IP Library Granted Patent US 10,246,789
Granted Patent B2
US 10,246,789 · App. 15/099,966 · Granted Apr 2, 2019

Systems and methods for copper recovery via roasting and leaching

Inventors: Joanna M Robertson (Thatcher, AZ); Thomas R Bolles (Tucson, AZ); Wayne W Hazen (Lakewood, CO); Lawrence D May (Westminster, CO); Jay C Smith (Pearl River, LA); David R Baughman (Golden, CO)
Assignee: FREEPORT MINERALS CORPORATION
C25C1/12C22B1/02C22B1/26C22B3/02C22B3/12C22B3/14C22B3/22C22B15/0002C22B15/0078C22B15/0086C22B23/005C22B23/0446C22B23/0453C25C1/00C25C5/02C25C7/02Y02P10/234
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Quick Facts
Patent No.
US 10,246,789
App. No.
15/099,966
Granted
Apr 2, 2019
Kind
B2
Abstract

Various embodiments provide a process roasting a metal bearing material under oxidizing conditions to produce an oxidized metal bearing material, roasting the oxidized metal bearing material under reducing conditions to produce a roasted metal bearing material, and leaching the roasted metal bearing material in a basic medium to yield a pregnant leach solution.

Claims (25)

1. A process comprising:

roasting a metal bearing material comprising a copper carbonate under oxidizing conditions, at a temperature between about 625° C. and about 675° C.;

roasting the metal bearing material under reducing conditions, at a temperature of about 500° C. or greater; and

leaching the metal bearing material in a basic medium to yield a pregnant leach solution.

2. The process of claim 1 , wherein the basic medium comprises at least one of ammonia, ammonium carbonate and ammonium sulfate.

3. The process of claim 1 , wherein the oxidizing conditions comprise an oxygen gas containing atmosphere.

4. The process of claim 1 , wherein the reducing conditions comprise a hydrogen gas containing atmosphere.

5. The process of claim 1 , further comprising subjecting the pregnant leach solution to a solution extraction process to yield a loaded aqueous stream.

6. The process of claim 5 , wherein an extraction stage of the solution extraction yields a cobalt-bearing raffinate.

7. The process of claim 6 , further comprising precipitating cobalt from the cobalt-bearing raffinate.

8. The process of claim 7 , wherein the precipitating yields cobalt sulfide.

9. The process of claim 8 , wherein the cobalt sulfide is subjected to leaching.

10. The process of claim 5 , subjecting the loaded aqueous stream to electrowinning.

11. The process of claim 1 , wherein the copper carbonate comprises at least one of azurite and malachite.

12. A process comprising:

oxidizing a metal bearing material comprising a copper carbonate to produce an oxidized metal bearing material at a temperature between about 625° C. and about 675° C.;

reducing the oxidized metal bearing material at a temperature of about 540° C. to produce a roasted metal bearing material; and

leaching the roasted metal bearing material in a basic medium to yield a pregnant leach solution.

13. The process of claim 12 , wherein the basic medium comprises at least one of ammonia, ammonium, ammonium carbonate and ammonium sulfate.

14. The process of claim 12 , wherein the oxidizing is performed using an oxidizing agent, and wherein the reducing is performed using a reducing agent.

15. The process of claim 12 , further comprising at least one of preparing the metal bearing material and quenching the roasted metal bearing material.

16. The process of claim 12 , further comprising subjecting the pregnant leach solution to a solution extraction process to yield at least one of a loaded aqueous stream and a cobalt-bearing raffinate.

17. The process of claim 16 , further comprising precipitating cobalt from the cobalt-bearing raffinate.

18. The process of claim 17 , wherein the precipitating yields cobalt sulfide.

19. The process of claim 18 , subjecting the loaded aqueous stream to electrowinning.

Assignments (3)
CHANGE OF NAME Recorded May 6, 2016
From: FREEPORT-MCMORAN CORPORATION
To: FREEPORT MINERALS CORPORATION
Reel/Frame 038634/0624 →
MERGER Recorded May 4, 2016
From: FREEPORT-MCMORAN CORPORATION
To: FREEPORT-MCMORAN CORPORATION
Reel/Frame 038456/0027 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 15, 2016
From: ROBERTSON, JOANNA M; BOLLES, THOMAS R; HAZEN, WAYNE W; MAY, LAWRENCE D; SMITH, JAY C; BAUGHMAN, DAVID R
To: FREEPORT-MCMORAN CORPORATION
Reel/Frame 038444/0745 →
Continuity (3)
Continuation 13716836 · Dec 17, 2012
Provisional Application 61577995 · Dec 20, 2011
Related Publication 20160230296A1 · Aug 11, 2016