IP Library Granted Patent US 9,873,982
Granted Patent B2
US 9,873,982 · App. 14/880,873 · Granted Jan 23, 2018

Method of increasing drainage performance of a pulp slurry during manufacture of paper products, and products therefrom

Inventors: John C. Harrington (Newark, DE); Kate Marritt Lusvardi (Chadds Ford, PA); Fushan Zhang (Hockessin, DE)
Assignee: Solenis Technologies, L.P.
D21H17/25D21H3/00D21H11/18D21H17/37D21H17/375D21H17/38D21H17/42D21H17/43D21H17/44D21H17/45D21H17/72D21H21/10D21H23/04
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Quick Facts
Patent No.
US 9,873,982
App. No.
14/880,873
Granted
Jan 23, 2018
Kind
B2
Abstract

A method of increasing the drainage performance of a pulp slurry during the manufacture of paper products by adding (a) at least one microfibrillated cellulose and (b) at least one associative polymer or at least one branched or crosslinked copolymer to the pulp slurry. This addition occurs before the dewatering step where the pulp slurry is formed into a fibrous mat.

Claims (18)

1. A method for increasing the drainage performance of a pulp slurry, comprising adding (a) at least one microfibrillated cellulose and (b) at least one associative polymer to a pulp slurry, wherein the at least one microfibrillated cellulose and the at least one associative polymer are added at a ratio of from about 10:1 to about 1:10 of the at least one microfibrillated cellulose to the at least one associative polymer.

2. The method of claim 1 , wherein the pulp slurry is present in a wet end of a paper machine prior to adding the at least one microfibrillated cellulose and the at least one associative polymer to the pulp slurry.

3. The method of claim 1 , wherein the at least one microfibrillated cellulose and the at least one associative polymer are added to the pulp slurry to form a mixture, and then introducing the mixture to a paper machine.

4. The method of claim 1 , wherein the active solids of the at least one microfibrillated cellulose and the at least one associative polymer are present in the pulp slurry at a range of from about 0.01 wt % to about 1 wt % based on the weight of dry pulp in the pulp slurry.

5. The method of claim 1 , wherein the active solids of the at least one microfibrillated cellulose and the at least one associative polymer are present in the pulp slurry at a range of from about 0.01 wt % to about 0.5 wt % based on the weight of dry pulp in the pulp slurry.

6. The method of claim 1 , wherein the at least one microfibrillated cellulose and the at least one associative polymer are added at a ratio of from about 5:1 to about 1:2 of the at least one microfibrillated cellulose to the at least one associative polymer.

7. The method of claim 6 , wherein the active solids of the at least one microfibrillated cellulose and the at least one associative polymer are present in the pulp slurry at a range of from about 0.01 wt % to about 0.15 wt % based on the weight of dry pulp in the pulp slurry.

8. The method of claim 1 , wherein the at least one microfibrillated cellulose is derivatized microfibrillated cellulose having an anionic charge.

9. The method of claim 8 , wherein the derivatized microfibrillated cellulose has a degree of substitution in a range of from about 0.02 to about 0.50.

10. The method of claim 8 , wherein the derivatized microfibrillated cellulose has a degree of substitution in a range of from about 0.10 to about 0.35.

11. The method of claim 8 , wherein the derivatized microfibrillated cellulose has a degree of substitution in a range of from about 0.1 to about 0.25.

12. The method claim 1 , wherein the at least one microfibrillated cellulose is derivatized microfibrillated cellulose having a cationic charge.

13. The method of claim 12 , wherein the derivatized microfibrillated cellulose has a degree of substitution in a range of from about 0.02 to about 0.50.

14. The method of claim 12 , wherein the derivatized microfibrillated cellulose has a degree of substitution in a range of from about 0.10 to about 0.35.

15. The method of claim 1 , wherein the at least one associative polymer is an anionic copolymer comprising the formula (I):

wherein B is a nonionic polymer segment comprising one or more ethylenically unsaturated nonionic monomers; F is an anionic polymer segment comprising one or more ethylenically unsaturated anionic monomers; and the molar percent ratio of B:F is in a range of from about 95:5 to about 5:95.

16. The method of claim 1 , wherein the at least one microfibrillated cellulose and the at least one associative polymer are added at a ratio of from about 10:1 to about 5:4 of the at least one microfibrillated cellulose to the at least one associative polymer.

17. A paper product comprising (a) cellulose pulp, (b) at least one microfibrillated cellulose, and (c) at least one associative polymer.

Assignments (14)
SECURITY INTEREST Recorded Nov 14, 2025
From: CHEM-AQUA, INC.; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; NCH CORPORATION; NCH LIFE SCIENCES LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073570/0838 →
RELEASE OF SECURITY INTEREST Recorded Nov 14, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073564/0864 →
SECURITY AGREEMENT (NOTES) Recorded Oct 10, 2025
From: DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073061/0885 →
RELEASE OF 2023 NOTES PATENT SECURITY INTERESTS Recorded Oct 10, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073074/0198 →
SECURITY AGREEMENT (2024 NOTES) Recorded Jun 24, 2024
From: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 067824/0278 →
2023 NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE GLOBAL CORPORATION
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064225/0170 →
SECURITY AGREEMENT (NOTES) Recorded Sep 14, 2022
From: SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A. AS COLLATERAL AGENT
Reel/Frame 061432/0821 →
NOTES SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 058103/0066 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: GOLDMAN SACHS BANK USA
Reel/Frame 058102/0407 →
ABL PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: BANK OF AMERICA, N.A.
Reel/Frame 058102/0122 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058856/0724 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CITIBANK, N.A.
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058848/0636 →
FIRST LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CITIBANK, N.A., COLLATERAL AGENT
Reel/Frame 046595/0241 →
SECOND LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 046629/0213 →
Continuity (1)
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