IP Library Granted Patent US 10,101,210
Granted Patent B2
US 10,101,210 · App. 15/359,759 · Granted Oct 16, 2018

Portable analyzer and method for determining a composition of a sample

Inventor: Tuomas Pylkkanen (Helsinki, FI)
Assignee: Hitachi High-Tech Analytical Science Limited
G01J3/443G01J3/0208G01J3/0272G01J3/10G01J3/45
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Quick Facts
Patent No.
US 10,101,210
App. No.
15/359,759
Granted
Oct 16, 2018
Kind
B2
Abstract

A portable analyzer determines composition of a sample and includes excitation means for invoking an optical emission from a surface of the sample, detector means for observing a selectable wavelength in said optical emission and for recording a detection signal that is descriptive of at least one characteristic of said optical emission at a selected wavelength, analysis means for determination of elemental composition of the sample on basis of one or more detection signals; and control means for carrying out a spectral analysis by operating the excitation means to generate the optical emission for recording respective detection signals at predefined wavelengths, operating the detector means to record the respective one or more detection signals at said one or more predefined wavelengths, and operating the analysis means to determine elemental composition of the sample on basis of said recorded detection signals.

Claims (25)

1. A portable analyzer for determining composition of a sample, the portable analyzer comprising:

a laser source arranged to generate a series of laser pulses for invoking an optical emission from a surface of the sample;

an adjustable Fabry-Pérot interferometer for observing a selectable wavelength in said optical emission and for recording one or more detection signals that are descriptive of at least one characteristic of said optical emission at a selected wavelength;

a processor and a memory including computer program code, which when executed by the processor causes the portable analyzer to implement a determination of elemental composition of the sample; and

a controller for carrying out a spectral analysis for the determination of elemental composition,

wherein the controller is arranged to carry out the spectral analysis by scanning over a predefined sequence of two or more wavelengths to record respective one or more detection signals at each wavelength of said sequence and analyzing to determine elemental composition of the sample, the spectral analysis being based on the one or more detection signals from the Fabry-Pérot interferometer, said scanning comprising,

selecting a wavelength of said sequence and adjusting the Fabry-Pérot interferometer to observe said selected wavelength,

operating the laser source to generate a respective sub-series of laser pulses for invoking the optical emission for recording respective one or more detection signals at said selected wavelength, and

operating the Fabry-Pérot interferometer to record the respective one or more detection signals at said selected wavelength based on the optical emission invoked by the respective sub-series of laser pulses.

2. A portable analyzer according to claim 1 , wherein the Fabry-Pérot interferometer is adjustable to observe said selected wavelength within a first range defined by a predefined minimum wavelength and a predefined maximum wavelength.

3. A portable analyzer according to claim 1 , wherein said selected wavelength denotes the center point of a predefined second range of wavelengths, which second range is substantially narrower than the first range.

4. A portable analyzer according to claim 1 , wherein the Fabry-Pérot interferometer is adjustable to observe one of two or more predefined wavelengths.

5. A portable analyzer according to claim 1 , wherein the Fabry-Pérot interferometer comprises a pair of optical flats arranged in parallel or substantially in parallel to each other and separated from each other by an adjustable air gap, and wherein the selectable wavelength observed by the Fabry-Pérot interferometer is selectable by adjusting the width of said adjustable air gap.

6. A portable analyzer according to claim 1 , wherein each sub-series consists of a predefined number of laser pulses.

7. A portable analyzer according to claim 1 , wherein said predefined sequence of two or more wavelengths covers wavelengths within a predefined range at predefined intervals.

8. A portable analyzer according to claim 1 , wherein said predefined sequence of two or more wavelengths consists of wavelengths that are characteristic to one or more predefined elements.

9. A portable analyzer according to claim 1 , wherein said at least one characteristic includes at least one of the following:

an indication of a presence or absence of radiation at the selected wavelength, and

an indication of a relative intensity of radiation at the selected wavelength.

10. A portable analyzer according to claim 1 , wherein the controller is arranged to display an indication of the determined elemental composition of the sample via a display means provided in the portable analyzer.

11. A method for determining a composition of a sample using a laser source arranged to generate a series of laser pulses for invoking an optical emission from a surface of the sample and an adjustable Fabry-Pérot interferometer for observing a selectable wavelength in said optical emission and for recording one or more detection signals that are descriptive of at least one characteristic of said optical emission at a selected wavelength, the method comprising:

carrying out a spectral analysis by scanning over a predefined sequence of two or more wavelengths to record respective one or more detection signals at each wavelength of said sequence and analyzing to determine elemental composition of the sample, the spectral analysis being based on the one or more detection signals from the Fabry-Pérot interferometer, wherein said scanning comprises,

selecting a wavelength of said sequence and adjusting the Fabry-Pérot interferometer to observe the selected wavelength,

operating the laser source to generate a respective sub-series of laser pulses for invoking the optical emission for recording respective one or more detection signals at said selected wavelength, and

operating the Fabry-Pérot interferometer to record the respective one or more detection signals at said selected wavelength based on the optical emission invoked by the respective sub-series of laser pulses.

Assignments (3)
CHANGE OF NAME Recorded Sep 22, 2017
From: MATERIALS ANALYSIS LIMITED
To: HITACHI HIGH-TECH ANALYTICAL SCIENCE LIMITED
Reel/Frame 043666/0861 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 10, 2017
From: OXFORD INSTRUMENTS INDUSTRIAL PRODUCTS LTD.
To: MATERIALS ANALYSIS LIMITED
Reel/Frame 042951/0022 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 23, 2016
From: PYLKKANEN, TUOMAS
To: OXFORD INSTRUMENTS INDUSTRIAL PRODUCTS LTD.
Reel/Frame 040408/0273 →
Priority Claims (1)
EP 15196012 · Nov 24, 2015 · regional
Continuity (1)
Related Publication 20170146404A1 · May 25, 2017