IP Library Granted Patent US 10,326,164
Granted Patent B2
US 10,326,164 · App. 15/060,109 · Granted Jun 18, 2019

High-conduction GE substituted LiAsS4 solid electrolyte

Inventors: Chengdu Liang (Knoxville, TN); Nancy J. Dudney (Knoxville, TN); Ezhiylmurugan Rangasamy (San Jose, CA); Gayatri Sahu (Knoxville, TN)
Assignee: UT-BATTELLE, LLC
H01M10/0562H01B1/06H01M10/052H01M2300/0068
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,326,164
App. No.
15/060,109
Granted
Jun 18, 2019
Kind
B2
Abstract

A solid electrolyte for a lithium battery includes Li 3+x Ge x As 1-x S 4 where x=0 to 0.50. The value of x can be a range of any high value and any lower value from 0 to 0.50. For example, x can be 0.25 to 0.50, and x can be 0.3 to 0.4, among many other possible ranges. In one embodiment x=0.33 such that the solid electrolyte is Li 3.334 Ge 0.334 As 0.666 S 4 . A solid electrolyte for a lithium battery can include LiAsS 4 wherein ½ to ⅔ of the As is substituted with Ge. A lithium battery and a method for making a lithium battery are also disclosed.

Claims (15)

1. A solid electrolyte for a lithium battery, comprising Li 3+x Ge x As 1-x S 4 where x=0 to 0.50, and having an ionic conductivity of greater than 1 mScm −1 at 27° C. and an activation energy of no more than 0.3 eV.

2. The solid electrolyte of claim 1 wherein x=0.25 to 0.5.

3. The solid electrolyte of claim 1 , wherein x=0.3 to 0.4.

4. The solid electrolyte of claim 1 , wherein x=0.33.

5. The solid electrolyte of claim 1 , wherein the electrolyte has an ionic conductivity of at least 1.12 mScm −1 at 27° C.

6. A lithium battery comprising a solid electrolyte, the solid electrolyte comprising Li 3+x Ge x As 1-x S 4 , wherein x=0 to 0.50, and having an ionic conductivity of greater than 1 mScm −1 at 27° C. and an activation energy of no more than 0.3 eV.

7. The lithium battery of claim 6 , wherein x=0.25 to 0.50.

8. The lithium battery of claim 6 , wherein x=0.3 to 0.4.

9. The lithium battery of claim 6 , wherein x=0.33.

10. The lithium battery of claim 6 , wherein the electrolyte has an ionic conductivity of at least 1.12 mScm −1 at 27° C.

11. A solid electrolyte for a lithium battery, comprising LiAsS 4 wherein ½ to % of the As is substituted with Ge.

12. A lithium battery comprising a solid electrolyte, the solid electrolyte comprising LiAsS 4 wherein ½ to ⅔ of the As is substituted with Ge.

13. A method of making a lithium battery, comprising the steps of:

providing an anode and a cathode;

positioning between the anode and the cathode a solid electrolyte, wherein the electrolyte comprises Li 3+x Ge x As 1-x S 4 where x=0 to 0.50, and having an ionic conductivity of greater than 1 mScm −1 at 27° C. and an activation energy of no more than 0.3 eV.

Assignments (4)
CONFIRMATORY LICENSE Recorded Jul 18, 2016
From: UT-BATTELLE, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 039177/0051 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 22, 2016
From: LIANG, CHENGDU; DUDNEY, NANCY J.
To: UT-BATTELLE, LLC
Reel/Frame 038982/0411 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 22, 2016
From: RANGASAMY, EZHIYLMURUGAN; SAHU, GAYATRI
To: OAK RIDGE ASSOCIATED UNIVERSITIES
Reel/Frame 038982/0482 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 22, 2016
From: OAK RIDGE ASSOCIATED UNIVERSITIES
To: UT-BATTELLE, LLC
Reel/Frame 038982/0528 →
Continuity (2)
Provisional Application 62127334 · Mar 3, 2015
Related Publication 20160261001A1 · Sep 8, 2016