Process to extract and purify Δ
Δ 9 -THC carboxylic acid is extracted from cannabis flowers using a first organic solvent, then separated using a second aqueous solvent. Δ 9 -THC carboxylic acid is converted to Δ 9 -THC carboxylic salt before being extracted by a third organic solvent and converted back to Δ 9 -THC carboxylic acid. Using a solvent swap, Δ 9 -THC carboxylic acid is decarboxylated and extracted again with an organic solvent prior to purification to give Δ 9 -THC.
1. A method of producing delta 9 -THC consisting essentially of:
extracting delta 9 -THC carboxylic acid from cannabis flowers using heptane to obtain a heptane extract;
filtering the heptane extract to remove solid plant matter;
separating the delta 9 -THC carboxylic acid from the heptane extract by contacting the heptane extract with sodium chloride water adjusted to a pH range of 13.2 to 13.4 using an inorganic base to form a liquid mixture; stirring the liquid mixture; and leaving the liquid mixture to settle, wherein the liquid mixture forms three layers consisting of a first organic layer, a second oily layer, and third aqueous layer; and
separating out the oily layer from the other two layers to yield the delta 9 -THC.