonella typhi.

8. The method according to claim 1 , wherein the malachite green growth inhibiting agent is at a concentration of about 0.5% (v/v) to about 3% (v/v).

9. The method according to claim 1 , wherein the surfactant is at a concentration of about 0.5% (v/v) to about 5% (v/v).

Priority Claims (1)
ES 201330064 · Jan 22, 2013 · national
Continuity (2)
Provisional Application 61927401 · Jan 14, 2014
Related Publication 20140206016A1 · Jul 24, 2014