IP Library Granted Patent US 10,131,752
Granted Patent B2
US 10,131,752 · App. 14/776,026 · Granted Nov 20, 2018

Polymer nanocomposites

Inventors: Allen David Clauss (Madison, WI); Brian Jeffrey Koth (Madison, WI); Guiquan Pan (Middleton, WI); Nicholas Richard Wietfeldt (Madison, WI); Matthew Clayton Hall (Madison, WI)
Assignee: RELIANCE INDUSTRIES LIMITED
C08J5/00C08J3/201C08J3/2053C08J3/215C08K3/04C08K7/24B82Y30/00C08J2363/00C08K2201/011C08K2201/014
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Quick Facts
Patent No.
US 10,131,752
App. No.
14/776,026
Granted
Nov 20, 2018
Kind
B2
Abstract

Provided herein is technology relating to polymer nanocomposites, and particularly, but not exclusively, to polymer nanocomposites comprising two or more nanomaterials and methods of producing nanocomposites comprising two or more nanomaterials.

Claims (9)

1. A method of making a polymer nanocomposite containing a solvent coexfoliated mixture of pristine nanomaterials comprising two or more distinctly different particle morphologies, said method comprising the steps of:

a) exfoliating a pristine nanomaterial by solvent exfoliation to produce a first solution or stable dispersion of a first exfoliated pristine nanomaterial;

b) exfoliating one or more additional pristine nanomaterials of different particle morphology from the first exfoliated pristine nanomaterial with the first solution or stable dispersion of the first pristine exfoliated nanomaterial to provide a second solution or stable dispersion containing a coexfoliated mixture of pristine nanomaterials in a highly exfoliated state;

c) introducing the second solution or stable dispersion into a polymer matrix; and

d) removing solvents from said matrix to provide a polymer nanocomposite;

wherein said coexfoliated mixture of pristine nanomaterials is dispersed in said polymer nanocomposite to form a nanodispersion; and wherein steps (b) and (c) are carried out by high shear mixing.

2. The method of claim 1 , wherein the coexfoliated mixture of pristine nanomaterials comprises pristine graphene nanoplatelets and pristine carbon nanotubes.

3. The method of claim 1 , wherein a ratio of the first exfoliated pristine nanomaterial to the one or more additional pristine nanomaterials is 1:60 to 60:1, inclusive.

4. The method of claim 1 , wherein said solvent is N-alkyl-pyrrolidone.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 11, 2016
From: XOLVE, INC.
To: RELIANCE INDUSTRIES LIMITED
Reel/Frame 037762/0687 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 14, 2015
From: CLAUSS, ALLEN DAVID; KOTH, BRIAN JEFFREY; PAN, GUIQUAN; WIETFELDT, NICHOLAS RICHARD; HALL, MATTHEW CLAYTON
To: XOLVE, INC.
Reel/Frame 036558/0719 →
Continuity (2)
Provisional Application 61787402 · Mar 15, 2013
Related Publication 20160032062A1 · Feb 4, 2016