IP Library Granted Patent US 10,113,095
Granted Patent B2
US 10,113,095 · App. 14/804,185 · Granted Oct 30, 2018

Reinforced graphitic material

Inventor: Erin Hurbi (San Francisco, CA)
Assignee: MICROSOFT TECHNOLOGY LICENSING, LLC
C09K5/14C04B35/521C04B35/524C04B38/0022C23C14/22C23C14/5806C23C16/44C23C16/56C23C18/1204C23C18/1245C23C18/1275C23C18/1291C23C18/1295F28D15/0233F28D15/0241F28F21/02G06F1/163G06F1/1656G06F1/203G06F3/011C04B2235/425C04B2235/48C04B2235/5292C04B2235/614C04B2235/616C04B2235/9607
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Quick Facts
Patent No.
US 10,113,095
App. No.
14/804,185
Granted
Oct 30, 2018
Kind
B2
Abstract

Examples are disclosed that relate to the manufacture of a reinforced graphitic material. One example provides a method for making a reinforced graphitic material including sorbing an organic compound into void space of a graphitic host material, and heating the graphitic host material to pyrolyze the sorbed organic compound. Elemental carbon is thereby deposited in the void space.

Claims (27)

1. A method for making a reinforced graphitic material, the method comprising:

sorbing a solution of an organic compound into void space between graphitic platelets of a graphitic host material;

mechanically pressing the graphitic host material while heating the graphitic host material to evaporate a solvent of the solution and deposit sorbed organic compound into the void space;

heating the graphitic host material with the sorbed organic compound to pyrolyze the sorbed organic compound and thereby deposit elemental carbon in the void space, the elemental carbon crosslinking the graphitic platelets of the graphitic host material; and

after heating the graphitic host material with the sorbed organic compound to pyrolyze the sorbed organic compound, mechanically re-pressing while heating the graphitic host material.

2. The method of claim 1 , wherein the graphitic host material includes graphene.

3. The method of claim 1 , wherein the graphitic host material includes graphene flakes 100 to 1000 micrometers in thickness.

4. The method of claim 1 , wherein the graphitic host material includes from 10 to 20% void space by volume prior to sorbing the solution of the organic compound into void space of the graphitic host material.

5. The method of claim 1 , further comprising forming the graphitic host material by one or more of chemical vapor decomposition and physical vapor deposition.

6. The method of claim 1 , wherein the organic compound includes a carbohydrate.

7. The method of claim 1 , wherein the organic compound includes a sugar.

8. The method of claim 1 , further comprising:

making the solution by dissolving the organic compound in the solvent.

9. The method of claim 1 , wherein the solvent includes water.

10. The method of claim 1 , wherein mechanically pressing the graphitic host material while heating the graphitic host material includes loading the graphitic host material up to 10,000 pounds per square inch.

11. The method of claim 10 , wherein mechanically pressing the graphitic host material while heating the graphitic host material includes heating at a temperature at which the organic compound is not pyrolyzed.

12. The method of claim 1 , wherein the solution includes a surfactant.

13. The method of claim 1 , wherein heating the graphitic host material with the sorbed organic compound includes heating under vacuum.

14. The method of claim 1 , wherein heating the graphitic host material with the sorbed organic compound includes heating under an inert atmosphere.

15. The method of claim 1 , wherein mechanically re-pressing while heating the graphitic host material comprises loading the graphitic host material up to 10,000 pounds per square inch.

16. The method of claim 1 , further comprising machining the graphitic host material with the elemental carbon deposited therein.

17. A method for making a heat spreader, the method comprising:

making a solution by dissolving an organic compound in a solvent;

sorbing the solution into void space between graphitic platelets of a graphitic host material;

mechanically pressing while heating the graphitic host material to evaporate the solvent and leave behind a sorbed residue of the organic compound in the void space;

heating the graphitic host material with the sorbed residue of the organic compound to pyrolyze the organic compound and thereby deposit elemental carbon in the void space, the elemental carbon crosslinking the graphitic platelets of the graphitic host material; and

mechanically re-pressing the graphitic host material with the elemental carbon deposited therein.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 3, 2017
From: HURBI, ERIN
To: MICROSOFT TECHNOLOGY LICENSING, LLC
Reel/Frame 044032/0037 →
Continuity (1)
Related Publication 20170022406A1 · Jan 26, 2017
Cited By (1)
US 1,124,354