IP Library Granted Patent US 10,414,966
Granted Patent B2
US 10,414,966 · App. 15/762,075 · Granted Sep 17, 2019

Settable compositions with variable set times

Inventors: Paul Alan Brown (Duncan, OK); Thomas J. Pisklak (Cypress, TX); Darrell Chad Brennies (Marlow, OK)
Assignee: Halliburton Energy Services, Inc.
C09K8/42C04B26/02C04B28/02C04B40/0032C09K8/44C09K8/467C09K8/487E21B33/13E21B33/14
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Quick Facts
Patent No.
US 10,414,966
App. No.
15/762,075
Granted
Sep 17, 2019
Kind
B2
Abstract

A settable composition may be designed to thicken at substantially the same time downhole and/or set at substantially the same time downhole independent of when the settable composition was introduced into the wellbore by varying the concentration of set retarders and/or set accelerators during placement of settable compositions. For example, a method may include introducing a settable composition into a wellbore, the settable composition having an initial portion with a first concentration of a set-time additive, a middle portion with a second concentration of a set-time additive, and a final portion with a third concentration of a set-time additive; choosing the first and the third concentrations of the set-time additive so that the initial portion has a longer set-time than the final portion; and thickening the settable, wherein the initial and final portions thicken to exceed a consistency of about 70 Bc within about 3 hours of each other.

Claims (23)

1. A method comprising:

introducing a settable composition into a wellbore penetrating a subterranean formation, wherein the settable composition is placed as an initial portion having a first concentration of a set-time additive, a middle portion having a second concentration of a set-time additive, and a final portion having a third concentration of a set-time additive, wherein the initial, the middle, and the final portions correspond to different locations of the wellbore;

setting the first and the third concentrations of the set-time additive such that the initial portion of the settable composition has a longer set-time than the final portion of the settable composition; and

thickening the settable composition within the wellbore, wherein the initial and final portions of the settable composition thicken to exceed a consistency of about 70 Bearden units (Bc) within about 3 hours of each other.

2. The method of claim 1 , wherein the middle portion of the settable composition thickens to exceed the consistency of about 70 Bc within about 3 hours of the initial and final portions.

3. The method of claim 1 , wherein the initial and final portions of the settable composition thicken to exceed the consistency of about 70 Bc within about 1 hour of each other.

4. The method of claim 3 , wherein the middle portion of the settable composition thickens to exceed the consistency of about 70 Bc within about 1 hour of the initial and final portions.

5. The method of claim 1 , wherein the settable composition is a cement slurry that comprises water, cement, and the set-time additive, wherein the set-time additive comprises a set retarder at a concentration of about 0.1% to about 1.0% by weight of the cement in the initial portion of the cement slurry and about 1.0% to about 2.0% by weight of the cement in the final portion of the cement slurry.

6. The method of claim 1 , wherein the settable composition is a cement slurry that comprises water, cement, and the set-time additive, wherein the set-time additive comprises a set accelerator at a concentration of about 8.0% to about 10.0% by weight of the cement in the initial portion of the cement slurry and about 0.0% to about 2.0% by weight of the cement in the final portion of the cement slurry.

7. The method of claim 1 , wherein the settable composition is a cement slurry that comprises water, cement, and the set-time additive, wherein the set-time additive comprises a fluid loss additive at a concentration of about 8.0% to about 10.0% by weight of the cement in the initial portion of the cement slurry and about 0.0% to about 2.0% by weight of the cement in the final portion of the cement slurry.

8. The method of claim 1 , wherein the settable composition is a cement slurry that comprises water, cement, and the set-time additive, wherein the set-time additive comprises a dispersant at a concentration of about 0.5% to about 0.75% by weight of the cement in the initial portion of the cement slurry and about 2.5% to about 3% by weight of the cement in the final portion of the cement slurry.

9. The method of claim 1 , wherein the settable composition is a cement slurry that comprises water, cement, and the set-time additive, wherein the set-time additive comprises a viscosifier at a concentration of about 0.01% to about 0.02% by weight of the cement in the initial portion of the cement slurry and about 0.04% to about 0.06% by weight of the cement in the final portion of the cement slurry.

10. The method of claim 1 , wherein the settable composition is a hardenable resin composition that comprises a liquid hardenable resin, a hardening agent, and the set-time additive, wherein the set-time additive comprises filler particles at a concentration of about 50% to about 100% by weight of the liquid hardenable resin in the initial portion of the hardenable resin composition and about 150% to about 200% by weight of the liquid hardenable resin in the final portion of the hardenable resin composition.

11. The method of claim 1 , wherein the settable composition is a hardenable resin composition that comprises a liquid hardenable resin, a hardening agent, and the set-time additive, wherein the set-time additive comprises a solvent at a concentration of about 20% to about 30% by weight of the liquid hardenable resin in the initial portion of the hardenable resin composition and about 10% to about 20% by weight of the liquid hardenable resin in the final portion of the hardenable resin composition.

12. The method of claim 11 , wherein the middle portion of the hardenable resin composition comprises the solvent at a concentration of about 0% to about 10% by weight of the liquid hardenable resin.

13. The method of claim 1 , wherein the settable composition is a hardenable resin composition that comprises a liquid hardenable resin, a hardening agent, and the set-time additive, wherein the set-time additive comprises an accelerator at a concentration of about 15% to about 20% by weight of the liquid hardenable resin in the initial portion of the hardenable resin composition and about 10% to about 15% by weight of the liquid hardenable resin in the final portion of the hardenable resin composition.

14. The method of claim 13 , wherein the middle portion of the hardenable resin composition comprises the accelerator at a concentration of about 0% to about 10% by weight of the liquid hardenable resin.

15. A method comprising:

introducing a settable composition into a wellbore penetrating a subterranean formation, wherein the settable composition comprises an initial portion having a first concentration of a set-time additive and a final portion having a second concentration of a set-time additive, wherein the initial and the final portions correspond to different locations of the wellbore;

adjusting the first and the second concentrations of set-time additive such that the initial portion of the settable composition has a longer set-time than the final portion of the settable composition; and

hardening the settable composition within the wellbore, wherein the initial and final portions of the settable composition harden to exceed a compressive strength of about 50 pounds per square inch (psi) within about 3 hours of each other, and wherein a middle portion of the settable composition hardens to exceed the compressive strength of about 50 psi within about 3 hours of the initial and final portions.

16. The method of claim 15 , wherein the initial and final portions of the settable composition harden to exceed compressive strength of about 50 psi within about 1 hour of each other.

17. The method of claim 16 , wherein a middle portion of the settable composition hardens to exceed the compressive strength of about 50 psi within about 1 hour of the initial and final portions.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 1, 2018
From: BROWN, PAUL ALAN; PISKLAK, THOMAS J.; BRENNIES, DARRELL CHAD
To: HALLIBURTON ENERGY SERVICES, INC.
Reel/Frame 047020/0500 →
Continuity (1)
Related Publication 20180273825A1 · Sep 27, 2018
Cited By (1)
US 12,534,974