IP Library › Granted Patent US 9,889,424
Granted Patent B2
US 9,889,424 · App. 14/795,897 · Granted Feb 13, 2018

Method and apparatus for producing radionuclide

Inventors: Takahiro Tadokoro (Tokyo, JP); Yuko Kani (Tokyo, JP)
Assignee: Hitachi, Ltd.
B01J19/085B01J19/0013B01J19/10G21G1/10B01J2219/0801B01J2219/0871B01J2219/0879
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Quick Facts
Patent No.
US 9,889,424
App. No.
14/795,897
Granted
Feb 13, 2018
Kind
B2
Abstract

A method for producing a radionuclide is provided that produces molybdenum trioxide 99 (Mo-99.O 3 ) and technetium oxide 99m (Tc-99m 2 .O 7 ) by emitting an electron beam accelerated by an electron linear accelerator to a molybdenum trioxide 100 (Mo-100.O 3 ) powder sample, and which separates and purifies technetium oxide 99m from both the molybdenum trioxide 99 and the technetium oxide 99m by using a radionuclide separation/purification unit. The method for producing a radionuclide supplies temperature-regulated gas to the molybdenum trioxide 100 powder sample during an irradiation period during which the electron beam is emitted to the molybdenum trioxide 100 powder sample.

Claims (24)

1. A method for producing molybdenum trioxide 99 (Mo-99.O 3 ) and technetium oxide 99m (Tc-99m 2 .O 7 ), comprising:

emitting an electron beam accelerated by an electron linear accelerator to a molybdenum trioxide 100 (Mo-100.O 3 ) powder sample;

supplying a temperature-regulated gas to the molybdenum trioxide 100 powder sample during an irradiation period where the electron beam is emitted to the molybdenum trioxide 100 powder sample; and

vibrating the molybdenum trioxide 100 powder sample during the irradiation period.

2. The method according to claim 1 , further comprising:

separating and purifying the technetium oxide 99m from both the molybdenum trioxide 99 and the molybdenum trioxide 100.

3. The method according to claim 1 , wherein

the gas supplied to the molybdenum trioxide 100 powder sample during the irradiation period is a gas mixture of oxygen gas and a noble gas.

4. The method according to claim 1 , further comprising:

measuring a temperature of the molybdenum trioxide 100 Powder sample during the irradiation period;

regulating a temperature of the gas so that the temperature of the molybdenum trioxide 100 powder sample is adjusted to be greater than or equal to a boiling point of the technetium oxide 99m and less than or equal to a melting point of the molybdenum trioxide 100 during the irradiation period.

5. The method according to claim 1 , wherein

the vibrating is performed by an ultrasonic vibration device.

6. The method according to claim 1 , wherein

the vibrating is performed by stirring with a gas flow.

7. The method according to claim 2 , wherein

a first bellows-type pipe supplies the temperature-regulated gas to the molybdenum trioxide 100 powder sample, and a second bellows-type pipe supplies the molybdenum trioxide 99 and the technetium oxide 99m to the separation/purification unit for a separation/purification unit for separating and purifying the technetium oxide 99m.

8. The method according to claim 1 , wherein

a bellows-type container contains the molybdenum trioxide 100 powder sample during the irradiation period.

9. The method according to claim 1 , wherein

a first pipe supplies the temperature-regulated gas to the molybdenum trioxide 100 powder sample, and a second pipe supplies the molybdenum trioxide 99 and the technetium oxide 99m to a separation/purification unit for separating and purifying the technetium oxide 99m, and

a mesh filter having a mesh opening size smaller than a particle size of the molybdenum trioxide 100 powder sample, and which permits passage of the temperature-regulated gas is located between the first pipe and the molybdenum trioxide 100 powder sample and is located in the second pipe.

10. The method according to claim 1 , wherein

a thickness of the molybdenum trioxide 100 powder sample along an emission direction of the electron beam is greater than or equal to a beam path length of the electron beam in the molybdenum trioxide 100 powder sample.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 10, 2015
From: TADOKORO, TAKAHIRO; KANI, YUKO
To: HITACHI, LTD.
Reel/Frame 036054/0185 →
Priority Claims (1)
JP 2014-151342 · Jul 25, 2014 · national
Continuity (1)
Related Publication 20160023182A1 · Jan 28, 2016