IP Library Granted Patent US 10,096,410
Granted Patent B2
US 10,096,410 · App. 14/889,069 · Granted Oct 9, 2018

R-T-B based sintered magnet

Inventors: Masashi Miwa (Tokyo, JP); Haruna Nakajima (Tokyo, JP); Koji Mitake (Tokyo, JP); Chikara Ishizaka (Tokyo, JP)
Assignee: TDK CORPORATION
H01F1/01H01F1/0577H02K1/02H02K1/278
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Quick Facts
Patent No.
US 10,096,410
App. No.
14/889,069
Granted
Oct 9, 2018
Kind
B2
Abstract

An R-T-B based sintered magnet having R 2 T 14 B crystal grains and a grain boundary formed by two or more adjacent R 2 T 14 B crystal grains. An R—Co—Cu—N concentrated part whose concentrations of R, Co, Cu and N are respectively higher than those in the R 2 T 14 B crystal grains may be in the grain boundary. An R—O—C concentrated part or an R—O—C—N concentrated part may be further provided in the grain boundary.

Claims (26)

1. An R-T-B based sintered magnet comprising:

a plurality of R 2 T 14 B crystal grains;

at least one grain boundary formed by two or more adjacent R 2 T 14 B crystal grains; and

an R—Co—Cu—N concentrated part in the at least one grain boundary,

wherein concentrations of R, Co, Cu and N in the R—Co—Cu—N concentrated part are respectively higher than concentrations of R, Co, Cu and N in the plurality of R 2 T 14 B crystal grains, and

a ratio of atom number composition of N to a total atom number composition in the R—Co—Cu—N concentrated part is in the range of 10% to 15%.

2. The R-T-B based sintered magnet as set forth in claim 1 , further comprising an R—O—C concentrated part in the at least one grain boundary,

wherein concentrations of R, O and C in the R—O—C concentrated part are respectively higher than concentrations of R, O and C in the plurality of R 2 T 14 B crystal grains.

3. The R-T-B based sintered magnet as set forth in claim 2 , wherein the R—O—C concentrated part is formed within a boundary defined by the R—Co—Cu—N concentrated part in the grain boundary.

4. The R-T-B based sintered magnet as set forth in claim 1 , further comprising an R—O—C—N concentrated part in the at least one grain boundary,

wherein concentrations of R, O, C and N in the R—O—C—N concentrated part are respectively higher than concentrations of R, O, C and N in the plurality of R 2 T 14 B crystal grains.

5. The R-T-B based sintered magnet as set forth in claim 4 , wherein the R—O—C—N concentrated part is formed within a boundary defined by the R—Co—Cu—N concentrated part in the grain boundary.

6. The R-T-B based sintered magnet as set forth in claim 1 , wherein the at least one grain boundary is formed by two adjacent R 2 T 14 B crystal grains.

7. The R-T-B based sintered magnet as set forth in claim 1 , wherein the at least one grain boundary is formed by three adjacent R 2 T 14 B crystal grains.

8. The R-T-B based sintered magnet as set forth in claim 1 , wherein the plurality of R 2 T 14 B crystal grains have a tetragonal crystal structure.

9. The R-T-B based sintered magnet as set forth in claim 1 , wherein the plurality of R 2 T 14 B crystal grains have an average crystal diameter in the range of 1 μm to 30 μm.

10. The R-T-B based sintered magnet as set forth in claim 1 , wherein a ratio of an atom number composition of R to the total atom number composition in the R—Co—Cu—N concentrated part is in the range of 60% to 65%.

11. The R-T-B based sintered magnet as set forth in claim 1 , wherein a ratio of atom number composition of Co to the total atom number composition in the R—Co—Cu—N concentrated part is in the range of 10% to 14%.

12. The R-T-B based sintered magnet as set forth in claim 1 , wherein a ratio of atom number composition of Cu to the total atom number composition in the R—Co—Cu—N concentrated part is in the range of 4% to 7%.

13. The R-T-B based sintered magnet as set forth in claim 2 , wherein the R—O—C concentrated part has a cubic crystal structure.

14. The R-T-B based sintered magnet as set forth in claim 2 , wherein a ratio of an atom number of O to an atom number of R in the R—O—C concentrated part is in the range of less than 1.

15. The R-T-B based sintered magnet as set forth in claim 14 , wherein the ratio of the atom number of O to the atom number of R in the R—O—C concentrated part is in the range of 0.5 to 0.7.

16. The R-T-B based sintered magnet as set forth in claim 1 , wherein the content of R in the plurality of R 2 T 14 B crystal grains is in the range of 25 mass % to 35 mass %.

17. The R-T-B based sintered magnet as set forth in claim 1 , wherein the content of B in the plurality of R 2 T 14 B crystal grains is in the range of 0.5 mass % to 1.5 mass %.

18. The R-T-B based sintered magnet as set forth in claim 1 , wherein T comprises Fe and Co and the content of Co in the plurality of R 2 T 14 B crystal grains is in the range of 0.3 mass % to 4.0 mass %.

19. An electric motor having a rotor comprising a permanent magnet, wherein the permanent magnet includes the R-T-B based sintered magnet as set forth in claim 1 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 4, 2015
From: MIWA, MASASHI; NAKAJIMA, HARUNA; MITAKE, KOJI; ISHIZAKA, CHIKARA
To: TDK CORPORATION
Reel/Frame 036961/0142 →
Priority Claims (1)
JP 2013-139857 · Jul 3, 2013 · national
Continuity (1)
Related Publication 20160086701A1 · Mar 24, 2016