IP Library Granted Patent US 10,099,254
Granted Patent B2
US 10,099,254 · App. 12/532,909 · Granted Oct 16, 2018

Classification method of particulate water absorbent resin

Inventors: Kazumasa Konishi (Himeji, JP); Kenji Kadonaga (Kakogawa, JP); Yorimichi Dairoku (Setouchi, JP); Shinichi Fujino (Himeji, JP)
Assignee: NIPPON SHOKUBAI CO., LTD.
B07B9/00C08J3/12C08J3/122C08J2300/00
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Quick Facts
Patent No.
US 10,099,254
App. No.
12/532,909
Granted
Oct 16, 2018
Kind
B2
Abstract

A particulate water absorbent resin is obtained by polymerizing an unsaturated monomer so as to form a cross-linked polymer hydrogel and drying and pulverizing the cross-linked polymer hydrogel, and plural classification steps different from each other are carried out so as to remove fine powder. In this manner, the present invention provides the method for classification of particulate water absorbent resin which method allows particulate water absorbent resin having a desired particle diameter range to be efficiently obtained at low cost while securing the high productivity even in case where a larger production equipment is used.

Claims (19)

1. A method for classification of particulate water absorbent resin obtained by polymerizing an unsaturated monomer so as to form a cross-linked polymer hydrogel and drying and pulverizing the cross-linked polymer hydrogel,

said method comprising:

a first classification step in which a first screen and a gravity are used; and

a second classification step in which a second screen device and an aerial current are used,

the first classification step and the second classification step being carried out continuously,

the first and the second classification steps being different from each other so as to remove fine powder,

the first classification step being carried out by using a sieving device at a temperature ranging from 30° C. to 100° C., and

the particulate water absorbent resin, having been classified by the first classification step and having passed through the first screen, being further classified by the second classification step and passing through the second screen so as to remove fine powder,

whereby an amount of particulate water absorbent resin classified in second classification step is smaller than that in the first classification step; and

wherein the sieving device used in the first classification step and the second screen device used in the second classification step differ from each other

wherein a mesh size of the first screen is 150 μm or more and 300 μm or less, and

wherein a mesh size of the second screen is 106 μm or more and 180 μm or less

the sieving device is used at a temperature which is lower than a temperature of the particulate water absorbent resin so that the temperature difference therebetween is within 20° C. and

wherein, in the first classification step, a differential pressure equal to or more than 10 mm H 2 O is provided between an area where the particulate water absorbent resin has not passed through the screen and an area where the particulate water absorbent resin has passed through the screen so as to remove fine powder.

2. The method as set forth in claim 1 , wherein the plural classification steps are applied to a line for continuously producing particulate water absorbent resin so that a production amount is 500 kg/hr or more for each line.

3. The method as set forth in claim 1 , wherein a pneumatic classifier having the second screen is used in the second classification step.

4. The method as set forth in claim 1 , wherein a difference between the mesh size of the first screen and the mesh size of the second screen is 30 μm or more and 200 μm or less.

5. The method as set forth in claim 1 , wherein particles whose particle diameter is less than 180 μm are classified from the particulate water absorbent resin in the first classification step, and particles whose particle diameter is 106 μm or more are classified from the particles whose particle diameter is less than 180 μm in the second classification step.

6. The method as set forth in claim 1 , wherein particles whose particle diameter is less than 180 μm are classified from the particulate water absorbent resin in the first classification step, and particles whose particle diameter is 150 μm or more are classified from the particles whose particle diameter is less than 180 μm in the second classification step.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 24, 2009
From: KONISHI, KAZUMASA; KADONAGA, KENJI; DAIROKU, YORIMICHI; FUJINO, SHINICHI
To: NIPPON SHOKUBAI CO., LTD.
Reel/Frame 023279/0010 →
Priority Claims (1)
JP 2007-080052 · Mar 26, 2007 · national
Continuity (1)
Related Publication 20100101982A1 · Apr 29, 2010