IP Library › Granted Patent US 10,391,561
Granted Patent B2
US 10,391,561 · App. 15/529,918 · Granted Aug 27, 2019

Cubic boron nitride-based sintered material and cutting tool made of cubic boron nitride-based sintered material

Inventors: Masahiro Yano (Naka-gun, JP); Yosuke Miyashita (Naka-gun, JP)
Assignee: MITSUBISHI MATERIALS CORPORATION
B23B27/148C04B35/5831C04B35/62836C04B35/62884C04B35/62897C04B35/645B23B2226/125C04B2235/3217C04B2235/3232C04B2235/3258C04B2235/386C04B2235/3813C04B2235/3843C04B2235/3847C04B2235/3856C04B2235/3865C04B2235/3886C04B2235/402C04B2235/404C04B2235/5436C04B2235/5445C04B2235/604C04B2235/6567C04B2235/6581C04B2235/661C04B2235/723C04B2235/80
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Quick Facts
Patent No.
US 10,391,561
App. No.
15/529,918
Granted
Aug 27, 2019
Kind
B2
Abstract

A cubic boron nitride-based sintered material includes cubic boron nitride particles of 70 to 95 vol %, in which in a structure of a cross-section of the sintered material, a binder phase with a width of 1 nm to 30 nm is present between the adjacent cubic boron nitride particles, the binder phase being made of a compound containing at least Al, B, and N and having a ratio of an oxygen content to an Al content of 0.1 or less in terms of atomic ratio.

Claims (32)

1. A cubic boron nitride-based sintered material comprising:

cubic boron nitride particles of 70 to 95 vol %,

wherein in a structure of a cross-section of the sintered material, a binder phase with a width of 1 nm to 30 nm is present between the adjacent cubic boron nitride particles, the binder phase being made of a compound containing at least Al, B, and N and having a ratio of an oxygen content to an Al content of 0.1 or less in terms of atomic ratio.

2. A cubic boron nitride-based sintered material comprising;

cubic boron nitride particles of 70 to 95 vol %,

wherein in a structure of a cross-section of the sintered material, there is a region where an interval between the adjacent cubic boron nitride particles is 30 nm or less, where a binder phase is made of a nitride containing at least one of Al and B, or both Al and B, and an Al oxide, and where a ratio of an oxygen content to an Al content in the binder phase is 0.1 or less in terms of atomic ratio.

3. The cubic boron nitride-based sintered material according to claim 1 ,

wherein the average particle diameter of the cubic boron nitride particles is 0.5 to 8.0 μm,

in at least five fields of view of the structure of the cross-section of the cubic boron nitride-based sintered material with a field of view of 5 times×5 times the average particle diameter of the cubic boron nitride particles as one field of view, the cubic boron nitride particles having a binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle are observed in fields of view of 60% or more of the total number of the fields of view, the binder phase having a ratio of an oxygen content to an Al content of 0.1 or less.

4. The cubic boron nitride-based sintered material according to claim 1 ,

wherein in the structure of the cross-section of the cubic boron nitride-based sintered material:

an average particle number ratio of the number of the cubic boron nitride particles having the binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle with respect to the total number of the cubic boron nitride particles in the observed cross-section is 0.4 or more; and

among the cubic boron nitride particles having the binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle, an average ratio of the number of the cubic boron nitride particles having the binder phase with a ratio of an oxygen content to an Al content of 0.1 or less with respect to the number of the cubic boron nitride particles having the binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle is 0.5 or more.

5. The cubic boron nitride-based sintered material according to claim 1 ,

wherein the binder phases which are present between the adjacent cubic boron nitride particles and have a width of 1 nm to 30 nm are dotted between the adjacent cubic boron nitride particles.

6. A cutting tool made of cubic boron nitride-based sintered material comprising:

a cutting edge portion made of the cubic boron nitride-based sintered material according to claim 1 .

7. The cubic boron nitride-based sintered material according to claim 2 ,

wherein the average particle diameter of the cubic boron nitride particles is 0.5 to 8.0 μm,

in at least five fields of view of the structure of the cross-section of the cubic boron nitride-based sintered material with a field of view of 5 times×5 times the average particle diameter of the cubic boron nitride particles as one field of view, the cubic boron nitride particles having a binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle are observed in fields of view of 60% or more of the total number of the fields of view, the binder phase having a ratio of an oxygen content to an Al content of 0.1 or less.

8. The cubic boron nitride-based sintered material according to claim 2 ,

wherein in the structure of the cross-section of the cubic boron nitride-based sintered material:

an average particle number ratio of the number of the cubic boron nitride particles having the binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle with respect to the total number of the cubic boron nitride particles in the observed cross-section is 0.4 or more; and

among the cubic boron nitride particles having the binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle, an average ratio of the number of the cubic boron nitride particles having the binder phase with a ratio of an oxygen content to an Al content of 0.1 or less with respect to the number of the cubic boron nitride particles having the binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle is 0.5 or more.

9. The cubic boron nitride-based sintered material according to claim 7 ,

wherein in the structure of the cross-section of the cubic boron nitride-based sintered material:

an average particle number ratio of the number of the cubic boron nitride particles having the binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle with respect to the total number of the cubic boron nitride particles in the observed cross-section is 0.4 or more; and

among the cubic boron nitride particles having the binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle, an average ratio of the number of the cubic boron nitride particles having the binder phase with a ratio of an oxygen content to an Al content of 0.1 or less with respect to the number of the cubic boron nitride particles having the binder phase with a width of 1 nm to 30 nm between the adjacent cubic boron nitride particle is 0.5 or more.

10. The cubic boron nitride-based sintered material according to claim 2 ,

wherein the binder phases which are present between the adjacent cubic boron nitride particles and have a width of 1 nm to 30 nm are dotted between the adjacent cubic boron nitride particles.

11. A cutting tool made of cubic boron nitride-based sintered material comprising:

a cutting edge portion made of the cubic boron nitride-based sintered material according to claim 2 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 13, 2017
From: YANO, MASAHIRO; MIYASHITA, YOSUKE
To: MITSUBISHI MATERIALS CORPORATION
Reel/Frame 042695/0413 →
Priority Claims (2)
JP 2014-240418 · Nov 27, 2014 · national
JP 2015-229737 · Nov 25, 2015 · national
Continuity (1)
Related Publication 20170341155A1 · Nov 30, 2017