IP Library Granted Patent US 9,974,720
Granted Patent B2
US 9,974,720 · App. 15/381,145 · Granted May 22, 2018

Compositions containing microcapsules coated with deposition proteins

Inventors: Takashi Sasaki (Matawan, NJ); Johan G. L. Pluyter (Middletown, NJ)
Assignee: INTERNATIONAL FLAVORS & FRAGRANCES INC.
A61K8/11A61K8/645A61K8/8152A61K8/84A61Q5/02C11D3/3726C11D3/505C11D17/0039C12P21/00A61K2800/56
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Quick Facts
Patent No.
US 9,974,720
App. No.
15/381,145
Granted
May 22, 2018
Kind
B2
Abstract

A microcapsule composition containing microcapsules coated with a deposition protein, e.g., a protein-silanol copolymer, a protein-silane copolymer, a protein-siloxane copolymer, or a cationically modified protein, is provided as is a method for making the microcapsule composition and using the microcapsule composition in consumer products, in particular rinse-off consumer product.

Claims (19)

1. A method for preparing a microcapsule composition comprising:

(a) providing a microcapsule slurry having a plurality of microcapsules each containing a polymeric wall and an active material encapsulated within the polymeric wall;

(b) curing the microcapsules; and

(c) coating each of the microcapsules with a deposition protein,

wherein the deposition protein is cross-linked on the surface of the microcapsules (i) at a temperature between 35 to 75° C. after curing the microcapsules or (ii) by adding an alkoxysilane after step (b); and the active material contains a fragrance, pro-fragrance, flavor, malodor counteractive agent, anti-inflammatory agent, anesthetic, analgesic, anti-viral agent, anti-infectious agent, anti-acne agent, skin lightening agent, insect repellant, emollient, skin moisturizing agent, vitamin or derivative thereof, or any combination thereof.

2. The method of claim 1 , wherein the microcapsules are coated with the deposition protein at a temperature between 35 to 75° C.

3. The method of claim 1 , further comprising step (d) adding a second deposition aid after step (b).

4. The method of claim 1 , wherein the deposition protein is a cationically modified protein.

5. The method of claim 4 , wherein the cationically modified protein is a protein-acrylate copolymer having a nitrogen-containing acrylic moiety.

6. The method of claim 5 , wherein the nitrogen-containing acrylic moiety comprises a tertiary or quaternary amine group.

7. The method of claim 1 , wherein the deposition protein is cross-linked on the surface of the microcapsules using the alkoxysilane.

8. The method of claim 1 , wherein the plurality of microcapsules are prepared by cross-linking a polyisocyanate with an activation agent selected from the group consisting of an amine cross-linker, an alcohol cross-linker, an epoxy cross-linker, an acrylate cross-linker, a hybrid cross-linker, and a combination thereof.

9. The method of claim 1 , wherein the deposition protein is a modified vegetable protein, wheat protein, marine collagen protein, keratin protein, silk protein, or milk protein.

10. The method of claim 1 , wherein the deposition protein has a molecular weight in the range of 1000 to 500,000.

11. The method of claim 1 , wherein the microcapsule composition comprising a second deposition aid selected from the group consisting of anionically, cationically, nonionically, or amphoteric water-soluble polymers.

12. A microcapsule composition prepared by the method of claim 1 .

13. A consumer product comprising the microcapsule composition of claim 12 .

14. The consumer product of claim 13 , further comprising one or more different microcapsules, free active material, or a combination thereof.

15. The consumer product of claim 13 , wherein the consumer product is a shampoo, hair conditioner, body wash, detergent, softener, bar soap, scent booster, or hard surface cleaner.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 16, 2016
From: SASAKI, TAKASHI; PLUYTER, JOHAN G. L.
To: INTERNATIONAL FLAVORS AND FRAGRANCES INC.
Reel/Frame 040639/0374 →
Continuity (2)
Provisional Application 62272743 · Dec 30, 2015
Related Publication 20170189283A1 · Jul 6, 2017