IP Library Granted Patent US 10,449,469
Granted Patent B2
US 10,449,469 · App. 15/848,560 · Granted Oct 22, 2019

Oil extraction aids in bioproduct production

Inventor: Scott Romak Lewis (Wilmington, DE)
Assignee: SOLENIS TECHNOLOGIES, L.P.
B01D11/0492A23D9/00A23D9/02C10L1/02C10L1/1802C11B1/02C11B1/10C11B3/006C11B13/00C10L2200/0484C10L2290/141C10L2290/544
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Quick Facts
Patent No.
US 10,449,469
App. No.
15/848,560
Granted
Oct 22, 2019
Kind
B2
Abstract

A method is provided for the use of a process additive system to improve the recovery of oil from a process stream generated in a bioproduct production process.

Claims (29)

1. A method for recovering oil from grain to bioproduct production, the method comprising adding a process additive system to a process stream in a grain to bioproduct production wherein the process additive system comprises at least one first nonionic surfactant and at least one second nonionic surfactant,

wherein the first nonionic surfactant comprises POE (20) sorbitan monooleate and the second nonionic surfactant comprises an alkoxylated triglyceride and

wherein the first nonionic surfactant comprises at least 3% of the total weight of the process additive system and the second nonionic surfactant comprises at least 3% of the total weight of the process additive system and

wherein the ratio by weight of the first nonionic surfactant to the second nonionic surfactant is from 1:3 to 3:1.

2. The method of claim 1 wherein the first nonionic surfactant comprises a functionalized polyol derived from a sorbitan.

3. The method of claim 1 wherein the second nonionic surfactant comprises an alkoxylated castor oil.

4. The method of claim 1 wherein the second nonionic surfactant comprises an alkoxylated castor oil that has been alkoxylated with from about 15 to about 60 moles of an alkyl oxide wherein the alkyl oxide is selected from ethylene oxide, propylene oxide, and mixtures thereof.

5. The method of claim 1 wherein the second nonionic surfactant comprises an ethoxylated castor oil.

6. The method of claim 1 wherein the process additive system further comprises silica wherein the silica comprises from 3% to 15% of the total weight of the process additive system.

7. The method of claim 6 wherein the silica is a hydrophobic silica.

8. The method of claim 1 wherein the ratio by weight of the first nonionic surfactant to the second nonionic surfactant is from 1:2 to 2:1.

9. The method of claim 1 wherein the first nonionic surfactant comprises at least 8% of the total weight of the process additive system and the second nonionic surfactant comprises at least 8% of the total weight of the process additive system.

10. The method of claim 1 wherein the ratio by weight of the first nonionic surfactant to the second nonionic surfactant is from 1:1 to 3:1.

11. The method of claim 1 wherein the process additive system further comprises additional additives, wherein the additional additives comprise from 0.1% to 50% of the total weight of the process additive system, wherein at least one additional additive is selected from the group consisting of fatty acid alkyl esters, PEG fatty alcohol esters, monoglycerides, diglycerides, triglycerides, mineral oils, fatty alcohols, and combinations thereof.

12. The method of claim 1 wherein the process additive system further comprises additional additives, wherein the additional additives comprise from 0.1% to 50% of the total weight of the process additive system, wherein at least one additional additive comprises PEG fatty acid esters.

13. The method of claim 11 wherein the additional additives comprises fatty acid alkyl esters and wherein the additional additives comprise from 5% to 30% of the total weight of the process additive system.

14. The method of claim 13 wherein the additional additives comprise fatty acid methyl esters.

15. The method of claim 1 wherein the process additive system is added to the process stream in an amount of from 50 to 2000 ppm (mg/L) based on the weight of the process additive system and the volume of the process stream.

16. A method of recovering oil from a process stream of a bioproduct production process, the method comprising the addition of a process additive system to a process stream in a bioproduct production process wherein the process additive system comprises at least one first nonionic surfactant and at least one second nonionic surfactant,

wherein the first nonionic surfactant comprises POE (20) sorbitan monooleate a and the second nonionic surfactant comprises an ethoxylated castor oil,

wherein the ratio by weight of the first nonionic surfactant to the second nonionic surfactant is from 1:1 to 3:1,

wherein the first nonionic surfactant comprises at least 11% of the total weight of the process additive system and the second nonionic surfactant comprises at least 7% of the total weight of the process additive system.

17. A method of recovering oil from a process stream of a bioproduct production process, the method comprising the addition of a process additive system to a process stream in a bioproduct production process wherein the process additive system comprises at least one first nonionic surfactant and at least one second nonionic surfactant,

wherein the first nonionic surfactant comprises POE (20) sorbitan monooleate a and the second nonionic surfactant comprises an ethoxylated castor oil,

wherein the ratio by weight of the first nonionic surfactant to the second nonionic surfactant is from 1:1 to 3:1,

wherein the first nonionic surfactant comprises at least 50% of the total weight of the process additive system and the second nonionic surfactant comprises at least 25% of the total weight of the process additive system.

18. The method of claim 1 wherein the process additive system is added to a process stream prior to the oil separation step wherein the process stream is selected from the group consisting of the thin stillage, syrup concentrate, and combinations thereof.

19. The method of claim 1 wherein the process additive system is added to the process stream via more than one addition point.

20. The method of claim 19 wherein the process additive system is added to the process stream in an amount of from 50 to 2000 ppm (mg/L) based on the weight of the process additive system and the volume of the process stream.

Assignments (15)
RELEASE OF SECURITY INTEREST Recorded Nov 14, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073564/0864 →
SECURITY INTEREST Recorded Nov 14, 2025
From: CHEM-AQUA, INC.; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; NCH CORPORATION; NCH LIFE SCIENCES LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073570/0838 →
RELEASE OF 2023 NOTES PATENT SECURITY INTERESTS Recorded Oct 10, 2025
From: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
To: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 073074/0198 →
SECURITY AGREEMENT (NOTES) Recorded Oct 10, 2025
From: DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 073061/0885 →
SECURITY AGREEMENT (2024 NOTES) Recorded Jun 24, 2024
From: BIRKO CORPORATION; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A., AS NOTES COLLATERAL AGENT
Reel/Frame 067824/0278 →
2023 NOTES PATENT SECURITY AGREEMENT Recorded Jul 7, 2023
From: BIRKO CORPORATION; SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC; DIVERSEY, INC.; DIVERSEY TASKI, INC.; INNOVATIVE WATER CARE GLOBAL CORPORATION
To: BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 064225/0170 →
SECURITY AGREEMENT (NOTES) Recorded Sep 14, 2022
From: SOLENIS TECHNOLOGIES, L.P.; INNOVATIVE WATER CARE, LLC
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A. AS COLLATERAL AGENT
Reel/Frame 061432/0821 →
TERM LOAN PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: GOLDMAN SACHS BANK USA
Reel/Frame 058102/0407 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CITIBANK, N.A.
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058848/0636 →
RELEASE OF SECURITY INTEREST Recorded Nov 10, 2021
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 058856/0724 →
NOTES SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: THE BANK OF NEW YORK MELLON TRUST COMPANY, N.A.
Reel/Frame 058103/0066 →
ABL PATENT SECURITY AGREEMENT Recorded Nov 10, 2021
From: INNOVATIVE WATER CARE, LLC; SOLENIS TECHNOLOGIES, L.P.
To: BANK OF AMERICA, N.A.
Reel/Frame 058102/0122 →
SECOND LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 046629/0213 →
FIRST LIEN NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Jul 20, 2018
From: SOLENIS TECHNOLOGIES, L.P.
To: CITIBANK, N.A., COLLATERAL AGENT
Reel/Frame 046595/0241 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 10, 2018
From: LEWIS, SCOTT ROMAK
To: SOLENIS TECHNOLOGIES, L.P.
Reel/Frame 044586/0620 →
Continuity (2)
Provisional Application 62447077 · Jan 17, 2017
Related Publication 20180200644A1 · Jul 19, 2018
Cited By (1)
US 12,480,142