IP Library Granted Patent US 10,246,619
Granted Patent B2
US 10,246,619 · App. 15/251,509 · Granted Apr 2, 2019

Method for increasing the reactivity of lignin

Inventors: Suvi Pietarinen (Lappeenranta, FI); Okko Ringena (Neusass, DE); Kati Eskelinen (Imatra, FI); Sanna Valkonen (Augsburg, DE)
Assignee: UPM-KYMMENE CORPORATION
C09J197/005C07G1/00C08G8/20C08G8/24C08H6/00C08L97/005C08L97/02C09J161/12
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Quick Facts
Patent No.
US 10,246,619
App. No.
15/251,509
Granted
Apr 2, 2019
Kind
B2
Abstract

The present invention relates to a method for increasing the reactivity of lignin, wherein the method comprises the following steps: a) forming, under heating at a temperature of 30-70° C., an aqueous dispersion comprising alkali and lignin, wherein the alkali comprises a hydroxide of an alkali metal; and b) heating the dispersion formed in step a) at a temperature of 50-95° C. for producing alkalated lignin.

Claims (10)

1. A method for producing a binder composition, the method comprising:

(a) forming, under heating at a temperature of 30-70° C., an aqueous dispersion consisting of alkali, lignin, and water, wherein the alkali comprises a hydroxide of an alkali metal, and wherein the concentration of the lignin is 10-50 weight-% based on the total weight of the aqueous dispersion;

(b) heating the aqueous dispersion formed in step (a) at a temperature of 50-95° C., thereby producing alkalated lignin, wherein the alkalated lignin has an increased reactivity relative to the lignin; and

(c) cooking an aqueous composition comprising reactant components including the alkalated lignin, a polymerizable substance, and a crosslinking agent in the presence of a catalyst at a temperature of 60-95° C. for polymerizing the reactant components until a binder composition is formed.

2. The method of claim 1 , wherein step of cooking an aqueous composition comprises cooking the aqueous composition at a temperature of 65-90° C.

3. The method of claim 1 , wherein step of cooking an aqueous composition comprises cooking the aqueous composition at a temperature of 75-85° C.

4. The method of claim 1 , wherein the crosslinking agent is an aldehyde.

5. The method of claim 1 , wherein the crosslinking agent is formaldehyde.

6. The method of claim 1 , wherein the polymerizable substance is selected from a group consisting of phenol, cresol, resorcinol, and mixtures thereof.

7. The method claim 1 , wherein the catalyst is selected from a group consisting of sodium hydroxide, potassium hydroxide, and mixtures thereof.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 6, 2019
From: PIETARINEN, SUVI; RINGENA, OKKO; ESKELINEN, KATI; VALKONEN, SANNA
To: UPM-KYMMENE CORPORATION
Reel/Frame 048245/0258 →
Priority Claims (1)
FI 20125358 · Mar 29, 2012 · national
Continuity (2)
Division 14351701
Related Publication 20160369141A1 · Dec 22, 2016
Cited By (1)
US 12,252,593