IP Library › Granted Patent US 10,155,966
Granted Patent B2
US 10,155,966 · App. 15/013,366 · Granted Dec 18, 2018

Method and apparatus for conversion of cellulosic material to ethanol

Inventors: Borge Holm Christensen (Alsgarde, DK); Lena Holm Gerlach (Helsingor, DK)
Assignee: INBICON A/S
C12P7/10B01J19/245C08B1/003C08B15/00C08B37/0057C08H6/00C08H8/00C12M21/12C12M45/02C12M45/04C12M45/09C12M45/20C12P7/14C12P7/56C12P19/02C12P19/14C12P21/00C13B20/165C13K1/02D21C9/18B01J2219/00006C12P2201/00C12P2203/00Y02E50/16Y02E50/17
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Quick Facts
Patent No.
US 10,155,966
App. No.
15/013,366
Granted
Dec 18, 2018
Kind
B2
Abstract

The present invention provides an apparatus and a method for conversion of cellulosic material, such as chopped straw and corn stover, and household waste, to ethanol and other products. The cellulosic material is subjected to continuous hydrothermal pre-treatment without addition of chemicals, and a liquid and a fiber fraction are produced. The fiber fraction is subjected to enzymatic liquefaction and saccharification. The method of the present invention comprises: performing the hydrothermal pre-treatment by subjecting the cellulosic material to at least one soaking operation, and conveying the cellulosic material through at least one pressurized reactor, and subjecting the cellulosic material to at least one pressing operation, creating a fiber fraction and a liquid fraction; selecting the temperature and residence time for the hydrothermal pretreatment, so that the fibrous structure of the feedstock is maintained and at least 80% of the lignin is maintained in the fiber fraction.

Claims (24)

1. An apparatus for the treatment of cellulosic material, said apparatus comprising:

a first pressurized reactor section comprising a reactor pressure zone configured to operate at an elevated pressure;

a separation device attached to the first pressurized reactor section, wherein said separation device is configured to create a fibre fraction and a liquid fraction from the cellulosic material, wherein said separation device is a pressing device;

a discharge device capable of discharging the fibre fraction from the first pressurized reactor section to a second pressurized reactor section operable at a lower pressure than the first pressurized reactor section;

a liquid fraction unloading mechanism configured to unload the liquid fraction from the first pressurized reactor section to a closed collection zone; and

a closed collection zone configured to receive the liquid fraction from the first pressurized reactor section through the unloading mechanism.

2. The apparatus of claim 1 , wherein said liquid fraction unloading mechanism comprises a sluice device for removal of liquid following discharge after the first pressurized reactor section.

3. The apparatus of claim 1 , wherein said separation device is a screw press.

4. The apparatus of claim 1 , further comprising a cleaning device configured to clean the the cellulosic material, attached upstream of said first reactor section.

5. The apparatus of claim 1 , further comprising a soaking apparatus attached upstream of the first pressurized reactor section.

6. The apparatus of claim 5 , wherein a separation device is attached between the soaking apparatus and the first pressurized reactor section.

7. The apparatus of claim 1 , wherein the first pressurized reactor section and the second pressurized reactor section are in separate zones of a single reactor.

8. The apparatus of claim 1 , wherein the first pressurized reactor section and the second pressurized reactor section are in separate reactors.

9. The apparatus of claim 1 , further comprising a means for counter current cooling of the fibre fraction after the first pressurized reactor section.

10. The apparatus of claim 1 , further comprising an ethanol fermentation device attached downstream of the second pressurized reactor section for fermentation of the separated liquid fraction.

11. An apparatus for the treatment of lignocellulosic material, said apparatus comprising:

a first pressurized reactor section comprising a reactor pressure zone at an elevated pressure and comprising a lignocellulosic biomass;

a separation device attached to the first pressurized reactor section, wherein said separation device is configured to create a fibre fraction and a liquid fraction from the lignocellulosic material, wherein said separation device is a pressing device;

a discharge device configured to discharge the fibre fraction from the first pressurized reactor section to a second pressurized reactor section, wherein the second pressurized reactor section is at a different pressure than the first pressurized reactor section;

a liquid fraction unloading mechanism configured to unload the liquid fraction from the first pressurized reactor section to a closed collection zone; and

a closed collection zone configured to receive the liquid fraction from the first pressurized reactor section through the unloading mechanism.

12. The apparatus of claim 11 , further comprising a soaking apparatus attached upstream of the first pressurized reactor section.

13. The apparatus of claim 11 , wherein the first pressurized reactor section and the second pressurized reactor section are in separate zones of a single reactor.

14. The apparatus of claim 11 , further comprising an ethanol fermentation device attached downstream of the second pressurized reactor section for fermentation of the separated liquid fraction.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 12, 2025
From: INBICON A/S
To: NEW ENERGY BLUE LLC
Reel/Frame 070485/0337 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 9, 2024
From: INBICON A/S
To: NEW ENERGY BLUE LLC
Reel/Frame 068847/0683 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 13, 2016
From: CHRISTENSEN, BØRGE HOLM; GERLACH, LENA HOLM
To: HOLM CHRISTENSEN BIOSYSTEMER APS
Reel/Frame 040005/0936 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 13, 2016
From: HOLM CHRISTENSEN BIOSYSTEMER APS
To: INBICON A/S
Reel/Frame 040006/0068 →
Priority Claims (1)
EP 05015641 · Jul 19, 2005 · regional
Continuity (6)
Continuation 14702210 · May 1, 2015
Continuation 13753541 · Jan 30, 2013
Division 13361981 · Jan 31, 2012
Division 11989027
Provisional Application 60700323 · Jul 19, 2005
Related Publication 20160153010A1 · Jun 2, 2016