IP Library Granted Patent US 10,463,768
Granted Patent B2
US 10,463,768 · App. 15/432,606 · Granted Nov 5, 2019

Composite material for tissue restoration

Inventors: Xuesong Jiang (Baltimore, MD); Sashank Reddy (Baltimore, MD); Gerald Brandacher (Baltimore, MD); Hai-Quan Mao (Baltimore, MD); Justin Sacks (Baltimore, MD); Xiaowei Li (Henrico, VA); Kevin Feng (Baltimore, MD); Russell Martin (Baltimore, MD); Georgia C. Yalanis (Milcreek, UT); Ji Suk Choi (Baltimore, MD)
Assignee: The Johns Hopkins University
A61L27/52A61L27/16A61L27/18A61L27/24A61L27/3633A61L27/56A61L27/58A61L27/48A61L2400/06A61L2430/06A61L2430/34
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Quick Facts
Patent No.
US 10,463,768
App. No.
15/432,606
Granted
Nov 5, 2019
Kind
B2
Abstract

A composite material can include a gel and at least one nanostructure disposed within the gel. A method for healing a soft tissue defect can include applying a composite material to a soft tissue defect, wherein the composite material includes a gel and a nanostructure disposed within the gel. A method for manufacturing a composite material for use in healing soft tissue defects can include providing a gel and disposing nanofibers within the gel.

Claims (33)

1. An injectable scaffold complex comprising a polymeric fiber or fragments thereof having a mean diameter of from about 100 nm to about 8000 nm covalently linked to a hydrogel material,

wherein the hydrogel material is capable of forming a network,

wherein the polymeric fiber or fragments comprise functional groups and the surface density of the functional groups on the polymeric fiber or fragments is from about 10 nmole/mg of fibers to about 160 nmole/mg of the fiber or fragments,

wherein the ratio of polymeric fiber or fragments to hydrogel material is from about 1:10 to about 10:1 on a component-mass basis or from about 1 to 50 mg/mL on a concentration basis,

wherein the scaffold complex comprises a plurality of pores, and

the polymeric fiber or fragments thereof comprise a mean length of less than 500 micrometers.

2. The scaffold complex of claim 1 , wherein the scaffold complex is capable of being injected through a 21 gauge or smaller gauge needle.

3. The scaffold complex of claim 1 , wherein the scaffold complex is capable of forming an elastic gel prior to, during, or following injection.

4. The scaffold complex of claim 1 , wherein the scaffold complex is isotropically reinforced.

5. The scaffold complex of claim 1 , wherein the scaffold can form a gel comprising an arbitrary volumetric geometry.

6. The scaffold complex of claim 1 , wherein the polymeric fiber or fragments thereof are uniformly dispersed.

7. The scaffold complex of claim 1 , wherein the hydrogel material is bonded to the outer surface of the polymeric fiber or fragments.

8. The scaffold complex of claim 1 , further comprising a polymeric fiber or fragments thereof non-covalently linked to a hydrogel material,

wherein the hydrogel material is capable of forming a network,

wherein the non-covalent link comprises (i) electrostatic interactions and/or (ii) hydrogen-bonding.

9. The scaffold complex of claim 1 , wherein the polymeric fiber or fragments thereof comprises an electrospun fiber.

10. The scaffold complex of claim 1 , wherein the polymeric fiber or fragments thereof comprises a synthetic polymeric material comprising a poly(lactic-co-glycolic acid), poly(lactic acid), and/or a polycaprolactone, or a combination or derivatives thereof; or a biological polymeric material selected from the group consisting of a silk, collagen, elastin, hyaluronic acid, chitosan, a derivative thereof, and a combination thereof.

11. The scaffold complex of claim 1 , wherein the hydrogel material comprises a poly(ethylene glycol), a collagen, a dextran, an elastin, an alginate, a hyaluronic acid, a poly(vinyl alcohol), a derivative thereof, or a combination thereof.

12. The scaffold complex of claim 1 , wherein the hydrogel material comprises a processed tissue extracellular matrix, wherein the processed tissue extracellular matrix is derivable from an adipose tissue.

13. The scaffold complex of claim 1 , wherein the polymeric fiber or fragments thereof comprise a synthetic polymeric material comprising a poly(lactic-co-glycolic acid), poly(lactic acid), a polycaprolactone, or a combination or derivative thereof,

and wherein the hydrogel material comprises a poly(ethylene glycol), a collagen, a dextran, an elastin, an alginate, a hyaluronic acid, a poly(vinyl alcohol), a derivative thereof, or a combination thereof.

14. The scaffold complex of claim 1 , wherein the plurality of pores are present on a surface of the scaffold complex and within the scaffold complex,

wherein the pores are present at a concentration of at least about 50 pores per square centimeters of the surface,

and wherein at least 80% of the pores have an average pore diameter of at least 5 micrometers.

15. A medical device for retaining tissue shape in a subject undergoing a surgical procedure, comprising the scaffold complex of claim 1 in an amount effective to provide for the retention of a tissue shape when administered to the subject.

16. An injectable scaffold complex comprising a polymeric fiber or fragments thereof having a mean diameter of from about 100 nm to about 8000 nm covalently linked to a hydrogel material,

wherein the hydrogel material is capable of forming a network;

the ratio of polymeric fiber to hydrogel material is from about 1:10 to about 10:1 on a component-mass basis or from about 1 to 50 mg/mL on a concentration basis;

wherein the polymeric fiber or fragments comprise functional groups and the surface density of the functional groups on the polymeric fiber or fragments is from about 10 nmole/mg of fibers to about 160 nmole/mg of the fiber or fragments

the hydrogel material is bonded to the outer surface of the polymeric fiber or fragments; and

the polymeric fiber or fragments thereof comprises an electrospun fiber.

17. The scaffold complex of claim 1 , wherein the scaffold complex further comprises a crosslinking agent, wherein the crosslinking agent comprises poly(ethylene glycol) diacrylate (PEGDA), thiolated poly(ethylene glycol) (PEGSH), or combination thereof.

18. The scaffold complex of claim 1 wherein the functional groups comprise maleimide groups.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 18, 2018
From: JIANG, XUESONG; REDDY, SASHANK; BRANDACHER, GERALD; MAO, HAI-QUAN; SACKS, JUSTIN; LI, XIAOWEI; FENG, KEVIN; MARTIN, RUSSELL; YALANIS, GEORGIA C.; CHOI, JI SUK
To: THE JOHNS HOPKINS UNIVERSITY
Reel/Frame 047597/0802 →
Continuity (3)
Continuation PCTUS2015045494 · Aug 17, 2015
Provisional Application 62038030 · Aug 15, 2014
Related Publication 20180050130A1 · Feb 22, 2018