IP Library Granted Patent US 10,357,510
Granted Patent B2
US 10,357,510 · App. 15/501,243 · Granted Jul 23, 2019

Metal nanoclusters and uses thereof

Inventors: Theodore Goodson, III (Ann Arbor, MI); Oleg Varnavski (Ypsilanti, MI); Sung Hei Yau (Ann Arbor, MI)
Assignee: THE REGENTS OF THE UNIVERSITY OF MICHIGAN
A61K33/00A61K41/0057C08K3/014C09D5/32C09D7/61G01N33/587B82Y5/00Y10S977/773
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Quick Facts
Patent No.
US 10,357,510
App. No.
15/501,243
Granted
Jul 23, 2019
Kind
B2
Abstract

Provided herein are metal nanoclusters, having a high absorption to volume ratio, and uses of the same, such as in generating singlet oxygen, or in protecting surfaces from high intensity light.

Claims (15)

1. A conjugate comprising a metal nanocluster having at least a portion of the surface of the metal nanocluster modified with a moiety having a structure -X-Lk-Lg;

wherein

the metal nanocluster comprises Au 144 , Ag 32 , or a combination thereof;

Lk is C 1-50 alkylene, wherein the carbon backbone optionally has one or more heteroatoms selected from O, NH, and S;

X is a functional group capable of attaching to the metal nanocluster surface; and

Lg is a ligand selected from the group consisting of a peptide, a protein, an oligonucleotide, a fluorophore, and a chromophore.

2. The conjugate of claim 1 , wherein X comprises an alcohol, an ether, a thiol, a phosphate, a phosphonate, phosphinate, or a carboxylate.

3. The conjugate of claim 1 , wherein the metal nanocluster is Au 144 .

4. The conjugate of claim 1 , wherein Lg is a two-photon chromophore.

5. The conjugate of claim 1 , wherein Lg is a fluorophore.

6. A composition comprising the conjugate of claim 1 in a liquid.

7. A composition comprising the conjugate of claim 1 in the form of a coating or a film.

8. The composition of claim 7 , wherein the film comprises a polymer selected from the group consisting of polyvinylpyrrolidone, polyvinyl alcohol, poly-methyl methacrylate, polystyrene, polyethylene oxide, polyethylene glycol, and a mixture thereof.

9. The composition of claim 7 , further comprising a photosensitive additive.

10. The conjugate of claim 1 , wherein the metal nanocluster exhibits an absorption to volume ratio of at least 10 7 m −1 under linear or non-linear excitation, has an excited state longer than 10 psec, and exhibits no plasmon resonance.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 27, 2017
From: GOODSON, THEODORE, III; VARNAVSKI, OLEG; YAU, SUNG HEI
To: THE REGENTS OF THE UNIVERSITY OF MICHIGAN
Reel/Frame 042167/0844 →
Continuity (2)
Provisional Application 62034285 · Aug 7, 2014
Related Publication 20170216348A1 · Aug 3, 2017