IP Library Granted Patent US 9,796,797
Granted Patent B2
US 9,796,797 · App. 14/383,050 · Granted Oct 24, 2017

Polyethylene with controlled wax content, chlorinated polyethylene thereof and molded article produced from the chlorinated polyethylene

Inventors: Soung Hun Yoo (Daejeon, KR); Geun Yeol Bae (Daejeon, KR); Sang Rok Do (Daejeon, KR)
Assignee: LG Chem, Ltd.
C08F110/02B29B7/52B29C47/88B29C71/02B32B1/02B32B1/08C08F8/20C08F210/02C08F210/04C08F210/06C08F210/08C08F210/10C08F255/023C08J3/247C08J5/18C08J7/08C08K5/14H01B3/441C08J2323/28C08J2391/06Y10T428/139Y10T428/1352Y10T428/1393
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Quick Facts
Patent No.
US 9,796,797
App. No.
14/383,050
Granted
Oct 24, 2017
Kind
B2
Abstract

Disclosed are polyethylene, chlorinated polyethylene thereof and a molded article produced from the chlorinated polyethylene. More specifically, disclosed are polyethylene for preparation of chlorinated polyethylene, the polyethylene having a molecular weight distribution (MWD) of 5 or less, a melting index (5.0 kg) of 0.1 to 10 dg/min, a weight average molecular weight of 50,000 to 300,000 g/mol, a melting temperature of 125 to 135° C., a wax content of 0.0001 to 3% by weight or 0.01 to 0.3% by weight and a density of 0.94 g/cm 3 or more, chlorinated polyethylene thereof and a molded article produced from the chlorinated polyethylene.

Claims (25)

1. Polyethylene for preparation of chlorinated polyethylene, the polyethylene having a molecular weight distribution (MWD) of 5 or less, a melting index (5.0 kg) of 0.1 to 10 dg/min, a weight average molecular weight of 50,000 to 300,000 g/mol, a melting temperature of 125 to 140° C., a density of 0.94 g/cm 3 or more and a wax content of 0.01 to 0.3% by weight.

2. The polyethylene according to claim 1 , wherein the polyethylene has a low molecular weight (≦5,000 g/mol) content of 0.01 to 5% by weight.

3. The polyethylene according to claim 1 , wherein the molecular weight distribution (MWD) is 2.1 to 3.4.

4. The polyethylene according to claim 1 , wherein the melting index (5.0 kg) is 0.3 to 7 dg/min.

5. The polyethylene according to claim 1 , wherein the melting temperature is 125 to 135° C.

6. The polyethylene according to claim 1 , wherein the density is 0.945 to 0.955 g/cm 3 .

7. The polyethylene according to claim 1 , wherein the polyethylene has a wax content of 0.05 to 0.2% by weight.

8. The polyethylene according to claim 1 , wherein the polyethylene has an average particle size of 30 to 400 μm.

9. The polyethylene according to claim 1 , wherein the polyethylene is prepared in the presence of a metallocene catalyst.

10. Chlorinated polyethylene prepared by reacting the polyethylene according to claim 1 with chlorine.

11. The chlorinated polyethylene according to claim 10 , wherein the chlorinated polyethylene has a chlorine content of 20 to 45% by weight.

12. The chlorinated polyethylene according to claim 10 , wherein the chlorinated polyethylene has a Mooney viscosity of 70 to 110.

13. The chlorinated polyethylene according to claim 10 , wherein the chlorinated polyethylene has a volume resistance of 10 13 to 10 17 Ωcm and thermal stability of 150 to 180° C.

14. An extrusion-molded article produced from the chlorinated polyethylene according to claim 10 .

15. The extrusion-molded article according to claim 14 , wherein the extrusion-molded article is cross-linked using a peroxide cross-linking agent.

16. The extrusion-molded article according to claim 15 , wherein the extrusion-molded article has a volume resistance of 1×10 14 Ωcm to 200×10 14 Ωcm.

17. The extrusion-molded article according to claim 14 , wherein the extrusion-molded article is a wire cable or a hose.

18. A method for preparing chlorinated polyethylene comprising:

dispersing 100 parts by weight of the polyethylene according to claim 1 , 0.1 to 0.2 parts by weight of an emulsifier, and 1 to 5 parts by weight of a dispersant in water; and

reacting the resulting dispersion with 80 to 200 parts by weight of chlorine in the presence of 0.01 to 1.0 parts by weight of a catalyst.

19. A method for producing an extrusion-molded article comprising:

a) roll-mill compounding the chlorinated polyethylene according to claim 10 with a cross-linking agent;

b) extruding the compounded chlorinated polyethylene;

c) allowing the extrudate to stand at 100 to 180° C. for 3 to 60 minutes; and

d) cross-linking (curing) the extrudate.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 4, 2014
From: YOO, SOUNG HUN; BAE, GEUN YEOL; DO, SANG ROK
To: LG CHEM, LTD.
Reel/Frame 033672/0065 →
Priority Claims (2)
KR 10-2013-0043729 · Apr 19, 2013 · national
KR 10-2014-0044897 · Apr 15, 2014 · national
Continuity (1)
Related Publication 20160229931A1 · Aug 11, 2016