IP Library › Granted Patent US 10,428,088
Granted Patent B2
US 10,428,088 · App. 15/987,506 · Granted Oct 1, 2019

Muscarinic receptor agonists

Inventors: Miles Stuart Congreve (Cambridge, GB); Giles Albert Brown (Cambridge, GB); Benjamin Gerald Tehan (Cambridge, GB); Mark Pickworth (Cambridge, GB); Julie Elaine Cansfield (Cambridge, GB)
Assignee: Heptares Therapeutics Limited
C07D519/00A61K31/438A61K31/439C07D471/10C07D498/10
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Quick Facts
Patent No.
US 10,428,088
App. No.
15/987,506
Granted
Oct 1, 2019
Kind
B2
Abstract

This invention relates to compounds that are agonists of the muscarinic M 1 receptor and which are useful in the treatment of muscarinic M 1 receptor mediated diseases. Also provided are pharmaceutical compositions containing the compounds and the therapeutic uses of the compounds. Compounds provided are of formula where m, p, q, W, Z, Y, X 1 , X 2 , R 1 , R 2 , R 3 and R 4 are as defined herein.

Claims (49)

1. A compound of the formula (1a):

or a salt thereof, wherein:

m is 1;

p is 0;

q is 0;

W is C;

Z is CH 2 ;

Y is O;

X 1 and X 2 are saturated hydrocarbon groups which together contain a total of five to nine carbon atoms and which link together such that the moiety:

is selected from ring systems BA to BH below:

R 1 can be H, optionally substituted C 1-6 alkyl or CH 2 -aryl;

R 2 is H;

R 3 is H, OH, or an optionally substituted C 1-6 non-aromatic hydrocarbon group;

R 4 can be H, optionally substituted C 1-5 alkyl or optionally substituted C 2-5 alkynyl.

2. The compound according to claim 1 , wherein R 1 is selected from H, C 1-5 alkyl and benzyl.

3. The compound according to claim 1 , wherein R 3 is selected from H, OH, ethyl, n-propyl, isopropyl, isobutyl, cyclopropylmethyl and 2-methoxyethyl.

4. The compound according to claim 1 , wherein R 4 is selected from H, methyl, fluoromethyl, ethyl, ethynyl and 1-propynyl.

5. The compound according to claim 1 which is selected from the group consisting of:

ethyl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate and prop-2-yn-1-yl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate

or a salt thereof.

6. The compound according to claim 1 which is selected from the group consisting of:

ethyl (3-endo)-3-(2-hydroxy-3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate and

ethyl 5-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-2-azabicyclo[2.2.2]octane-2-carboxylate or a salt thereof.

7. The compound according to claim 1 which is selected from the group consisting of:

ethyl 5-(2-oxo-1-oxa-3,8-diazaspiro[4.5]dec-8-yl)-2-azabicyclo[2.2.1]heptane-2-carboxylate,

methyl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate, 2-fluoroethyl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate,

but-2-yn-1-yl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-(1-methyl-3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-(1-ethyl-3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-(3-oxo-1-propyl-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-(1-benzyl-3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-(2-ethyl-3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-(2-hydroxy-3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-(3-oxo-2-propyl-2,8-diazaspiro[4.5]dec-8-yl)-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-[3-oxo-2-(propan-2-yl)-2,8-diazaspiro[4.5]dec-8-yl]-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-[2-(2-methylpropyl)-3-oxo-2,8-diazaspiro[4.5]dec-8-yl]-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-[2-(cyclopropylmethyl)-3-oxo-2,8-diazaspiro[4.5]dec-8-yl]-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 3-[2-(2-methoxyethyl)-3-oxo-2,8-diazaspiro[4.5]dec-8-yl]-8-azabicyclo[3.2.1]octane-8-carboxylate,

ethyl 8-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-3-azabicyclo[3.2.1]octane-3-carboxylate,

ethyl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-9-azabicyclo[3.3.1]nonane-9-carboxylate,

prop-2-yn-1-yl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-9-azabicyclo[3.3.1]nonane-9-carboxylate,

but-2-yn-1-yl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-9-azabicyclo[3.3.1]nonane-9-carboxylate,

methyl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-6-azabicyclo[3.2.1]octane-6-carboxylate,

ethyl 3-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-6-azabicyclo[3.2.1]octane-6-carboxylate, and

ethyl 6-(3-oxo-2,8-diazaspiro[4.5]dec-8-yl)-3-azabicyclo[3.1.1]heptane-3-carboxylate,

or a salt thereof.

8. A pharmaceutical composition comprising the compound as defined in claim 1 and a pharmaceutically acceptable excipient.

9. A method of treating dementia in a subject, comprising administering an effective amount of the compound according to claim 1 to the subject in need thereof.

10. A method of treating Alzheimer's disease in a subject, comprising administering an effective amount of the compound according to claim 1 to the subject in need thereof.

Assignments (3)
CHANGE OF NAME Recorded Sep 9, 2024
From: HEPTARES THERAPEUTICS LIMITED
To: NXERA PHARMA UK LIMITED
Reel/Frame 068524/0400 →
CHANGE OF ADDRESS Recorded Mar 21, 2019
From: HEPTARES THERAPEUTICS LIMITED
To: HEPTARES THERAPEUTICS LIMITED
Reel/Frame 048661/0096 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 7, 2018
From: CONGREVE, MILES STUART; BROWN, GILES ALBERT; TEHAN, BENJAMIN GERALD; PICKWORTH, MARK; CANSFIELD, JULIE ELAINE
To: HEPTARES THERAPEUTICS LIMITED
Reel/Frame 046574/0048 →
Priority Claims (1)
GB 1404922.5 · Mar 19, 2014 · national
Continuity (2)
Continuation 15126935
Related Publication 20180327426A1 · Nov 15, 2018
Cited By (3)
US 12,202,843 US 12,215,099 US 12,291,512