IP Library › Granted Patent US 10,273,238
Granted Patent B2
US 10,273,238 · App. 15/852,179 · Granted Apr 30, 2019

Indazolones as modulators of TNF signaling

Inventors: Eric C. Breinlinger (Charlton, MA); Andrew Burchat (Shrewsbury, MA); Justin Dietrich (Lindenhurst, IL); Michael Friedman (Brookline, MA); David Ihle (Worcester, MA); David Kinsman (Ashland, MA); Kelly Mullen (Charlton, MA); Augustine Osuma (Lindenhurst, IL); Anil Vasudevan (Lake Forest, IL); Noel S. Wilson (Kenosha, WI)
Assignee: AbbVie Inc.
C07D487/04C07D498/04C07D519/00
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Quick Facts
Patent No.
US 10,273,238
App. No.
15/852,179
Granted
Apr 30, 2019
Kind
B2
Abstract

The disclosure provides compounds of Formula (I) pharmaceutically acceptable salts, pro-drugs, biologically active metabolites, stereoisomers and isomers thereof wherein the variable are defined herein. The compounds of the disclosure are useful for treating immunological and oncological conditions.

Claims (59)

1. A compound of Formula (I),

or a pharmaceutically acceptable salt or stereoisomer thereof, wherein:

X is —CR 4 , and Y and Z are independently —CR 4 — or N;

provided that Y and Z are not both N;

A is —C(R z ) 2 —;

E is CH 2 or O and G is CH; or E is CH 2 and G is CH or N;

R 1 is optionally substituted aryl or optionally substituted heteroaryl;

R 2 is —R 2a —R 2b , wherein:

R 2a is an optionally substituted saturated, unsaturated or partially saturated heterocyclyl, or optionally substituted heteroaryl; and

R 2b is —N(R a )(R b ), —O(R a ), optionally substituted (C 1 -C 5 )alkyl, optionally substituted (C 3 -C 6 )cycloalkyl, —(CH 2 ) p -optionally substituted heteroaryl, or

—(CH 2 ) p -optionally substituted heterocyclyl;

wherein R a and R b are independently selected from the group consisting of H, optionally substituted (C 1 -C 5 )alkyl, and —(CH 2 ) n -optionally substituted heterocyclyl;

each instance of R 4 is independently H, halo, CF 3 , or (C 1 -C 3 )alkyl;

each instance of R z is independently H, halo, CF 3 , or (C 1 -C 3 )alkyl;

n is 1; and

p is 0 or 1;

wherein heterocyclyl is:

a non-aromatic monocyclic, bicyclic, tricyclic, or spirocyclic ring having 5 to 12 ring atoms which include at least one nitrogen, oxygen, or sulfur ring atom; or

an azetidinyl ring.

2. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein:

R 2b is —N(R a )(R b ), —O(R a ), optionally substituted (C 1 -C 5 )alkyl, optionally substituted (C 3 -C 6 )cycloalkyl, or —(CH 2 ) p -optionally substituted heterocyclyl; and

R a and R b are independently selected from the group consisting of H, optionally substituted (C 1 -C 5 )alkyl, and —(CH 2 ) n -optionally substituted heterocyclyl.

3. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein E is CH 2 , and G is CH or N.

4. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein X is CH, Y is CH, and Z is CR 4 .

5. The compound according to claim 4 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 4 is F.

6. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein X is CH, Y is CH, and Z is CH.

7. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein E is CH 2 , and G is N.

8. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 1 is optionally substituted phenyl, optionally substituted pyrazolyl, optionally substituted pyridyl, optionally substituted pyrimidinyl, or optionally substituted thiazolyl.

9. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 1 is optionally substituted phenyl.

10. The compound according to claim 9 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 1 is optionally substituted by one or more substituents independently selected from the group consisting of —CF 3 , —CN, —C(O)NH 2 , —OCHF 2 , —OCH 3 , and (C 1 -C 3 )alkyl.

11. The compound according to claim 10 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 1 is optionally substituted by one or more substituents independently selected from the group consisting of —CH 3 and —OCHF 2 .

12. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 2a is optionally substituted pyrimidinyl or optionally substituted dihydropyranyl.

13. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 2a is 1,2,4-oxadiazolyl, optionally substituted pyrazolyl, optionally substituted pyridinyl, optionally substituted pyrimidinyl, or optionally substituted 1,2,4-thiadiazolyl.

14. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 2b is N(R a )(R b ), optionally substituted (C 1 -C 4 )alkyl, optionally substituted morpholinyl, optionally substituted piperazinyl, optionally substituted piperidinyl, 1,1-dioxidothiomorpholinyl, optionally substituted hexahydroimidazo[1,5-a]pyrazin-3 (2H)-one, optionally substituted 7-azaspiro[3.5]nonane, or optionally substituted pyrrolidinyl.

15. The compound according to claim 14 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R a is H or (C 1 -C 3 )alkyl, R b is (C 1 -C 3 )alkyl, methoxypropyl, 5-oxopyrrolidin-3-ylmethyl, or tetrahydrofuranyl, and R 2b is optionally substituted by —CH 2 OH, —C(OH)(CH 3 ) 2 , —C(O)CH 3 , —C(O)OH, —OH, or alkoxyalkyl.

16. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 2a is optionally substituted pyrimidinyl.

17. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein R 2b is optionally substituted morpholinyl, optionally substituted piperidinyl, or 1,1-dioxidothiomorpholinyl.

18. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein:

X is CH;

Y is CH;

Z is CR 4 , wherein R 4 is H or F;

A is —C(R z ) 2 — wherein R z is H;

E is CH 2 ;

G is N;

R 1 is phenyl optionally substituted by one or more substituents independently selected from the group consisting of —CF 3 , —CN, —C(O)NH 2 , —OCHF 2 , —OCH 3 , and (C 1 -C 3 )alkyl;

R 2 is —R 2a —R 2b , wherein R 2a is pyrimidinyl, and R 2b is selected from the group consisting of:

—N(R a )(R b ) wherein R a is H or (C 1 -C 3 )alkyl, and R b is (C 1 -C 3 )alkyl, methoxypropyl, 5-oxopyrrolidin-3-ylmethyl, or tetrahydrofuranyl;

(C 1 -C 3 )alkyl optionally substituted by —CH 2 OH, —C(OH)(CH 3 ) 2 , —C(O)CH 3 , —C(O)OH, —OH, or alkoxyalkyl;

7-azaspiro[3.5]nonanyl optionally substituted by —CH 2 OH, —C(OH)(CH 3 ) 2 , —C(O)CH 3 , —C(O)OH, —OH, or alkoxyalkyl;

morpholinyl optionally substituted by —CH 2 OH, —C(OH)(CH 3 ) 2 , —C(O)CH 3 , —C(O)OH, —OH, or alkoxyalkyl;

piperazinyl optionally substituted by —CH 2 OH, —C(OH)(CH 3 ) 2 , —C(O)CH 3 , —C(O)OH, —OH, or alkoxyalkyl;

piperidinyl optionally substituted by —CH 2 OH, —C(OH)(CH 3 ) 2 , —C(O)CH 3 , —C(O)OH, —OH, or alkoxyalkyl;

hexahydroimidazo[1,5-a]pyrazin-3(2H)-one optionally substituted by —CH 2 OH, —C(OH)(CH 3 ) 2 , —C(O)CH 3 , —C(O)OH, —OH, or alkoxyalkyl; and

pyrrolidinyl optionally substituted by —CH 2 OH, —C(OH)(CH 3 ) 2 , —C(O)CH 3 , —C(O)OH, —OH, or alkoxyalkyl.

19. The compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof, wherein optionally substituted refers to substitution with one or more substituents selected from the group consisting of (C 1 -C 8 )alkyl; (C 2 -C 8 )alkenyl; (C 2 -C 8 )alkynyl; (C 3 -C 10 )cycloalkyl; F; Cl; Br; I; halogenated (C 1 -C 8 )alkyl; —O—(C 1 -C 8 )alkyl; ═O; ═CH 2 ; —OH; —CH 2 OH; —CH 2 OCH 3 ; —CH 2 NH 2 ; (C 1 -C 4 )alkyl-OH; —CH 2 CH 2 OCH 2 CH 3 ; —S—(C 1 -C 8 )alkyl; —SH; —NH(C 1 -C 8 )alkyl; —N((C 1 -C 8 )alkyl) 2 ; —NH 2 ; —C(O)NH 2 ; —CH 2 NHC(O)(C 1 -C 4 )alkyl; —CH 2 NHC(O)CH 2 Cl; —CH 2 NHC(O)CH 2 CN; —CH 2 NHC(O)CH 2 CH 2 N(CH 3 ) 2 ; —CH 2 NHC(O)C(═CH 2 )CH 3 ; —CH 2 NHC(O)(C 2 -C 4 )alkynyl; —CH 2 NHC(O)CH 2 CH 2 -piperidinyl; —(C 1 -C 4 )alkyl-morpholinyl; —CH 2 NHC(O)CH 2 O-phenyl wherein the phenyl is optionally substituted with halogen; (C 1 -C 4 )alkoxy; —C(O)(C 1 -C 4 )alkyl; —C(O)(C 1 -C 4 )alkoxy; —C(O)N(CH 3 ) 2 ; —N(CH 3 ) 2 ; —NHC(O)(C 1 -C 4 )alkyl; —NHC(O)(C 2 -C 4 )alkenyl; —NHC(O)CH 2 CN; —S(O) 2 (C 1 -C 4 )alkyl; 4-methylpiperazinecarbonyl; —(C 1 -C 4 )alkylC(O)NH 2 ; —C(O)NH(C 1 -C 8 )alkyl; —C(O)N((C 1 -C 8 )alkyl) 2 ; —C(O)N(H)(C 3 -C 8 )cycloalkyl; —C(O)(C 1 -C 4 )alkyl-OH; —(C 1 -C 4 )alkyl(C 1 -C 4 )alkoxy; —NHC(O)H; —NHC(O)(C 1 -C 8 )alkyl; —NHC(O)(C 3 -C 8 )cycloalkyl; —N((C 1 -C 8 )alkyl)C(O)H; —N((C 1 -C 8 )alkyl)C(O)(C 1 —C)alkyl; —NHC(O)NH 2 ; —NHC(O)NH(C 1 -C 8 )alkyl; —N((C 1 -C 8 )alkyl)C(O)NH 2 ; —NHC(O)N((C 1 -C 8 )alkyl) 2 ; —N((C 1 -C 8 )alkyl)C(O)N((C 1 -C 8 )alkyl) 2 ; —N((C 1 -C 8 )alkyl)C(O)NH((C 1 -C 8 )alkyl); —NHCH 2 -heteroaryl; benzyl; —OCH 2 -heteroaryl; —C(O)H; —C(O)(C 1 -C 8 )alkyl groups; —CN; —NO 2 ; —S(O)(C 1 -C 8 )alkyl; —S(O) 2 (C 1 -C 8 )alkyl; —S(O) 2 N((C 1 -C 8 )alkyl) 2 ; —S(O) 2 NH(C 1 -C 8 )alkyl; —S(O) 2 NH(C 3 -C 8 )cycloalkyl; —S(O) 2 NH 2 ; —NHS(O) 2 (C 1 -C 8 )alkyl; —N((C 1 -C 8 )alkyl)S(O) 2 (C 1 -C 8 )alkyl; —(C 1 -C 8 )alkyl-O—(C 1 -C 8 )alkyl; —O—(C 1 -C 8 )alkyl-O—(C 1 -C 8 )alkyl; —C(O)OH; —C(O)O(C 1 -C 8 )alkyl; NHOH; NHO(C 1 -C 8 )alkyl; —O-halogenated (C 1 -C 8 )alkyl; —S(O) 2 -halogenated (C 1 -C 8 )alkyl; —S-halogenated (C 1 -C 8 )alkyl; —NHC(O)O—(C 1 -C 6 )alkyl; —N((C 1 -C 6 )alkyl)C(O)O—(C 1 -C 6 )alkyl; —C(═NH)—(C 1 -C 6 )alkyl; —C(═NOH)—(C 1 -C 6 )alkyl; and —C(═N—O—(C 1 -C 6 )alkyl)-(C 1 -C 6 )alkyl.

20. The compound of claim 1 , wherein the compound is:

or a pharmaceutically acceptable salt thereof.

21. A pharmaceutical composition comprising a compound according to claim 1 , or a pharmaceutically acceptable salt or stereoisomer thereof; and one or more pharmaceutically acceptable excipients.

22. A pharmaceutical composition comprising a compound according to claim 20 , or a pharmaceutically acceptable salt thereof; and one or more pharmaceutically acceptable excipients.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 26, 2017
From: BREINLINGER, ERIC C.; BURCHAT, ANDREW F.; DIETRICH, JUSTIN D.; FRIEDMAN, MICHAEL M.; IHLE, DAVID C.; KINSMAN, DAVID A.; MULLEN, KELLY D.; OSUMA, AUGUSTINE T.; VASUDEVAN, ANIL; WILSON, NOEL S.
To: ABBVIE INC.
Reel/Frame 044485/0089 →
Continuity (3)
Division 15130323 · Apr 15, 2016
Provisional Application 62149336 · Apr 17, 2015
Related Publication 20180215764A1 · Aug 2, 2018