IP Library › Granted Patent US 10,335,713
Granted Patent B2
US 10,335,713 · App. 15/075,017 · Granted Jul 2, 2019

Extraction apparatus and method

Inventor: Nicholas Tennant (Royal Oak, MI)
Assignee: Precision Extraction Corporation
B01D11/0296B01D11/0288C07D311/80
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Quick Facts
Patent No.
US 10,335,713
App. No.
15/075,017
Granted
Jul 2, 2019
Kind
B2
Abstract

An extraction apparatus and a processes for preparing extracts of natural products, such as plant material, and for preparing purified extracts from crude extracts of natural products by extraction with a non-polar solvent hot gas.

Claims (19)

1. A closed-loop extraction apparatus for extracting constituent components from a plant material by exposing them to a solvent, the closed-loop extractor apparatus comprising:

a solvent tank for receiving and collecting the solvent;

a material tank for receiving the plant material and for receiving a liquid solvent from the solvent tank and exposing the plant material to the solvent for extracting constituent components from the plant material;

a collection tank for receiving the solvent from the material tank including the extracted constituent components; and

a cooled, inline lipid coagulation apparatus coupled between the material tank and the collection tank.

2. The closed-loop extraction apparatus of claim 1 , including a hydrocarbon recovery pump coupled to receive the heated solvent form the collection tank and pump it into the solvent tank.

3. The closed-loop extraction apparatus of claim 1 , wherein the solvent tank is a jacketed solvent tank and wherein the material column is a jacketed material column and the apparatus further comprising a cryogenic chiller coupled to the jacket of the solvent tank and to the jacket of the material column and cools the solvent tank in the material column.

4. The closed-loop extraction apparatus of claim 2 , wherein the solvent tank is a jacketed solvent tank and wherein the material column is a jacketed material column and the apparatus further comprising a cyrogenic chiller coupled to the jacket of the solvent tank and to the jacket of the material column and cools the solvent tank and the material column.

5. The closed-loop extraction apparatus of claim 1 , wherein said solvent is a non-polar solvent.

6. The closed-loop extraction apparatus of claim 1 , said closed-loop extraction apparatus further comprising a wheeled mounting rack, wherein said solvent tank, said material tank, and said collection tank are positioned on said wheeled mounting rack.

7. The closed-loop extraction apparatus of claim 1 , wherein said solvent is a light hydrocarbon solvent.

8. The closed-loop extraction apparatus of claim 1 , said closed-loop extraction apparatus further comprising an expansion filter tank, a recovery pump, and a recirculating heater.

9. The closed-loop extraction apparatus of claim 1 , said closed loop extraction apparatus further comprising a recovery pump that provides for returning solvent to said solvent tank.

10. The closed-loop extraction apparatus of claim 1 , said closed loop extraction apparatus further comprising a shutoff valve for isolating said solvent tank.

11. The closed-loop extraction apparatus of claim 1 , said closed loop extraction apparatus further comprising a vacuum pump coupled to said solvent tank, wherein said vacuum pump provides for removing oxygen.

12. The closed-loop extraction apparatus of claim 1 , wherein said cooled, inline lipid coagulation apparatus includes a coiled tubing within a chamber.

13. The closed-loop extraction apparatus of claim 1 , wherein said cooled, inline lipid coagulation apparatus includes a chamber cooled to between −40° F. and −120° F.

14. The closed-loop extraction apparatus of claim 1 , wherein the constituent components include a specific cannabinoid.

15. The closed-loop extraction apparatus of claim 1 , wherein said cooled, inline lipid coagulation apparatus includes a filter stack space that holds a filter.

Assignments (7)
SECURITY INTEREST Recorded Apr 11, 2023
From: AGRIFY CORPORATION; HARBOR MOUNTAIN HOLDINGS, LLC; TRIGROW SYSTEMS LLC; AGM SERVICE COMPANY LLC; AGXION, LLC; ARIAFY FINANCE, LLC; CASCADE SCIENCES, LLC; PUREPRESSURE, LLC; PURE SERVICES LLC; PRECISION EXTRACTION NEWCO, LLC; LAB SOCIETY NEWCO, LLC; LAB SOCIETY LLC; ERS LTD; LS ANALYTICS LLC; ELECTRUM EXTRACTORS LLC; ELITELAB LLC; LS SOLUTIONS LLC; AGRIFY BRANDS, LLC
To: HIGH TRAIL SPECIAL SITUATIONS LLC, AS COLLATERAL AGENT
Reel/Frame 063291/0836 →
SECOND AMENDMENT TO INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Apr 11, 2023
From: AGRIFY CORPORATION; HARBOR MOUNTAIN HOLDINGS, LLC; TRIGROW SYSTEMS LLC; AGM SERVICE COMPANY LLC; AGXION, LLC; ARIAFY FINANCE, LLC; CASCADE SCIENCES, LLC; PUREPRESSURE, LLC; PURE SERVICES LLC; PRECISION EXTRACTION NEWCO, LLC; LAB SOCIETY NEWCO, LLC; LAB SOCIETY LLC; ERS LTD; LS ANALYTICS LLC; ELECTRUM EXTRACTORS LLC; ELITELAB LLC; LS SOLUTIONS LLC; AGRIFY BRANDS, LLC
To: HIGH TRAIL SPECIAL SITUATIONS LLC, AS COLLATERAL AGENT
Reel/Frame 063374/0196 →
AMENDMENT TO INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Apr 11, 2023
From: AGRIFY CORPORATION; HARBOR MOUNTAIN HOLDINGS, LLC; TRIGROW SYSTEMS LLC; AGM SERVICE COMPANY LLC; AGXION, LLC; ARIAFY FINANCE, LLC; CASCADE SCIENCES, LLC; PUREPRESSURE, LLC; PURE SERVICES LLC; PRECISION EXTRACTION NEWCO, LLC; LAB SOCIETY NEWCO, LLC; LAB SOCIETY LLC; ERS LTD; LS ANALYTICS LLC; ELECTRUM EXTRACTORS LLC; ELITELAB LLC; LS SOLUTIONS LLC; AGRIFY BRANDS, LLC
To: HIGH TRAIL SPECIAL SITUATIONS LLC, AS COLLATERAL AGENT
Reel/Frame 063297/0188 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 12, 2022
From: PRECISION EXTRACTION NEWCO, LLC
To: AGRIFY CORPORATION
Reel/Frame 058637/0291 →
MERGER AND CHANGE OF NAME Recorded Nov 16, 2021
From: MASS2MEDIA, LLC; PRECISION EXTRACTION NEWCO, LLC
To: PRECISION EXTRACTION NEWCO, LLC
Reel/Frame 058125/0584 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 30, 2021
From: TENNANT, NICHOLAS
To: PRECISION EXTRACTION CORPORATION
Reel/Frame 057663/0451 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 30, 2021
From: PRECISION EXTRACTION CORPORATION
To: MASS2MEDIA, LLC
Reel/Frame 057663/0612 →
Continuity (2)
Provisional Application 62134621 · Mar 18, 2015
Related Publication 20170043276A1 · Feb 16, 2017