IP Library Granted Patent US 10,018,540
Granted Patent B2
US 10,018,540 · App. 15/277,118 · Granted Jul 10, 2018

Clearing agent and mounting media for microscopy

Inventors: James E. Simon (Princeton, NJ); Thomas Villani (New Brunswick, NJ); Adolfina Koroch (Highland Park, NJ)
Assignee: RUTGERS, THE STATE UNIVERSITY OF NEW JERSEY
G01N1/30G01N2001/307
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Quick Facts
Patent No.
US 10,018,540
App. No.
15/277,118
Granted
Jul 10, 2018
Kind
B2
Abstract

A clearing agent and mounting solution for microscopy is disclosed comprising at least trichloroethanol and/or derivatives thereof, where the refractive index of the solution is greater than or equal to about 1.3810. Also disclosed are methods of preparing specimens for microscopy.

Claims (58)

1. A clearing agent and mounting solution, comprising:

5% to 97% (v/v) trichloroethanol or derivative thereof;

16.5% to 36% (v/v) benzyl alcohol; and

12.5% to 50% glycerol, polyethylene glycol (PEG), propylene glycol (PG), ethylene glycol (EG), and/or derivatives thereof; and optionally water.

2. The clearing agent and mounting solution of claim 1 , comprising:

36% (v/v) of trichloroethanol or derivative thereof;

36% (v/v) benzyl alcohol; and

27% (v/v) glycerol.

3. The clearing agent and mounting solution of claim 1 , comprising:

33% (v/v) of trichloroethanol or derivative thereof;

33% (v/v) benzyl alcohol; and

33% (v/v) glycerol.

4. The clearing agent and mounting solution of claim 1 , comprising:

33% (v/v) trichloroethanol or derivative thereof;

33% (v/v) benzyl alcohol; and

17% (v/v) glycerol; and further comprising:

17% (v/v) benzyl benzoate.

5. The clearing agent and mounting solution of claim 1 , comprising:

29% (v/v) trichloroethanol or derivative thereof;

29% (v/v) benzyl alcohol; and

17% (v/v) glycerol; and further comprising:

13% (v/v) benzyl benzoate; and

13% (v/v) benzyl ether.

6. The clearing agent and mounting solution of claim 1 , comprising:

42% (v/v) trichloroethanol or derivative thereof;

16.5% (v/v) benzyl alcohol; and

16.5% (v/v) glycerol; and further comprising:

25% (v/v) benzyl ether.

7. The clearing agent and mounting solution of claim 1 , comprising:

36% (v/v) of trichloroethanol or derivative thereof;

36% (v/v) benzyl alcohol; and

27% (v/v) PEG, PG, EG, and/or derivatives thereof.

8. The clearing agent and mounting solution of claim 1 , comprising:

33% (v/v) of trichloroethanol or derivative thereof;

33% (v/v) benzyl alcohol; and

33% (v/v) PEG, PG, EG, and/or derivatives thereof.

9. The clearing agent and mounting solution of claim 1 , comprising:

33% (v/v) of trichloroethanol or derivative thereof;

33% (v/v) benzyl alcohol; and

17% (v/v) PEG, PG, EG, and/or derivatives thereof; and further comprising:

17% (v/v) benzyl benzoate.

10. The clearing agent and mounting solution of claim 1 , comprising:

29% (v/v) of trichloroethanol or derivative thereof;

29% (v/v) benzyl alcohol; and

17% (v/v) PEG, PG, EG, and/or derivatives thereof; and further comprising:

13% (v/v) benzyl benzoate; and

13% (v/v) benzyl ether.

11. The clearing agent and mounting solution of claim 1 , comprising:

42% (v/v) trichloroethanol or derivative thereof;

16.5% (v/v) benzyl alcohol; and

16.5% (v/v) PEG, PG, EG, and/or derivatives thereof; and further comprising:

25% (v/v) benzyl ether.

12. The clearing agent and mounting solution of claim 1 , wherein the trichloroethanol derivative comprises mono- or poly-halogenated branched or unbranched alcohols, diols, glycols, aldehydes, aldehyde-hydrates, hemi-acetals, acetals, ketals, aminals, and hemi-aminals of at least 2 carbon units, wherein branches are defined as any mono- or poly-halogenated aliphatic or aromatic side chains containing hydroxyl, amino, ether, carboxyl, carboxyamido, carbonate, carbamyl, carbonyl-chloride, polyethylene glycol, or aminoethanol groups, and a polymer thereof.

13. The clearing agent and mounting solution of claim 1 , further comprising C1-C6 alcohol.

14. The clearing agent and mounting solution of claim 1 , further comprising a solidification aid comprising polyethylene glycol, polyamide resin, polyvinylpyrrolidone, polyvinyl alcohol, or mixtures thereof.

15. A clearing agent and mounting solution, comprising:

5% to 90% (v/v) trichloroethanol or derivative thereof; and

5% to 90% (v/v) benzyl alcohol.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 30, 2017
From: SIMON, JAMES E.; VILLANI, THOMAS; KOROCH, ADOLFINA
To: RUTGERS, THE STATE UNIVERSITY OF NEW JERSEY
Reel/Frame 041555/0149 →
Continuity (5)
Continuation In Part 15258474 · Sep 7, 2016
Continuation In Part 14391106 · Oct 7, 2014
Continuation 14391106
Provisional Application 61622210 · Apr 10, 2012
Related Publication 20170016808A1 · Jan 19, 2017