IP Library Granted Patent US 9,949,979
Granted Patent B2
US 9,949,979 · App. 14/365,512 · Granted Apr 24, 2018

Use of inhibitors of the activity or function of PI3K

Inventors: Nigel Graham Cooke (Oberwil, CH); Paulo Antonio Fernandes Gomes Dos Santos (Basel, CH); Pascal Furet (Thann, FR); Christina Hebach (Muenchenstein, CH); Klemens Hoegenauer (Oberwil, CH); Gregory Hollingworth (Kent, GB); Christoph Kalis (Gundelfingen, DE); Ian Lewis (Riehen, CH); Alexander Baxter Smith (Niffer, FR); Nicolas Soldermann (Village-Neuf, FR); Frederic Stauffer (Hesingue, FR); Ross Strang (Hagenthal le Bas, FR); Frank Stowasser (Murg, DE); Nicola Tuffilli (Moehlin, CH); Anette Von Matt (Biel-Benken, CH); Romain Wolf (Schlierbach, FR); Frederic Zecri (Brookline, MA)
Assignee: Novartis AG
A61K31/519A61K31/517A61K31/5377A61K31/541A61K31/551C07D239/74C07D401/04C07D401/14C07D403/04C07D413/14C07D487/08
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Quick Facts
Patent No.
US 9,949,979
App. No.
14/365,512
Granted
Apr 24, 2018
Kind
B2
Abstract

The invention relates to new uses of PI3K inhibitors, wherein said inhibitors have an inhibitory action on the PI3K isoform delta for the treatment of immunopathology in a subject suffering from a disease or disorder selected from malaria, leishmaniasis, trypanosomiasis, toxoplasmosis and/or neurocysticercosis, via functional inhibition of TLR9 of the infected subject.

Claims (37)

1. A method of treating a host-mediated immunopathology caused by acute or cerebral malaria in a subject suffering from acute or cerebral malaria, the method comprising the step of administering to the subject a PI3K inhibitor, wherein said PI3K inhibitor has an inhibitory action on the host PI3K isoform delta, wherein inhibition of host PI3K isoform delta causes a reduction of the host immune response to the acute or cerebral malaria, and wherein the PI3K inhibitor is a compound of formula (I) or a tautomer and/or N-oxide and/or pharmaceutically acceptable salt or solvate thereof:

wherein

Y is selected from O and NR 3 ;

R 1 is —C(O)—R 4 ;

R 4 is selected from C 1 -C 8 -alkyl, halo-C 1 -C 8 -alkyl, hydroxy-C 1 -C 8 -alkyl, C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl, C 1 -C 8 -alkyl-sulfonyl-C 1 -C 8 -alkyl, heterocyclyl, heterocyclyl-oxy, heterocyclyl-C 1 -C 8 -alkyl, C 3 -C 12 -cycloalkyl, C 3 -C 12 -cycloalkyl-C 1 -C 8 -alkyl, heteroaryl, heteroaryl-oxy, heteroaryl-C 1 -C 8 -alkyl, hydroxy, C 1 -C 8 -alkoxy, amino, N—C 1 -C 8 -alkyl-amino, and N,N-di-C 1 -C 8 -alkyl-amino,

wherein ‘C 1 -C 8 -alkyl’ in N—C 1 -C 8 -alkyl-amino and N,N-di-C 1 -C 8 -alkyl-amino may be unsubstituted or substituted by halogen, hydroxyl, or C 1 -C 4 -alkoxy;

wherein ‘C 3 -C 12 -cycloalkyl’ in C 3 -C 12 -cycloalkyl and C 3 -C 12 -cycloalkyl-C 1 -C 8 -alkyl may be unsubstituted or substituted by 1-5 substituents independently selected from oxo, halogen, C 1 -C 8 -alkyl, halo-C 1 -C 8 -alkyl, hydroxy-C 1 -C 8 -alkyl, hydroxyl, C 1 -C 8 -alkoxy, C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl, amino, N—C 1 -C 8 -alkyl-amino, N,N-di-C 1 -C 8 -alkyl-amino, C 1 -C 8 -alkyl-carbonyl, halo-C 1 -C 8 -alkyl-carbonyl, hydroxy-C 1 -C 8 -alkyl-carbonyl, and C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl-carbonyl;

wherein ‘heterocyclyl’ is selected from oxiranyl, aziridinyl, oxetanyl, thiethanyl, acetitinyl, pyrrolidinyl, tetrahydrofuranyl, tetrahydrothiophenyl, 2,3-dihydrofuranyl, 2,5-dihydrofuranyl, 2,3-dihydrothiophenyl, 1-pyrrolinyl, 2-pyrrolinyl, 3-pyrrolinyl, tetrahydropyranyl, piperidinyl, tetrahydrothiopyranyl, morpholinyl, thiomorpholinyl, piperazinyl, azepanyl, thiepanyl, and oxepanyl; each of which is unsubstituted or substituted by 1-5 substituents independently selected from oxo, halogen, C 1 -C 8 -alkyl, halo-C 1 -C 8 -alkyl, hydroxy-C 1 -C 8 -alkyl, hydroxyl, C 1 -C 8 -alkoxy, C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl, amino, N—C 1 -C 8 -alkyl-amino, N,N-di-C 1 -C 8 -alkyl-amino, C 1 -C 8 -alkyl-carbonyl, halo-C 1 -C 8 -alkyl-carbonyl, hydroxy-C 1 -C 8 -alkyl-carbonyl, and C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl-carbonyl;

wherein ‘heterocyclyl’ can be attached at a heteroatom or a carbon atom and wherein the N and/or S heteroatoms can also optionally be oxidized to various oxidation states; and

wherein ‘heteroaryl’ is selected from furanyl, thiophenyl, pyrrolyl, imidazolyl, pyrazolyl, thiazolyl, isothiazolyl, oxazolyl, isoxazolyl, 1,2,5-oxadiazolyl, 1,2,4-oxadiazolyl, 1,2,3-oxadiazolyl,1,3,4-oxadiazolyl, 1,2,5-thiadiazolyl, 1,2,4-thiadiazolyl, 1,2,3-thiadiazolyl, 1,3,4-thiadiazolyl, 1,2,3-triazolyl, 1,2,4-triazolyl, 1,2,5-triazolyl, pyridyl, pyrimidinyl, pyrazinyl, pyridazinyl, 1,2,3-triazinyl, 1,2,4-triazinyl, and 1,3,5-triazinyl; each of which is unsubstituted or substituted by 1-5 substituents independently selected from halogen, C 1 -C 8 -alkyl, halo-C 1 -C 8 -alkyl, hydroxy-C 1 -C 8 -alkyl, hydroxyl, C 1 -C 8 -alkoxy, C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl, amino, N—C 1 -C 8 -alkyl-amino, N,N-di-C 1 -C 8 -alkyl-amino, C 1 -C 8 -alkyl-carbonyl, halo-C 1 -C 8 -alkyl-carbonyl, hydroxy-C 1 -C 8 -alkyl-carbonyl, and C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl-carbonyl; wherein ‘heteroaryl’ can be attached at a heteroatom or a carbon atom and wherein the N and/or S heteroatoms can also optionally be oxidized to various oxidation states;

R 2 is selected from phenyl, naphthyl, pyridyl, pyrimidinyl, pyrazinyl, pyridazinyl, quinoliny, and isoquinolinyl, each of which is unsubstituted or substituted by 1-5 substituents independently selected from halogen, cyano, nitro, C 1 -C 8 -alkyl, halo-C 1 -C 8 -alkyl, hydroxy-C 1 -C 8 -alkyl, hydroxyl, C 1 -C 8 -alkoxy, C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl, amino, N—C 1 -C 8 -alkyl-amino, N,N-di-C 1 -C 8 -alkyl-amino, C 1 -C 8 -alkyl-carbonyl, halo-C 1 -C 8 -alkyl-carbonyl, hydroxy-C 1 -C 8 -alkyl-carbonyl, and C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl-carbonyl;

R 3 is selected from H, C 1 -C 4 -alkyl, and halo-C 1 -C 4 -alkyl; and

m is selected from 0 and 1.

2. The method of claim 1 , wherein the PI3K inhibitor is a compound of formula (Id′)

and/or tautomers and/or N-oxides and/or pharmaceutically acceptable salts thereof.

3. The method of claim 1 , wherein the PI3K inhibitor is a compound of formula (Ie′)

and/or tautomers and/or N-oxides and/or pharmaceutically acceptable salts thereof.

4. The method of claim 1 , wherein the PI3K inhibitor is a compound in which

R 2 is selected from naphthyl, pyridyl, and pyrimidinyl; each of which is unsubstituted or substituted by 1-3 substituents independently selected from halogen, cyano, nitro, C 1 -C 8 -alkyl, halo-C 1 -C 8 -alkyl, hydroxy-C 1 -C 8 -alkyl, hydroxyl, C 1 -C 8 -alkoxy, C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl, amino, N—C 1 -C 8 -alkyl-amino, N,N-di-C 1 -C 8 -alkyl-amino, C 1 -C 8 -alkyl-carbonyl, halo-C 1 -C 8 -alkyl-carbonyl, hydroxy-C 1 -C 8 -alkyl-carbonyl, and C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl-carbonyl.

5. The method of claim 1 , wherein the PI3K inhibitor is a compound in which

R 1 is —C(O)—R 4 , and

R 4 is selected from heterocyclyl, C 4 -C 8 -cycloalkyl or heteroaryl;

wherein ‘C 3 -C 12 -cycloalkyl’ may be unsubstituted or substituted by 1-3 substituents independently selected from fluoro, C 1 -C 4 -alkyl, hydroxyl, and C 1 -C 4 -alkoxy;

wherein ‘heterocyclyl’ is selected from pyrrolidinyl, tetrahydropyranyl, piperidinyl, tetrahydrothiopyranyl, morpholinyl, and piperazinyl; each of which is unsubstituted or substituted by 1-3substituents independently selected from oxo, halogen, C 1 -C 4 -alkyl, hydroxyl, and C 1 -C 4 -alkyl-carbonyl;

wherein ‘heterocyclyl’ can be attached at a heteroatom or a carbon atom and wherein the N and/or S heteroatoms can also optionally be oxidized to various oxidation states;

wherein ‘heteroaryl’ is selected from furanyl, imidazolyl, pyrazolyl, thiazolyl, oxazolyl, isoxazolyl, 1,3,4-oxadiazolyl, pyridyl, and pyrazinyl; each of which is unsubstituted or substituted by 1-3 substituents independently selected from C 1 -C 4 -alkyl,and hydroxyl; and

wherein ‘heteroaryl’ can be attached at a heteroatom or a carbon atom and wherein the N and/or S heteroatoms can also optionally be oxidized to various oxidation states.

6. The method of claim 1 , wherein the PI3K inhibitor is a compound in which

R 1 is —C(O)—R 4 , and

R 4 is selected from C 1 -C 8 -alkyl, C 1 -C 8 -alkoxy-C 1 -C 8 -alkyl, C 1 -C 8 -alkoxy, and N,N-di-C 1 -C 8 -alkyl-amino, wherein ‘C 1 -C 8 -alkyl’ in N,N-di-C 1 -C 8 -alkyl-amino may be unsubstituted or substituted by halogen, hydroxyl, or C 1 -C 4 -alkoxy.

7. The method of claim 1 , wherein the PI3K inhibitor is selected from the group consisting of

{(S)-3-[6-(6-Methoxy-5-methyl-pyridin-3-yl)-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-yloxy]-pyrrolidin-1-yl}-(tetrahydro-pyran-4-yl)-methanone;

{3-[6-(6-Methoxy-5-methyl-pyridin-3-yl)-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-yloxy]-pyrrolidin-1-yl}-(tetrahydro-pyran-4-yl)-methanone;

(S)-1-(3-(6-(6-Methoxy-5-(trifluoromethyl)pyridin-3-yl)-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidin-4-ylamino)pyrrolidin-1-yl)propan-1-one; and

1-(3-(6-(6-Methoxy-5-(trifluoromethyl)pyridin-3-yl)-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidin-4-ylamino)pyrrolidin-1-yl)propan-1-one.

8. The method of claim 1 , wherein the PI3K inhibitor is a pharmaceutically acceptable salt selected from citrate, fumarate, napadisylate, phosphate, hydrochloride, and hippurate.

9. The method of claim 1 , wherein the subject is a human.

Assignments (21)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: COOKE, NIGEL GRAHAM
To: NOVARTIS PHARMA AG
Reel/Frame 038265/0983 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: FERNANDES GOMES DOS SANTOS, PAULO ANTONIO
To: NOVARTIS PHARMA AG
Reel/Frame 038266/0047 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: FURET, PASCAL
To: NOVARTIS PHARMA AG
Reel/Frame 038266/0114 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: HEBACH, CHRISTINA
To: NOVARTIS PHARMA AG
Reel/Frame 038266/0181 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: HOGENAUER, KLEMENS
To: NOVARTIS PHARMA AG
Reel/Frame 038266/0274 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: HOLLINGWORTH, GREGORY
To: NOVARTIS PHARMACEUTICALS UK LIMITED
Reel/Frame 038266/0333 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: KALIS, CHRISTOPH
To: NOVARTIS PHARMA AG
Reel/Frame 038266/0377 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: LEWIS, IAN
To: NOVARTIS PHARMA AG
Reel/Frame 038267/0158 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: SMITH, ALEXANDER BAXTER
To: NOVARTIS PHARMA AG
Reel/Frame 038267/0323 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: SOLDERMANN, NICOLAS
To: NOVARTIS PHARMA AG
Reel/Frame 038267/0455 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: STAUFFER, FREDERIC
To: NOVARTIS PHARMA AG
Reel/Frame 038268/0874 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: STRANG, ROSS
To: NOVARTIS PHARMA AG
Reel/Frame 038269/0534 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: STOWASSER, FRANK
To: NOVARTIS PHARMA STEIN AG
Reel/Frame 038269/0909 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: TUFILLI, NICOLA
To: NOVARTIS PHARMA AG
Reel/Frame 038270/0062 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: VON MATT, ANETTE
To: NOVARTIS PHARMA AG
Reel/Frame 038270/0182 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: WOLF, ROMAIN
To: NOVARTIS PHARMA AG
Reel/Frame 038270/0248 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: ZECRI, FREDERIC
To: NOVARTIS INSTITUTES FOR BIOMEDICAL RESEARCH INC.
Reel/Frame 038270/0367 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: NOVARTIS PHARMA AG
To: NOVARTIS AG
Reel/Frame 038270/0533 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: NOVARTIS INSTITUTES FOR BIOMEDICAL RESEARCH INC.
To: NOVARTIS AG
Reel/Frame 038271/0384 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: NOVARTIS PHARMACEUTICALS UK LIMITED
To: NOVARTIS AG
Reel/Frame 038272/0281 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2016
From: NOVARTIS PHARMA STEIN AG
To: NOVARTIS AG
Reel/Frame 038272/0318 →
Continuity (2)
Provisional Application 61576194 · Dec 15, 2011
Related Publication 20150342951A1 · Dec 3, 2015